SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
2545 Volatiles from microwave assisted extraction associated with SPME headspace GC-MS
mulberry leaves Chemistry and Industry of Forest Products 27, #3, 107-110 (2007)
Li JieHong; Chen DaiWu
2436 Fenitrothion in
Quantification of fenitrothion and its main metabolites in poplar leaves
by isotope dilution GC-MS coupled with SPME GC-MS
poplar leaves J. Chromatogr. A 1177, #1, 170-174 (Jan 4 2008)
Barrio, R.; Goicolea, M.; Millan, S.; Rodriguez, E.; Sampedro, M.;
Sanchez, A.; Unceta, N.
Changes in volatile compounds of small gamma -irradiated fresh cilantro leaves
during cold storage.
Volatile compounds
1085 from cilantro Journal of Agricultural and Food Chemistry (2002) 50 (26), 7622-7626.
Fan, X. T.; Sokorai, K. J. B.
GC-MS
1086 Ethanol in Tequila
Tequila authenticity assessment by headspace SPME-HRGC-IRMS analysis of
carbon-13/carbon-12 and oxygen-18/oxygen-16 ratios of ethanol.
Journal of Agricultural and Food Chemistry (2002) 50 (26), 7520-7523. GC-MS
1087
1088
Aguilar-Cisneros, B. O.; Lopez, M. G.; Richling, E.; Heckel, F.; Schreier, P. *
Survey on the presence of butyltin compounds in Chinese alcoholic beverages,
determined by using headspace solid-phase microextraction coupled with gas
chromatography-flame photometric detection.
Butyltin compounds in
alcoholic beverages Journal of Agricultural and Food Chemistry (2002) 50 (23), 6683-6687.
Liu, J. Y.; Jiang, G. B.*
GC-MS
Synthesis and stable isotope dilution assay of ethanethiol and diethyl disulfide
in wine using solid phase microextraction. Effect of aging on their levels in wine.
Ethanediol and diethyl
disulfide in wine. Journal of Agricultural and Food Chemistry (2002) 50 (23), 6653-6658. GC-MS
Majcenovic, A. B.; Schneider, R.; Lepoutre, J. -P.; Lempereur, V.; Baumes, R. *
Differential effects of tomato ( Lycopersicon esculentum Mill) matrix on the
volatility of important aroma compounds.
Aroma compounds
1089 from tomatoes. Journal of Agricultural and Food Chemistry (2003) 51 (3), 722-726.
Bezman, Y.; Mayer, F.; Takeoka, G. R.; Buttery, R. G.; Ben-Oliel, G.;
Rabinowitch, H. D.; Naim, M.
Stale flavour volatiles in Australian commercial UHT milk
2246 Flavour volatiles during storage headspace GC-FiD
in milk Australian J Dairy Technology 60, #3, 231-237 (2005)
Perkins, M.; Elliott, A.; D'Arcy, B.; Deeth, Hilton C.
Volatile fraction of milk: comparison between purge and trap and solid phase
microextraction techniques.
1090 Volatile fraction of milk Journal of Agricultural and Food Chemistry (2002) 50 (25), 7350-7355.
Contarini, G.; Povolo, M.
SPME applied to the study of volatile organic compounds emitted by three
species of Eucalyptus in situ.
VOC's from
1091 eucalyptus. Journal of Agricultural and Food Chemistry (2002) 50 (25), 7199-7205.
Zini, C. A.; Augusto, F.; Christensen, E.; Caramao, E. B.; Pawliszyn, J. *
65 um PDMS/DVB GC-MS
1105 Volatiles in mango
Headspace solid-phase microextraction and gas chromatography-mass
spectrometry analysis of free volatile compounds in Mango.
Chromatographia (2002) 55(11-12), 737-741
Shang, C. Q.; Deng, C. H.; Zhang, X. Y.; Chen, Z. F.; Hu, Y. M.
GC-MS
Optimization of headspace SPME-GC-AED analysis
Ambient temperature, unless otherwise indicated. 29