SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Marques, E; Vieira, D. N.; Lopez-Rivadulla, M. immersion sampling
Development of headspace SPME w/ on-fiber derivatization
1881 Hexanal, for determination of hexanal and heptanal in human blood 65µm PDMS-DVB GC-MS
heptanal J Chromatogr, B: 813, #1-2, 47-52 8min @ 60°C
in blood Deng, C. H.; Li, N.; Zhang, X. M.* PFBHA derivatives
headspace
Determination of low level methyl tert-butyl ether, ethyl tert-butyl ether
2585 TAMEM, MTBE, and methyl tert-amyl ether in human urine by HS-SPME GC-MS headspace GC-MS
ETBE and ANAL. CHIM. ACTA: 581,#1, 53-62 (02 JAN 2007) 65µm PDMS-DVB
in urine Scibetta, L.; Campo, L.; Mercadante, R.; Foa`, V.; Fustinoni, S.
Identification and elimination of polysiloxane curing agent
1882 Methyl tert- interference encountered in the quantification of low- headspace GC-MS
butyl ether picogram per milliliter methyl tert-butyl ether in blood by
in blood SPME headspace analysis
Anal. Chem, 77,#9, 2912-29-19.
Blount, Benjamin C.; Chambers, David M.; Hughes, T.;
Mauldin, J.; McElprang, David
SPME coupled w/ ion mobility spectrometry for the
1883 Ephedrine analysis of ephedrine in urine immersion sampling IMS
in urine J. Sep. Sci.28. #7,612-618
Lokhnauth, John K.; Snow, Nicholas H.
Determination of ethanol in human blood and urine by
1884 Ehtanol in automated headspace SPME and capillary GC headspace GC
biological Anal. Chim. Acta, 522, #2, 163-168
fluids De Martinis, B.; Martins R., Maria A.; Santos M., Carmen C.
A simple, rapid and sensitive method for determination
1885 Aldehydes in aldehydes in human blood by GC-MS and SPME PFBHA derivative GC-MS
blood with on-fibre derivatization. headspace
Rapid Communications in Mass Spect, 18, #15, 1715-1720
Deng, C. H.; Zhang, X. M.*
Identification of components responsible for the odor of cigar
2164 Odorous smoker's breath headspace GC-MS
compounds in J Ag Food Chem, 54, #2, 497-501 (2006)
SPME for analysis of alkanes and aromatic hydrocarbons in
2218 Hydrocarbons in human breath GC
breath J. Chromatogr. B, 826, #1-2,69-74 (2005)
Yu, Hao; Xu, Liang; Wang, Ping
Determination of acetone in human breath by GC-MS
1886 Acetone in and SPME with on-fiber derivatization 65µm PDMS-DVB GC-MS
human breath J. Chromatogr. B , 810, #2, 269-275 PFBHA derivative
& plasms Deng, Ci; Yu, X; Zhang, J; Zhang, W Zhang, X 4 min extract
agitated
Impact of inspired substance concentrations on the results
1887 Breath marker of breath analysis in mechanically ventilated patients headspace GC-MS
in blood & Biomarkers, 10, #2-3, 138-152
breath Schubert, J.; Miekisch, W.; Birken, T.; Geiger, K.;
Noelge-Schomburg, G
Capillary LC determination of cellular flavins
1888 Flavins J. Chromatogr. A, 1053, #1-2, 71-78 in-tube silica-ODS LC-MS
Jia, Li; Tanaka, Nobuo; Terabe, Shigeru
Study of ligand-receptor binding using SPME: Investigation
1889 Protein of receptor, free, and total ligand concentrations restricted access LC-MS
binders J of Proteome Res, 4, #3, 789-800 molecularly imprinted
Musteata, Florin Marcel; Pawliszyn, Janusz immobilized antibodies
Determination of sterols in biological samples by SPME
1890 Sterols in with on-fiber derivatization and GC/FID BSTFA derivative GC-FID
serum Anal. Bioanal. Chem., 381, #8, 1576-1583 headspace
samples Domeno, Celia; Nerin, Cristina; Ruiz, Barbara
Poly (methacrylic acid-ethylene glycol dimethacrylate)
1891 Basic drugs monlithic capillary for intube SPME coupled to HPLC and its polymethacrylate HPLC-UV
in serum application to determination of basic drugs in human serum coated tube
Anal. Chim. Acta, 523, #2. 251-258
Da, Shi-Lu; Fan, Yi; Feng, Yu-Qi; Shi, Zhi-Guo
Ambient temperature, unless otherwise indicated. 108