SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument and juices Cardeal, Z.; Guimaraes, E.; Parreira, F. headspace Storage and ultraviolet-induced tissue stress 1753 Flavors from effects on fresh-cut pineapple. headspace GC pineapple J Sci Food and Agri, 84, #14, 1812-1816 Lamikanra, O.; Richard, O. A. SPME For the determination of benzoylureas in orange juice 2355 Benzoylureas in using LC combined with post-column photochemically 60µm DVB/PDMS HPLC orange juice induced fluorimetry derivatization and fluorescence detection immersion fluorescence J Sep Sci 31, #1, 56-63 (Jan -2008) fluorimetric Parrilla Voazquez, Piedad; Mughari, A; Martonez Galera, M. derivative High pressure processing of Australian navel orange 1754 Flavors from juices: Sensory analysis and volatile flavor profiling headspace GC-MS navel oranges Innovative Food Sci. Emerg. Tech., 6, #4, 372-387 4°C and 10°C Baxter, I.; Easton, K; Schneebeli, K; Whitfield, F Evaluation of the thermally dried immobilized cells of Lactobacillus 2850 Aroma compounds delbrueckii subsp bulgaricus on apple pieces as a potent starter culture headspace GC fermented whey J Agr Food Chem 55, #24, 9829-9836 (NOV 28 2007) Kopsahelis, N.; Panas, P.; Kourkoutas, Y.; Koutinas, A. A sensitive determination method for carbendazim and thiabendazole 2774 Thiabendazole in apples by SPME-LC with fluorescence detection 60µm DVB/PDMS HPLC carbendazim in Food Additives and Contaminants 25, #3, 314-319 (2008) 35min @ 20°C fluorescence apples Hu, Yanxue; Yang, X.; Wang, Chun; Zhao, Jin; Li, Weining; Wang, Zhi Determination of thiabendazole in orange juice and rind 1755 Thiabendazole by LC w/fluorescence detection and confirmation by headspace GC-MS-SIM in orange GC-MS after extraction by matrix solid-phase dispersion juice & rind J AOAC Int, 87, #3, 664-670 Albero, B; Sanchez-Brunete, C; Tadeo, Jose L. Determination of the principal volatile compounds of Turkish Raki 2842 Volatiles from Journal of the Institute of Brewing 113, #3, 302-309 (2007) headspace GC-MS aniseed-flavored Anli, R. Ertan; Vural, Nilufer; Gucer, Yalcin spirits Characterization of aniseed-flavoured spirit drinks by headspace 2402 Volatiles from SPME-GC-MS and chemometrics headspace GC-MS aniseed-flavored Talanta 72, #2, 506-511 (2007-04-30) spirits Jurado, J. ; Ballesteros, O.; Alcazar, A.; Pablos, F. ; Martin, M. ; Vilchez, J. L.; Navalon, A. Effects of carbohydrate and noncarbohydrate 1756 Sweetners sweeteners on the orange spirit volatile compounds headspace GC in orange Food Sci. Technol., 39, #2, 159-165 spirits Cordaro, F.; Da Porto, C.; Marcassa, N. Comparison of two headspace SPME fibres for the 1757 Volatiles detection of volatile chemical concentration changes 100µm PDMS GC in orange due to industrial processing of orange juice 85µm polyacrylate juice J Sci of Food & Agi, 85, #6, 1065-1071 headspace Jordan, M.; Goodner, K.; Castillo, M; Laencina, J. Studies on the aroma of cupuassu liquor by 1758 Volatiles in headspace SPME and gas chromatography. 75µm Carboxen GC-MS, GC-AED liquor J Chromatogr A, 1025, #1, 115-124 headspace de Oliveira, A; Pereira, N; Marsaioli, A; Augusto, F Seasonal, populational and ontogenic variation in the 1759 Volatils from volatile oil content and composition of individuals of headspace GC oregano plants Origanum vulgare subsp. Hirtum , assessed by GC headspace analysis and by SPME sampling of individual oil glands. Phytochemical Analysis, 15,#5, 286-292 Johnson, C; Kazantzis, A.; Skoula, M.; Mitteregger, U.; Novak, J. Polymers & Coatings Application of headspace SPME-GC-MS in characterisation of odorous 2620 Volatiles from volatile organic compounds emitted from magnetic tape coatings headspace GC polyester based on poly(urethane-ester) after natural and artificial ageing Ambient temperature, unless otherwise indicated. 68
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument magnetic tape Polym. Test. (UK) 26, #2, 243-56 (April 2007) Thiebaut, B.; Lattuati-Derieux, A.; Hocevar, M.; Vilmont, L.-B. Variations in amounts and potential sources of volatile organic 2643 Odor from chemicals in new cars headspace GC-MS new cars Sci. Total Environ. 382, #2-3, 228-239 (Sep 1 2007) Chien, Yeh-Chung 791 Organics in The simplest sample treatment techniques to assess the quality and safety of food packaging materials. Review article packaging materials Reviews in AnalChem (2000) 19(6), 435-465 Nerin, C.; Rubio, C.; Salafranca, J.; Batlle, R. SPME as an Effective Means to Isolate Degradation 254 Degradation products Products in Polymers in polymers J. Environ. Polym. Degrad. 5 (2): 67-73 (1997) Hakkarainen, M., Karlsson, S., Albetsson, A. 2662 Ink solvents on Ballpoint pen inks: the quantitative analysis of ink solvents on paper by solid-phase microextraction headspace ink solvents on paper J Forensic Sci 52, #1, 209-15 (2007 Jan) Brazeau, Luc; Gaudreau, Marc 2489 Volatile in water- Comprehensive VOC analysis method for architectural coatings JCT CoatingsTech 4, #1, 48-55 (Jan. 2007) headspace GC-MS based + solvent borne coatings Brickweg, Lukas; Guillermo, Audrey; Jones, Dane; Wills, Max Direct VOC Analysis of Water-Based Coating by GC and SPME GC-FID 361 Volatile solvents in J. Coating Technology, June 1997 65µm Carbowax/PDMS GC-FID water-based coatings Censullo, A., Jones, D., Wills, M. 5 min headspace salt added 626 Volatile solvents in Analysis of exempt paint solvents by GC using SPME J. Coat Technol. (2000), 72(900), 69-74 65µm Carbowax/PDMS GC-FID water-based coatings Bodrian, R., Censullo, A., Jones, D., Rashkin, M., Wills, M. 5 min headspace salt added 466 Volatiles from Analysis of volatile varnishes of coated wires by SPME Fresenius' J. Anal. Chem. 1999, 364(7), 641-642 GC-MS varnished wire Hinz, D., Kwarteng-Acheampong, W., Wenclawiak, B. headspace 426 Acetaldehyde in Determination of Residual Acetaldehyde in Polyethylene Terephthalate Bottles on SPME polyethylene bottles Czech J. Food Sci. (1998), 36(8), 401-405 Cizkova, H., Voldrich, M., Dobias, J. 761 Terephthalic acid, Determination of plastic monomers in water by SPME coupled with liquid chromatography 85µm polyacrylate LC-UV vinyl acetate in J.AOAC Intl. Vol 84, No. 2, 2001, 432-436 65µm DVB/PDMS water Batlle, R., Sanchez, C., Nerin, C. Vinyl chloride analysis with (SPME)-GC-MS 20min. Immersed 5% salt, pH 5.7 853 Vinyl chloride in applied to analysis in materials and aqueous samples. 75µm Carboxen/PDMS GC-MS plastic and water Analusis (2000) 28(10) 980-987 Charvet, R.; Cun, C.; Leroy, P headspace Abbreviated analysis of bisphenol A with SPME 467 Bisphenol A in tableware and food containers in plastic Shigen Kankyo Taisaku, 1999, 35(5), 447-451 Takao, Y., Arizono, K. Characterization by SPME-GC-MS of matrix changes of 876 Poly(L-lactide) poly(L-lactide) exposed to outdoorsoil environment GC-MS Ambient temperature, unless otherwise indicated. 69
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