SPME Applications Guide - Overbrook Scientific

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1528 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Dynamic air sampling of volatile organic compounds using solid phase microextraction VOCs in air (dynamic sampling) Journal of Environmental Science and Health Part B Pesticides Food Contaminants and Agricultural Wastes (2002) B37(4) 365-378 Razote, Edna; Chobpattana, Wannee; Jeon, Ike; Maghirang, Ronaldo Configurations and calibration methods for passive sampling techniques 2674 passive sampling J. Chromatogr. A 1168, #1-2, 226-235 (19 OCT 2007) Ouyang, G.; Pawliszyn, J. 75um Carboxen PDMS GC-MS 2747 Volatile organics Compound-specific carbon isotope analysis of volatile organic compounds in water using solid-phase microextraction 75um Carboxen GC-MS in water J. CHROMATOGR. A 1163, #1-2, 260-268 (07 SEP 2007) headspace and Palau, J.; Soler, A.; Teixidor, P.; Aravena, R. immersion 2656 Volatiles in water Time-weighted average water sampling with a diffusion-based SPME J. Chromatogr. A 1138, #1-2, 42-46 (Jan 5 2007) PDMS coatings GC passive sampling Alaee, Mehran; Ouyang, Gangfeng; Pawliszyn, Janusz; Zhao, Wennan 2638 Volatiles in water Time-weighted average water sampling in Lake Ontario with SPME passive samplers PDMS coatings GC passive sampling Environ. Sci. Technol. 41, #11, 4026-4031 (Jun 1 2007) Alaee, M.; Bragg, L.; Ouyang, G.; Pawliszyn, J.; Qin, Z.; Zhao, W. 1547 Evaluation of indoor exposition to benzene, toluene, ethylbenzene, xylene, and styrene by passive sampling with a solid-phase microextraction device. Volatiles in air (passive Journal of Chromatographic Science (2002) 40(3), 122-126 sampling) Cardeal, Zenilda de L.; de Carvalho, Ciomara R.; Parreira, Fabricio V. 100um PDMS, 65um DVB PDMS 1388 Perfumes Atmospheric lifetimes and fates of selected fragrance materials and volatile model compounds. Environmental Science and Technology (2001) 35(18), 3595-3600. Aschmann, S. M.; Arey, J.; Atkinson, R. *; Simonich, S. L PDMS GC-MS Measuring the effect of photocatalytic purifiers on 2111 Hydrocarbons indoor air hydrocarbons and carbonyl pollutants 15 min sampling GC in air J. Air Waste Manage. Assoc., 55, #1, 88-96 Disdier, Jean; Mas, Denis; Pichat, Pierre Air sampling of aromatic hydrocarbons in the 2112 BTEX presence of ozone by SPME 100µm PDMS GC-FID, GC-MS in air J Chromatogr A, 1025, #1, 57-62 headspace Xiong, G; Koziel, J.; Pawliszyn, J. Sampling and analysis of PCBs in indoor air by 2113 PCBs in sorbent enrichment followed by headspace headspace GC-MS indoor air SPME and GC-MS J. Chromatogr. A,1072, #1, 99-106 Ares, S; Barro, R; Cela, R; Garcia-Jares, C; Llompart, M Air sampling of organophosphate triesters using 2114 Organo- SPME under non-equilibrium conditions. 100µm PDMS GC phosphate Anal & Bioanalytical Chem, 378, #7, 1847-1853 1 hr. sampling triesters in Isetun, S.; Nilsson, U.; Colmsjo, A.; Johansson, R. air Evaluation of SPME w/ PDMS for air sampling of 2115 Organo- gaseous organophosphate flame-retardants 100µm PDMS GC phosphate and plasticizers 8 hrs. sampling triesters in Anal & Bioanalytical Chem, 380, #2, 319-324 Air Isetun, Sindra; Nilsson, Ulrika; Colmsjo, Anders Suitability of SPME for the determination of organophosphate 2328 Flame retardants flame retardants and plasticizers in water samples 65µm PDMS-DVB GC-NPD & plasticizers J. Chromatogr. A 1108 #2, 158-165 (2006) Direct extraction in water Calvo, F.; Cela, R.; Quintana, J.B.; Rodil, R.; Rodriguez, I.; Rubi, E. 40 min @ 21°C NaCl added Investigation of artefact formation during analysis 2116 Volatile of volatile sulfur compounds "in air" using SPME 75µm Carboxen GC sulfur Chromatographiam 59, #9-10, 607-613 direct air sample Ambient temperature, unless otherwise indicated. 210
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument compounds Lestremau, F.; Andersson, F.; Desauziers, V. * in air Determination of benzene, toluene, ethylbenzene and 2117 BTEX in xylenes in air by SPME-GC-MS 75µm Carboxen GC-MS air Analytical & Bioanalytical Chem, 380, #5-6, 824-830 30 min sampling Tumbiolo, S.; Gal, J. -F.*; Maria, P. -C.; Zerbinati, O. SPME sampling of BTEX before GC/MS analysis:Examples of outdoor 2174 BTEX in and indoor air quality measurements in public and private sites GC-MS air Annali di Chimica 95, #11-12, 757-766 (2005) Tumbiolo, S.; GAL, Jean-Francois; Maria, P.; Zerbinati, O. Use of SPME for the detection of acetic acid by ion-trap 2118 Acetic acid GC-MS and application to indoor levels in museums GC-ITMS in air J. Chromatogr. A, 1067, #1-2, 331-336 Godoi, Ana F.L.; Van Grieken, Rene; Van Vaeck, Luc Development of a sensitive methodology for the 2119 Chloro- analysis of chlorobenzenes in air bycombination of 65µm PDMS-DVB GC-MS benzenes SPE and headspace SPME 65µm CW GC-ECD in air J. Chromatogr. A, 1045, #1-2, 189-196 headspace Ares,S; Barro,R; Cela,R; Garcia-Jares,C; Llompart,M Dynamic SPME for sampling of airborne sarin with 2120 Sarin in Air GC-MS for rapid field detection and quantification Direct sampling of air GC-MS J. Sep. Sci., 27,#12, 1017-1022 Hook, G.; Lepage, C; Miller, S.; Smith, P. Analysis of sulfur-containing compounds in ambient air 2121 Sulfur compd using SPME-GC with pulsed FPD direct sampling GC-FPD in air Int. J. Environ. Anal. Chem., 84, #10, 749-760 Li, Kwong-Chi; Shooter, David Determination of aniline in silica gel sorbent by one-step 2122 Aniline in situ microwave assisted desorption coupled to 65µm PDMS-DVB GC-FID in air headspace SPME and GC-FID headspace Talanta, 64, #3, 650-654 3 min extraction Jen, Jen-Fon; Shih, Ton-Sheng; Yan, Cheing-Tong Propylene glycol vapor contamination in controlled 2123 Popylene environment growth chambers: Toxicity to corn and headspace MD-GC-MS glycol in soybean plants air J. Environ. Sci. Health Part B, 40, #3, 443-448 McConnell, Laura; Niu, Genhua; Reddy, Vangimalla R. Theory / Technique 856 Volatiles An automated method for the determination of some volatile organic compounds in water samples after extraction by GC-ECD in water SPME and CGC-ECD analysis Rev. Port. Farm (2000) 50(4) 141-149 Cunha, E.; Goncalves, C.; Alpendrurada, M. F. (Portuguese) 2 VOCs, BTEX, PAHs Solid Phase MicroExtraction with Thermal Desorption Using Fused Silica Optical Fibers 56µm PDMS GC-FID, in water Anal. Chem. 62: 2145-2148 (1990) 2 min GC-ECD Arthur, C., Pawliszyn, J. stirring, salt added 5 BTEX Solid Phase MicroExtraction: An Attractive Alternative Environmental Lab. 11, Dec/Jan 1992/1993 pp 10-15 100µm PDMS GC-FID in water Arthur, C., Killam, L., Chai, M., Buchholdz, K., Potter, D., 14 min Zhang, Z., Pawliszyn, J. Automation and Optimization of Solid Phase MicroExtraction stirring salt added 9 BTEX Anal. Chem. 64: 1960-1966 (1992) 56µm & 100µm PDMS GC-FID in water Arthur, C., Killam, L., Buchholz, K., Pawliszyn, J. 2-40 min stirring, salt added 2392 PAHs Automation of solid-phase microextraction on a 96-well plate format J. Chromatogr., A 1149, #2, 127-137 (2007-05-18 ) PDMS fibers in water Hutchinson, J. P.; Setkova, L.; Pawliszyn, J. Ambient temperature, unless otherwise indicated. 211
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