SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Discrimination of combustion fuel sources using gas chromatography-planar field asymmetric-waveform ion mobility spectrometry Conditions Instrument 1144 Smoke plumes Journal of Separation Science (2003) 26 (6-7), 585-593. Eiceman, Gary A.; Funk, Paul A.; Hughs, S. Edgar; Miller, Raanan A.; Nazarov, Erkijon G.; Tarassov, Alexander GC-MS Potential of solid-phase microextraction fibers for the analysis of volatile organic compounds in air. 1175 VOCs in air Journal of Chromatographic Science (2001) 39(12), 521-529 Various fibers compared Tuduri, Ludovic; Desauziers, Valerie; Fanlo, Jean Louis Sampling and sample-preparation strategies based on solid-phase microextraction for analysis of indoor air. 1187 Trends in Analytical Chemistry (2002) 21 (12), 840-850. Koziel, J. A.; Novak, I. 1194 PAHs Screening direct analysis of PAHs in atmospheric particulate matter with SPME Talanta (2003) 60 (4), 687-693. Vaz, Jorge Moreira PDMS PAHs in air 2606 Monitoring of PAHs in air by collection on XAD-2 adsorbent then microwave-assisted thermal desorption coupled with headspace 65µm PDMS/DVB GC-MS SPME and GC with mass spectrometric detection. headspace Anal. Bioanal. Chem. 387, #3, 999-1005 (2007-02) 35°C for 40 min. Wei, M. C.; Chang, W. T.; Jen, J. F. sat. salt Determination of benzene at trace levels in air by a novel method based on solid phase microextraction gas chromatography/mass spectrometry. 1200 Benzene in air Rapid Communications in Mass Spectrometry (2001) 15(24), 2404-2408 GC-ITMS Salvadori, Piero; Cuzzola, Angela; Pucci, Sergio; Raffaelli, Andrea; Saba, Alessandro Determination of volatile aliphatic amines in air by solid-phase microextraction coupled with gas chromatography with flame ionization detection Volatile aliphatic 1305 amines in air. Journal of Chromatography, A (2003) 1016 (1), 1-9. Jastrzebska, Anna; Namiesnik, Jacek; Zygmunt, Bogdan GC-FID Solid phase microextraction sampling and gas chromatography/mass spectrometry for field detection of the chemical warfare agent O-ethyl S-(2diisopropylaminoethyl) methylphosphonothiolate (VX) Chemical warfare 1313 agents Journal of Separation Science (2003) 26 (12-13), 1091-1096. Betsinger, Geoffrey; Hook, Gary L.; Kimm, Gregory; Logan, Tom; Savage, Paul B.; Smith, Philip A.; Swift, Austin Various GC-MS Characterisation of odorants emissions from landfills by SPME and GC/MS Odorant emissions 1334 from landfills. Chemosphere (2003) 51 (5), 357-368. DVB/Carboxen/PDMS GC/MS Davoli, E.; Gangai, M.L.; Morselli, L.; Tonelli, D. 1342 A simple calibration procedure for volatile organic compounds sampling in air with adsorptive solid-phase microextraction fibres. Analyst (2003) 128 (9), 1028-1032. PDMS/CAR GC-FID Tuduri, L.; Desauziers, V. *; Fanlo, J. L. Screening for sarin in air and water by solid-phase microextraction-gas chromatography-mass spectrometry. 1373 Sarin in air and water. Journal of Chromatographic Science (2001) 39(10), 420-424. Schneider, J. F.; Boparai, A. S.; Reed, L. L. GC-MS Determination of perfume oil in household products by headspace solid-phase microextraction and fast capillary gas chromatography. Ambient temperature, unless otherwise indicated. 208
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Perfume oil in Literature Reference Conditions Instrument 1186 household products. Chromatographia (2003) 57 (Supp), S199-S206. Bothe, F.; Dettmer, K.; Engewald, W. * Various FCGC Volatile organic compounds produced during irradiation of mail. VOC's from irradiated 1141 mail. AIHA Journal (2003) 64 (2), 189-195. Smith, Philip A.; Hakspiel, Shelly J.; Miller, Stephen; Sheely, Michael V. Evaluation of solid-phase microextraction for time-weighted average sampling of volatile sulfur compounds at ppb concentrations 1126 Sulfur compounds Analytical Chemistry (2003) 75 (11), 2626-2632. Andersson, Fras Annika T.; Desauziers, Valerie; Fanlo, Jean-Louis; Lestremau, Francois Carboxen/PDMS Determination of low-level residual ethylene oxide by using solid-phase microextraction and gas chromatography. 1098 Ethylene oxide Journal of AOAC International (2002) 85 (6), 1205-1209. Ayoub, K.; Harris, L.; Thompson, B. 1447 Volatile compounds in air Characterization of volatile effluents of livestock buildings by solid-phase microextraction Int. J. Environ. Anal. Chem. (2003) 83(10), 837-849 75um Carboxen PDMS GC-MS Begnaud, Frederic; Berdague, Jean-Louis; Peres, Christophe Development of a personal isocyanate sampler based on DBA derivatization on solid-phase microextraction fibers. 1476 Isocyanates in air Fresenius' Journal of Analytical Chemistry (2001) 371(4), 514-518 Nilsson, Ulrika; Batlle, Ramon; Colmsjo, Anders Traditional sampling with laboratory analysis and solid phase microextraction sampling with field gas chromatography/mass spectrometry by military industrial hygienists. 1478 Volatiles in air AIHAJ (2002) 63(3), 284-292 Thomas, Richard J.; Smith, Philip A.; Lee, Arthur P.; Kluchinsky, Timothy A., Jr.; Erickson, Richard P.; Savage, Paul B.; Stevens, Michael; Williams, Kenneth 1479 VOCs in air Solid phase microextraction : Measurement of volatile organic compounds (VOCs) in Dhaka City air pollution. Journal of Environmental Science and Health Part A Toxic-Hazardous Substances & Environmental Engineering (2002) A37(7), 1223-1239 Hussam, A.; Alauddin, M.; Bhattacharjee, M.; Bibi, H.; Chowdhury, D.; Khan, A. H.; Sultana, S. Gas chromatographic determination of glutaraldehyde in the workplace atmosphere after derivatization with O-(2,3,4,5,6pentafluorobenzyl)hydroxylamine on a solid-phase microextraction fibre. 1523 Glutaraldehyde in air Journal of Chromatography A (2002) 955(1), 117-124 1524 Valeraldehyde in air (TWA) 1543 Nicotine in air Pieraccini, Giuseppe; Bartolucci, Gianluca; Boccalon, Pierpaolo; Dugheri, Stefano; Focardi, Leonardo; Pacenti, Marco Time-weighted average sampling of airborne n-valeraldehyde by a solid-phase microextraction device. Journal of Chromatography A (2002) 954(1-2), 191-198 Tsai, S.-W.; Chang, T.-A. Trace analysis of nicotine in indoor air by a SPME method. Bulletin of Environmental Contamination and Toxicology (2002) 68(4), 485- 489 Shuokui, H.; Huali, Y.; Jianfang, F.; Songting, G. Ambient temperature, unless otherwise indicated. 209 65um PDMS/DVB, dibutylamine (DBA) derivative On-fiber derivatization with PFBHA 65um DVB PDMS, onfiber derivatization with PFBHA HPLC-MS GC-MS GC GC-FID
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