SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 39 Halogenated volatiles Application of SPME to the Headspace GC Analysis of GC in food Halogenated Volatiles in Selected Foods J. Chromatogr. 648 (1): 199-211 (1993) Page, B., Lacroix, G. 41 Fatty acids C2-C10 Determination of Fatty Acids Using SPME 85µm polyacrylate GC/GC-MS in water Anal. Chem: 67(23): 4396-4403 (1995) Low pH, salt Pan, L., Adams, M., Pawliszyn, J. derivative: 1-pyrenediazomethane 2646 Volatiles from Chemical composition and volatile constituents of Anthyllis barba-jovis headspace GC-MS flavonol NAT. PROD. RES. 21, #5, 418-425 (01 MAY 2007) glycosides Pistelli, L.; Noccioli, C.; Bertoli, A.; Scapecchi, G.; Potenza, D. 2176 Volatile organics Headspace solid-phase microextraction analysis of artificial flavors headspace GC-MS from artificial J Sci of Food and Agri., (2005) 85, #25, 2645-2654 30 min flavors Coleman, William M.; Dube, Michael F. 42 Flavors in Measuring Flavors Using SPME 100µm PDMS GC-MS corn oil Food Quality January/February 1995, pp40-41 Mindrup, R. 40°C, 45 min 925 Flavors, off-flavors Sample preparation for the analysis of flavors and Review article in food off-flavors in foods J. Chromatogr A, 2000, 873(1), 3-11 Wilkes, J., Conte, E., Kim, Y., Holcomb, M., Sutherland, J. Miller, D. 883 Flavors in Recent application of SPME for monitoring flavor 75µm Carboxen/PDMS GC-MS food components in foods Food Testing & Analysis Feb./March 2000, 17-20 Mindrup, R. 65µm DVB/PDMS 181 Flavors in SPME Associated with Microwave Assisted 100µm PDMS SIM GC-MS coffee, potato Extraction of Food Products pH 2, salt chip J. High Res. Chromatogr. 20 (4): 213-216 (1997) headspace Wang, Y., Bonella, M., Khaled, M., McNair, H. 10 min 60 Sulfur volatiles in Headspace SPME Analysis of Volatile Organic Sulfur truffle aroma Compounds in Black and White Truffle Aroma J. Agric. Food Chem, 43 (8): 2138-2143 (1995) Pelusio, F., Nilsson, T., Tino, R., Larsen, B., Montnarell, L. 830 Sulfur compounds Changes of aroma in shell eggs from egg shell Czech J. Food Sci (2000) 18, 231-233 Adamiec, J.; Dolezal, M.; Mikova, K.; Davidek, J 831 Sulfur compounds Limitations to the use of SPME for quantitation of mixtures of volatile organic sulfur compounds Anal. Chem (2001) 73(7) 1646-1649 Murray, R. A. 2245 Aroma Aroma active compounds of Bulgogi GCO compounds Journal of Food Science (2005) 70 #8, C517-C522 of Bulgogi Ko, H.; Kim, T.; Cho, I.; Yang, J; Kim, Y.; Lee, H. 604 Aroma compounds Determination of major aroma impact compounds in 75µm Carboxen/PDMS GC-MS in fermented fermented cucumbers by SPME-GC-MS- 20min @50°C cucumbers Olfactometry detection J. Chromatogr. Sci. (2000), 38(7), 307-314 Marsili, R., Miller, N. NaCl added 61 Flavors in SPME of Flavor Compounds -- A Comparison of Two Fiber 100µm PDMS, GC-FID cinnamon bark Coatings and Discussion of the Rules of Thumb for Adsorption 85µm polyacrylate LC-GC 13 (11): 882-886 (1995) 120°C Yang, X., Peppard, T. headspace Ambient temperature, unless otherwise indicated. 4
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 62 Flavors in SPME and Chiral Gas Chromatography Separations 100µm PDMS GC-FID apple essence, LC-GC 13 (9): 734-740 (1995) 30°C or 40°C seeds, candy Mani, V., Woolley, C. headspace 2544 Aroma compounds HS-SPME analysis of the volatile compounds from spices as a source 65µm PDMS/DVB GC-MS from spices of flavour in 'Campo Real' table olive preparations Flavour and Fragrance J. 22, #4, 265-273 (JUL-AUG 2007) Perez, R. A.; Navarro, T.; de Lorenzo, C. headspace 2578 Volatiles in Analysis of volatile components during potherb mustard (Brassica headspace GC-MS potherb mustard juncea, Coss.) pickle fermentation using SPME-GC-MS LWT - Food Science and Technology 40, #3, 439-447 (2007) Zhao, Dayun; Tang, Jian; Ding, Xiaolin 772 Volatiles in Analysis of volatile constituents of mustard paste by GC/MS 100µm PDMS GC-MS mustard paste w/SPME and simultaneous distillation and extraction Fenxi Huaxue (2000) 28(12) 1489-1492 30min @ 70°C Liu, B. in Chinese 2437 Volatiles in Comparison of headspace-SPME-GC-MS and LC-MS for the detection headspace GC-MS vanilla extracts and quantification of coumarin, vanillin, and ethyl vanillin in vanilla extract products Food Chem 107, #4, 1701-1709 (15 APR 2008) De, Jager L. S.; Perfetti, G. A.; Diachenko, G. W. 854 Volatiles in Analysis of the volatile components in vanilla extracts and 85µm polyacrylate GC-MS vanilla extracts flavourings by SPME and gas chromatography J Ag Food Chem (2000) 48(12), 5802-5807 Sostaric, T.; Boyce, M. C.; Spickett, E. E. 40min @ 20°C 829 Volatiles of Analysis of headspace compounds of distillers grains using 75µm Carboxen/PDMS GC-MS distillers grains SPME in conjunction with GC/MS and TGA. 60min J Cereal Sci. (2001) 33(2), 223-229 Staff, C., Biswas, S. headspace 2211 Essential oil of Comparison of essential oil of Xanthogalum purpurascens GC-MS Xanthogalum Lallem. Obtained via different isolation techniques purpurascens J. Essent. Oil Res. 18 #2, 181-184 (2006) Lallem Baser, K.H.C.; Duran, A.; Ozek, G.; Ozek, T.; Sagiroglu, M. 878 Essential oils in SPME of hop volatiles Potential use for determination and 100µm PDMS GC-MS hops verification of hop varieties 30min @ 70°C J. Chromatogr A 918 (2001) 159-167 Kovacevic, M., Kac, M. headspace 63 Essential oils in Determination of Essential Oils in Hops by Headspace SPME 100µm PDMS GC-FID hops J. Agric. Food. Chem, 44: 1768-1772 (1996) Field, J., Nickerson, G., James, D. Heider, C. 50°C, 4 hr 2860 Volatiles from Comparison of liquid-liquid extraction with headspace methods for the characterization of volatile fractions of commercial hydrolats from typically Mediterranean species GC-MS Essential oils J. Chromatogr A 1193, 1-2, 37-49 (Jun 6 2008) Barboni, T.; Costa, J.; Desjobert, J.; Leandri, C.; Paolini, J. 605 Essential oils Production of Yarrow (Achillea millefolium L.) in Norway: 100µm PDMS GC-MS in yarrow Essential Oil Content and Quality 40min @ 50°C J. Agric. Food Chem, (2000) 48 No,12, 6205-6209 Rohloff, J., Skagen, E., Steen, A., Iversen, T. headspace 2917 Volatiles from Inheritance of aroma compounds in a model population of Fragaria headspace GC-MS plants Plant Breeding 127, #1, 87-93 (FEB 2008) Olbricht, K.; Grafe, C.; Weiss, K.; Ulrich, D. Ambient temperature, unless otherwise indicated. 5
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