SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Characterization of three Agave species by GC 1571 Terpenes & and SPME-GC-MS headspace GC, GC-MS fatty acids in J Chromatogr A, 1027, #1-2, 131-136 steam distillation plants Pena-Alvarez, A.; Diaz, L.; Medina, A.; Labastida, C.; Capella, S.; Vera,L.. Analysis of volatile compounds of camu-camu (Myrciaria dubia (HBK) 2628 Volatiles in Mcvaugh) fruit isolated by different methods headspace GC-MS camu-camu fruit J. Essent. Oil Res. 19, #6, 527-533 (Nov/Dec 2007) Pino, Jorge A.; Quijano, Clara E. Analysis of volatile secondary metabolites 1572 Volatiles from Colombian Xylopia ronatica (Lamarck) by headspace GC-MS in fruit different extraction and headspace methods and GC J Chromatogr A, 1025, #1, 105-113 Stashenko, E.; Jaramillo, B.; Martinez, J Comparison of volatile compounds of corn oil and 1573 Volatiles modified corn oil by electronic nose and SPME-GC-MS headspace GC-MS in corn oil Agri Chem and Biotechnology, 47, #3, 153-156 Vu, Phuong-Lan; Shin, Jung-Ah; Lee, Ki-Teak Application of the SPME and in food analysis 1574 Review Polish J Food and Nutrition Sci, 13, #4, 355-361 100µm PDMS GC-MS Ligor, Magdalena; Wojcik, Jan; Buszewski, Boguslaw 85µm polyacrylate headspace Essential oil in fruits of Peucedanum alsaticum L. and Peucedanum 2812 Volatiles from cervaria (L.) Lap.Composition and antibacterial activity essential oils Planta Medica 73, #9, 883-884 (AUG 2007) Skalicka-Wozniak, K.; Los, R.; Glowniak, K.; Malm, A. Use of SPME in diffusive sampling of the atmosphere generated 2318 Volatiles from by different essential oils headspace GC/MS essential oils Anal. Chim. Acta 559 #2, 97-104 (2006) 30 min @ 20°C Batlle, R.; Huerga, M.A.; Lopez, P.; Nerin, C. High-throughput analysis of bergamot essential oil by fast SPME 2222 Volatiles in capillary GC-FID 30 and 7µm PDMS GC-FID essential oils J. Chromatogr. A, 1103, #1, 162-165 (2006) headspace Costa, R.; Dugo, G.; Dugo, P.; Mondello, L.; Presti, M.; Tranchida, P. Steam distillation-SPME for the detection of 1575 Volatiles from Ephedra sinica in herbal preparations headspace GC-MS essential oils J Chromatogr A, 1025, #1, 51-56 Tellez, M.; Khan, I.; Schaneberg, B.; Crockett, S.; Rimando, A.; Kobaisy,M Testing of microencapsulated flavours by electronic 1576 Volatiles from nose and SPME-GC headspace GC-MS essential oils Food Chem, 92, #1, 45-54 Baranauskiene, R; Venskutonis, P, Galdikas,A., Senuliene, Daiva; Setkus, Arunas SPME-GC-MS a fast and simple screening method 1577 Organo- for the assessment of organophosphorus headspace GC-MS phosphorus pesticides residues in wine and fruit juices. pesticides Food Chemistry, 86,#2, 269-274 in wine/juice Zamabonin, C; Quinto, M; deVietro, N; Palmisano, F Metabolites of lesser grain borer in grains. 1578 Volatiles J Agrl Food Chem, 52, #4, 898-908 headspace GC-MS from wheat Seitz, L. M.; Ram, M. S. 0-240min @ 20°-40°C Headspace SPME-GC-Mass spectrometric 1579 Volatiles of analysis of the essential oils of two traditional headspace GC-MS essential oils Chinese medicines, Angelica pubescens and Angelica sinensis. Chromatographia, 59, #5-6, 343-349 Song, G. X.; Deng, C. H.; Wu, D.; Hu, Y. M.* Comparative study on volatile components of Nardostachys Rhizome 2853 Volatiles from Journal of Natural Medicines 62, #1, 112-116 (JAN 2008) headspace GC-MS chinese grandiflora Tanaka, Ken; Komatsu, Katsuko Fast determination of curcumol, curdione and germacrone in three Ambient temperature, unless otherwise indicated. 48
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2704 Active ingredients species of Curcuma rhizomes by microwave-assisted extraction 100 µm PDMS GC-MS from chinese followed by headspace SPME-GC-MS 20min @ 80°. medicine J. Chromatogr., A 1117, #2, 115-120 (2006-06-09) headspace Deng, C. H.; Ji, J.; Li, N.; Yu, Y. J.; Duan, G. L.; Zhang, X. 30% NaCl Analysis of the volatile compounds in Ligusticum chuanxiong Hort. 2589 Volatiles from using HS-SPME-GC-MS 65µm PDMS-DVB GC-MS chinese medicines J. PHARM. BIOMED. ANAL. 44, #2, 464-470 (28 JUN 2007) headspace Zhang, C.; Qi, M.; Shao, Q.; Zhou, S.; Fu, R. GC-MS following microwave distillation and headspace SPME for fast 2570 Essential oils analysis of essential oil in dry traditional Chinese medicine headspace GC-MS in Chinese J. Chromatogr., A 1133, #1-2, 29-34 (2006-11-10) medicine Li, N.; Deng, C. H.; Li, Y.; Ye, H.; Zhang, X. M. Rapid determination of essential oil compounds in Artemisia 2166 Essential oils Selengensis Turcz by GC-MS with microwave distillation and headspace GC-MS in Chinese simultaneous SPME medicine Anal. Chim. Acta, 556, #2, 289-294 (2006) Deng, Chunhui; Xu, Xiuqin; Yao, Ning; Li, Ning; Zhang, Xiangmin Headspace SPME-GC-MS for analysis of volatile components 2553 Volatiles from from Atractylodes macrocephala Koidz 65µm PDMS-DVB GC-MS chinese medicines Sepu 25, #1, 43-47 (2007-01) 30 min @ 70°C Guo, F. Q.; Huang, L. F.; Zhou, S. Y. headspace Recent developments in sample preparation techniques for 2500 Review article chromatography analysis of traditional Chinese medicines. J Chromatogr A 1153, #1-2, 90-96 (2007 Jun 15) Deng, Chunhui; Liu, Ning; Gao, Mingxia; Zhang, Xiangmin SPME-multicapillary GC coupled to different 1580 Organo- detection systems and applied to volatile headspace ICP-MS, MIP-AES, selenium in organo-selenium speciation in yeast. AFS yeast J Analytical Atomic Spectrometry, 19, #2, 260-266 Dietz, C.; Sanz Landaluze, J.; Ximenez-Embun, P.; Madrid-Albarran, Y.; Camara, C. Volatile organoselenium monitoring in production and gastric 1581 Organo- digestion processes of selenized yeast by SPME-multicapillary headspace MIP-AES selenium in GC coupled microwave-induced plasma atomic yeast emission spectrometry Appl. Organomet. Chem., 18, #12, 606-613 Camara, C.; Dietz, C.; Madrid, Y.; Sanz Landaluze, J. Production of volatile organic sulfur compounds (VOSCs) 1582 Sulfur compd by basidiomycetous yeasts headspace GC-MS in yeast FEMS Yeast Research, 5, #4-5, 379-385 Buzzini, Pietro; Romano, Sergio; Turchetti, Benedetta; Vaughan, Ann; Pagnoni, Ugo Maria; Davoli, Paolo Direct coupling of SPME and quartz tube-atomic 1583 Methyl absortpion spectrometry for selective and sensitive 65µm PDMS-DVB GC-MS, AA mercury in determination of methylmercury in seafood: An bare silica fiber seafood assessment of chloride & hydride generation headspace J Analytical Atomic Spectrometry, 19, #2, 220-254 chloride derivative. Fragueiro, S; Lavilla, I; Bendicho, C. Volatile changes in cantaloupe during growth, maturation, and in 2258 Flavor volatiles stored fresh-cuts prepared from fruit harvested at various maturities headspace GC-MS in cantaloupe J Am Society for Horticultural Sci. 131, #1, 127-139 (2006) Beaulieu, John Volatile profile, sensory attributes, and quality of 1584 Flavor volatiles freshcut cantaloupe is maturity-at-cutting dependent headspace GC-MS in cantaloupe Hortscience, 38, #5, 833 Beaulieu, John C.; Bett, Karen L. Fatty acid composition of tomato affects fruit and 1585 Fatty acids leaf biosynthesis of C6 aldehydes and alcohols GC-MS in tomatos Hortscience, 38, #5, 833 Canoles, M; Li, C; Howe, Gg; Beaudry, R Rapid determination of C6-aldehydes in tomato plant emission 1586 C6 aldehydes by GC-MS and SPME with on-fiber derivatization 65µm PDMS-DVB GC-MS Ambient temperature, unless otherwise indicated. 49
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