SPME Applications Guide - Overbrook Scientific

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1540 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Pragst, Fritz; Huebner, Sandra; Mills, Graham; Sporkert, Frank Conditions Instrument carbamazepine, carbamazepine epoxide, phenytoin, phenobarbital, and primidone in human plasma Determination of lamotrigine simultaneously with carbamazepine, carbamazepine epoxide, phenytoin, phenobarbital, and primidone in human plasma by SPME-GC-TSD. Journal of Chromatographic Science (2002) 40(4), 219-223 Lancas, F. M.; Carvalho, D.; Queiroz, M. E. C.; Silva, S. M. 1427 Microcystins Determination of microcystins in cyanobacterial blooms by solid-phase microextraction : High-performance liquid chromatography. Environmental Toxicology and Chemistry (2001) 20(8), 1648-1655. HPLC Lam, Michael Hon-wah; Lam, Paul K. S.; Poon, Ka-Fai; Wong, Bryan S. F. New trends in hair analysis and scientific demands on validation 2597 Review of Trends and technical notes forensic analysis Forensic Sci Intl 165, #2-3, 204-215 (JAN 17 2007) Musshoff, Frank; Madea, Burkhard Simple and sensitive determination of tetrahydrocannabinol, cannabidiol 2516 Cannabinols and cannabinol in hair by combined silylation, headspace SPME-GC-MS Headspace GC-MS in hair J. CHROMATOGR. B 846, #1-2, 78-85 (01 FEB 2007) trifluoroacetamide Nadulski, T.; Pragst, F derivative Rapid screening procedure based on headspace 1828 Drugs in SPME-GC-MS for the detection of many Headspace, GC-MS hair recreational drugs in hair. 5min @ 90°C J. Chromatogr. B, 801, #2, 289-296 Gentili, S.; Cornetta, M.; Macchia, T. * Determination of methyl and ethyl esters of methanesulfonic, 2273 Sulfonic acids benzenesulfonic and p-toluenesulfonic acids in active pharmaceutical GC-MS esters in ingredients by solid-phase microextraction pharmaceutical J Pharma Biomedical Analysis, 39, #3-4, 477-485 (2005) ingredients Colon, Ivelisse; Richoll, Stephen M. Optimisation of a SPME method for the determination of parabens in 2709 Parabens in water samples at the low ng per litre level 85µm polyacrylate GC-MS/MS water J. Chromatogr. A, 1124, #1-2, 3-10 (2006-08-18) immersed Canosa, P.; Rodriguez, I. ; Rubi, E.; Bollain, M. H.; Cela, R. TBMS derivative sat. salt Determination of parabens in pharmaceutical formulations by 1829 Parabens in SPME ion-mobility spectrometry GC-IMS pharmaceutics Anal. Chem., 77, #18, 5938-5946 Lokhnauth, John; Snow, Nicholas Simultaneous derivatization and extraction of amphetamine-like 1830 Amphetamine drugs in urine with headspace SPME followed by GC-MS 100µm PDMS GC-MS drugs in Anal. Chim. Acta, 539, #1-2, 49-54 30min @ 90°C urine Chia, Kan-Jung; Huang, Shang-Da HFBA derivative headspace Poly(methacrylic acid-ethylene glycol dimethacrylate) 1831 Amphetamine monolith in-tube SPME coupled to HPLC and analysis of polycrylate coated HPLC-UV drugs in amphetamines in urine samples capillary tube urine J. Chromatogr. A, 1074, #1-2, 9-16 Da, Shi-Lu; Fan, Yi; Feng, Yu-Qi; Zhang, J; Zhang, M Application of SPME combined with derivatization to 1832 Amphetamine the determination of amphetamines by liquid chromatog 50µm CW-TPR HPLC-UV drugs in Analytical Biochemistry, 333, #2, 328-335 FMOC derivative urine Chafer-Pericas, C.; Campins-Falco, P.; Herraez-Hernandez, R. 1833 Amphetamine Enantiomeric determination of amphetamines: Exploring A novel one-step SPME-based approach 100µm PDMS GC-SIM-MS drugs in J. Chromatogr. B, 825, #1, 79-87 10min @ 70°C urine Wang, Sheng-Meng SPME with LC-electrospray ionization-tandem MS prolyl chloride derivative 1834 Amphetamine for analysis of amphetamine and methamphetamine in serum LC-ESI-MS/MS Ambient temperature, unless otherwise indicated. 102
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in serum Anal. Chim. Acta, 538, #1-2, 49-56 Chou, Chi-Chi; Lee, Maw-Rong Comparison and classification of methamphetamine seized in Japan 2800 Methyl and Thailand using GC with liquid-liquid extraction and SPME GC-FID amphetamine Forensic Science International 175, #2-3, 85-92 (MAR 5 2008) Kuwayama, K.; Inoue, H.; Phorachata, J.; Kongpatnitiroj, K.; Puthaviriyakorn, V.; Tsujikawa, K.; Miyaguchi, H.; Kanamori, T.; Iwata, Yuko T.;Kamo, Naoki; Kishi, Tohru Excretion of unchanged volatile organic compounds (toluene, 2836 Volatile organics ethylbenzene, xylene and mesitylene) in urine as result of headspace GC in human urine experimental human volunteer exposure Intl Archives of Occupational Environ. Health 81, #4, 443-449 (2008) Janasik, Beata; Jakubowski, Marek; Jalowiecki, Piotr Quantitative analysis of benzene, toluene, 1835 BTX solvents and xylenes in urine by headspace SPME headspace GC-MS in urine J Chromatogr A, 1027, #1-2, 37-40 Alkalde, T; Peralba, M; Zini, C; Caramao, E. SPME w/ on-fiber derivatization for the determination of 1836 PCB metabolite hydroxy-polychlorinated biphenyl compounds in urine 65µm PDMS-DVB GC/MS in urine Anal. Chim. Acta, 539, #1-2 55-60 60min @ 90°C Hong, Jee Eun; Lee, Won; Park, Song-Ja; Pyo, Heesoo BSTFA derivative headspace Single drop microextraction or SPME-GC-MS 1837 Iodine in for the determination of iodine in pharmaceuticals, iodate derivatives GC various iodized salt, mil powder and vegetables matrices involving conversion into 4-iodo-N,N-dimethylaniline J Chromatogr A, 1023, #1, 33-39 Das, P; Gupta, M; Jain, A; Verma, K. Determination of quinalphos in blood and urine by direct SPME 2315 Quinalphos in combined with GC-MS 100µm PDMS GC/MS blood J. Chromatogr. B 832 #1, 162-168 (2006) direct Barroso, M.; Cruz, A.; Gallardo, E.; Lopez-Rivadulla, M.; Margalho, C.; Vieira, D.N Investigations on the medico-legal relevance of spirits containing 2290 Thujone thujone with special regard to toxicological-analytical aspects headspace GC/MS in blood Blutalkohol 42 #4, 263-271 (2005) (German) Kroner, L.; Padosch, S.; Lachenmeier, D.; Madea, B. Monitoring of drugs and metabolites in whole blood 1838 Diazipenes in by restricted-access SPME coupled to LC-MS restricted access LC-MS biological fluid J Chromatogr A, 1025, #1, 85-92 coated fibers Walles, M.; Mullett, W. M.; Pawliszyn, J. headspace An accurate and sensitive method for determination 1839 Methyl methylmercury in biological specimens 100µm PDMS ICP-MS mercury from using GC-ICP-MS with solid phase microextraction methyl, ethyl, phenyl biological J Anal At Spectrom, 19, #12, 1546-1551 derivatives specimens Christopher, S.J.; Davis, W. Clay; Day, Rusty D.; microwave extraction Long, S.E.; Schantz, Michele M.; Vander Pol, Stacy S. Sampling and analysis of volatile organic compounds 1840 Volatiles in in bovine breath by SPME-GC-MS 50/30µm DVB/CAR GC-MS bovine breath J Chromatogr A, 1025, #1, 63-69 15min @ 22°C Spinhirne, J.; Koziel, J.; Chirase, N. headspace High-throughput analysis of phthalate esters in 1841 Phlated esters human serum by direct immersion SPME followed 85µm polyacrylate GC-MS in serum by isotope dilution-fast GC/MS direct immersion Anal. Bioanal. Chem., 380,#2, 275-283 Colon, Ivelisse; Dimandja, Jean-Marie D. Development of pressurized hot water extraction 1842 Ligustilides followed by headspace SPME-GC-MS determination headspace GC-MS in Chinese ligustilides in Ligusticum chuanxiong and Angelica sinensis medicines J. Sep. Sci., 28, #11, 1237-1243 Deng, Chunhui; Ji, Jie; Wang, Xiaochuan; Zhang, X 1843 Benzene Urinary benzene determination by SPME/GC-MS: A study of variables by fractional factoria 1 min @ 15°C GC-MS from urine design and response surface methodology headspace Ambient temperature, unless otherwise indicated. 103
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SPME Literature Literature No. Titl
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