SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument State of the art in the determination of MTBE in natural waters & soils 2232 MTBE in water Crit. Rev. Anal. Chem.35 #4, 317-337 (2005) headspace FID and soil Aragon, P.; Atienza, J.; Herrero, M; M., Angel; Aragon, P.; Atienza, J.; Herrero, Ma. Asuncion; Maquieira, A.; Puchades, R. Sensitive method for determination of methyl tert-butyl ether (MTBE) in water by use of headspace-SPME/GC-MS. 1475 MTBE in water Fresenius' Journal of Analytical Chemistry (2001) 371(4), 519-525 Achten, Christine; Kolb, Axel; Puettmann, Wilhelm 75um Carboxen/PDMS, headspace Methyl tert-butyl ether (MTBE) in finished drinking water in Germany 2230 MTBE in Environ. Pollut 140 #2, 294-303 (2006) drinking water Kolb, Axel; Puttmann, Wilhelm GC-MS 1480 MIB in drinking water Correlation of musty odor and 2-MIB in two drinking water treatment plants in South Taiwan. Science of the Total Environment (2002) 289(1-3), 225-235 Lin, Tsair-Fuh; Kao, Hsiao-Pin; Wong, Jiun-Yue GC-MS 1484 1488 1493 Gas chromatographic determination of 2-hydroxy-4-methoxybenzophenone and octyldimethyl-p-aminobenzoic acid sunscreen agents in swimming pool and bathing waters by solid-phase microextraction 2-hydroxy-4methoxybenzophenone and octyldimethyl-p- Journal of Chromatography A (2002) 967(2), 243-253 aminobenzoic acid sunscreen agents in water Organochlorines in water Albanis, T. A.; Giokas, D. L.; Karayannis, M. I.; Lambropoulou, D. A.; Sakkas, V. A. Determination of organochlorides in water using solid-phase microextraction coupled to gas chromatography. 100µm PDMS, 85µm Polyacrylate American Laboratory (2002) 34(17), 12-14 GC Ou Qing-Yu; Liang Bing; Li Ju-bai; Huang Min-jia Method based on solid-phase microextraction-high-performance liquid chromatography with UV and electrochemical detection to determine estrogenic compounds in water samples. Estrogenic compounds Journal of Chromatography A (2002) 964(1-2), 153-160 in water Pocurull, E.; Borrull, F.; Marce, R. M.; Penalver, A. 85um Polyacrylate HPLC-UV, HPLC-ED Application of SPME for the quantitative determination of methylmercury in aqueous solutions. 1504 Mehylmercury in water Abstracts of Papers American Chemical Society (2002) 223(1-2) CHED 125 1536 1538 Phthalic acid esters in water Phenolic compounds in water Moore, J. Taylor; McDowell, Derek R.; Ambler, Rich B. Development of a solid-phase microextraction method for the determination of phthalic acid esters in water. Analytica Chimica Acta (2002) 457(2), 211-223 Various fibers compared GC-ECD Holadova, Katerina; Hajslova, Jana; Poustka, Jan; Prokupkova, Gabriela Solid-phase microextraction coupled to high-performance liquid chromatography to determine phenolic compounds in water samples. Journal of Chromatography A (2002) 953(1-2), 79-87 85um Polyacrylate HPLC-UV Marce, R. M.; Borrull, F.; Penalver, A.; Pocurull, E. Vial position in the determination of chlorophenols in water by SPME 2154 Chlorophenols J. Chromatogr. A, 1103, #1, 29-34 (2006) headspace GC-MS in water Portillo, A; Prohibas, N.; Salvado, V.; Simonet, B. M. Determination of chlorophenols by solid-phase microextraction and liquid chromatography with electrochemical detection. Ambient temperature, unless otherwise indicated. 170
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1552 Chlorophenols in water Journal of Chromatography A (2002) 947(2), 155-165 Various fibers compared HPLC-ELCD 1354 Aldehydes in drinking water Galceran, M. T.; Santos, F. J.; Sarrion, M. N. Determination of aldehydes in drinking water using pentafluorobenzylhydroxylamine derivatization and solid-phase microextraction Journal of Chromatography A (2002) 943(1), 1-13 Ventura, Francesc; Cancho, Beatriz; Galceran, Ma. Teresa 65um DVB PDMS, onfiber derivatization with PFBHA GC-ECD 1156 Chlorophenols Solid-phase microextraction liquid chromatography/tandem mass spectrometry for the analysis of chlorophenols in environmental samples. Rapid Communications in Mass Spectrometry (2002) 17 (1), 39-48. Sarrion, M. N.; Santos, F. J.; Moyano, E.; Galceran, M. T.* Carbowax/TPR LC-TMS 1166 Simultaneous mercury and tin speciation in environmental samples by GC- MIP/AES after preconcentration by solid phase microextraction Mercury and tin in environmental samples. Journal De Physique. IV : JP (2003) 107 (II), 1423. PDMS GC-MIP/AES Carrera, R.; De Diego, A.; Delgado, A.; Madariaga, J.; Sanz, J.; Zuloaga, O. 1074 Tributyltin Improvement of measurement precision of SPME-GC/MS determination of tributyltin using isotope dilution calibration. Analytical Chemistry (2002) 74 (21), 5606-5613. Bancon-Montigny, C.; Maxwell, P.; Yang, L.; Mester, Z.; Sturgeon, R. E. GC-MS Determination of methylphosphonic acid in water by SPME-GC 1952 Methyl Fenxi Ceshi Xuebao, 23, #1, 106-108 GC phosphoric Yuan, L.; Xu, D. N. acid in wate Electrochemically controlled (EC) SPME based 1953 Nickle-cadmium on over oxidized sulfonate polypyrrole sulfortated polypyrrole ETAAS from water Talanta, 67, #1,, 245-251 coated fiber Ertas, N; Pekmez, K; Sahin, Y; Tamer, U Udum, Y.; immersed Yildiz, A. Risk assessment of domestic and industrial effluents 1954 Industrial unloaded into a freshwater environment GC-MS effluent in Ecotoxicology & Environmental Safety, 61, #3, 380-391 freshwater Di Marzio, W.; Saenz, M.; Alberdi, J.; Tortorelli, M.; Silvana, G. Low part per trillion determination of reactive 1955 Alkanethiols alkanethiols in wastewater by in situ derivatization- N-ethylmaleimide GC-MS in wastewater SPME followed by GC/MS derivatives Anal. Chem., 77, #18, 6012-6018 immersion sampling Alzaga, R.; Bayona, J.M.; Garcia-Jares, C.; Llompart, M.; Salgado-Petinal, C. 2876 Alcohol Sediment toxicity of a rapidly biodegrading nonionic surfactant: Comparing the equilibrium partitioning approach with GC-MS ethoxylates in measurements in pore water marine sediment Env Sci & Tech. 42, #11, 4215-4221 (Jun 1 2008) Droge, Steven T. J.; Hermens, Joop L. M.; Postma, Jaap F. Analysis of freely dissolved alcohol ethoxylate homologues in various 2443 Ethoxylates seawater matrixes using solid-phase microextraction headspace GC in seawater Anal. Chem. 79, #7, 2885-2891 (2007-04-01) Droge, S. T.; Sinnige, T. L.; Hermens, J. L. M. Determination of total chromium in seawater by 1956 Chromium in isotope dilution sector field ICPMS using GC s PDMS fiber ICPMS seawater sample introduction TFA derivatives Anal. Chem., 76, #13, 3510-3516 headspace Abranko, L; Mester, ; Sturgeon, .; Yang, L Ambient temperature, unless otherwise indicated. 171
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