SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in water Anal. Chem. 68: 130-133 (1996) min to 20 hr Dean, J., Tomlinson, W., Makovskaya, V., Cumming, R., Hetheridge, M., Comber, M. immersion, stirring 546 PAHs Solubility and partitioning studies with PAHs using an optimized SPME procedure 100µm SPME GC-MS in water and Fresenius' J. Anal. Chem. (1999), 363(4), 426-428 stirred octanol-water Paschke, A., Popp, P., Schueuermann, G. 728 PAHs Determination of PAHs in waste water by off-line coupling SPME with column liquid chromatography 100µm PDMS HPLC in waste water J. Chjromtogr. A, 897(2000) 153-159 Popp, P., Bauer, C., Moder, M., Paschke, A. 60 min fluorescence 547 Pesticides in Extracted amounts by SPME: a realistic approach to the partition coefficient K. water J. Chromtogr. Sci. 1999, 37(8), 277-282 Urruty, L., Montury, M 548 Volatiles Determination of Henry's law coefficient by combination of the equilibrium partitioning in closed systems and 100µm PDMS GC-FID in water SPME techniques J. Chromatogr, A., (1999), 830(2), 353-363 Dewulf, J., Van Langenhove, H., Everaert, P 30 min @ varied temp. 237 Organics in Partitioning of Organic Chemicals to Polyacrylate-Coated Solid-Phase Microextraction Fibers: Kinetic Behavior and 85µm polyacrylate GC-FID, -ECD water and air Quantitative Structure-Property Relationships immersion GC-MS Anal. Chem. 68: 4458-4462 (1996) Vaes, W., Hamwik, C., Ramos, E., Verhaar, H., Hermens, J. stirring Solid Phase Microextracting Using Fused-Silica Fibers Coated 84 with Graphitized Carbon Black Chromatographia 41: 678-684 (1995) Mangani, R., Cenciarini, R. 88 Overview New Direction in Sample Preparation for Analysis of Organic Compounds Trends Anal. Chem. 14 (3): 113-122 (1995) Pawliszyn, J. Multiple applications 121 Eugenol, Solid Phase Microextraction for Quantitative Analysis in Nonequilibrium Situations 85µm polyacrylate GC-MS 2,4-dimethylphenol, Anal. Chem. 69: 1230-1236 (1997) 1-160 min 2-phenylethanol Ali, J. immersion, stirring in water SPME in Headspace Analysis, Dynamics in Non-Steady State salt added 360 2-Octanol Mass Transfer 85µm polyacrylate, GC-MS in water Anal. Chem., 70: 4822-4826, (1998) 100µm PDMS Ali, J. headspace 2623 Volatiles from Analysis of volatile compounds from Malaysian durians (Durio zibethinus) using headspace SPME coupled to fast GC-MS headspace GC-MS Malaysian durians J. Food Compos. Anal. (UK) 20, #1, 31-44 (Feb. 2007) Nazimah, S.; Chin, S.; Quek, S.; Man, Y.; Rahman, R.; Hashim, D. M. 2637 Volatiles from Characterization of volatile compounds in selected citrus fruits from Asia. Part I: freshly-squeezed juice headspace GC-MS citrus fruit Flavour and Fragrance J. 22, #3, 228-232 (MAY-JUN 2007) Dharmawan, Jorry; Kasapis, Stefan; Curran, Philip; Johnson, Jeffrey R. 2725 Volatiles from Postharvest survey of volatile compounds in five tropical fruits using headspace-solid phase microextraction (HS-SPME). headspace GC-MS tropical fruit HortScience 42, #2, 309-314 (2007) Natta Laohakunjit; Orapin Kerdchoechuen; Matta, F.; Silva, J.; Holmes, W. sat. salt Ambient temperature, unless otherwise indicated. 214
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2556 Volatiles from Screening of Tropical Fruit Volatile Compounds Using SPME Fibers and Internally Cooled SPME Fiber PDMS coating GC-MS tropical fruit J. Agric. Food Chem. 54, #23, 8688-8696 (2006-11-15) Carasek, E.; Pawliszyn, J. 214 Strawberries Solid-Phase Microextraction: Artifact Formation and Its Avoidance 85µm polyacrylate GC-MS and apples Chromatographia 46: 63-66 (1997) 30 sec in fruit homogenate Verhoeven, H., Beuerle, T., Schwab, W. immersion 2518 Isophorone Determination of isophorone in food samples by SPME-GC-MS J Chromatography A 1155, #1, 100-104 (2007) 65µm PDMS/DVB GC/MS in food samples Kataoka, H.; Terada, Y.; Inoue, R.; Mitani, K. 60°C, 45 min headspace Study of barrier properties and chemical resistance of recycled PET 2327 Organics from coated with amorphous carbon through a plasma enhanced headspace GC/MS PET coating chemical vapour deposition (PECVD) process Food Additives and Contaminants 23 #1, 100-106 (2006) Cruz, S. A.; Zanin, M.; Nerin, C.; De Moraes, M. A. B. 139 McReynolds probes Studying Activity Coefficients of Probe Solutes in Selected Liquid Polymer Coatings Using SPME 7µm PDMS GC-FID in methanol J. Phys. Chem. 100: 17648 (1996) 25-100°C, 15 min Zhang, Z., Pawliszyn, J. headspace 729 Lidocane Multiple solid phase microextraction J. Chromatogr. A. (2000) 878, 27-33 100µm PDMS HPLC from water Koster, E., de Jong, G. 45min Fibers coated with molecularly imprinted polymers for SPME 939 Anal. Chem (2001) 73(13) 3140-3145 Koster, E; Crescenzi, C; den Hoedt, W; Ensing, K; de Jong, G 579 BTEX and solvents Study of polymer coatings for solid-phase microextraction Sepu. Jan 1999; 17(1): 10-13 88µm PDMS in water Zhang,-DN; Wu,-CY; Ai,-F 148 Maillard reaction A Study of the Behavior of Maillard Reaction Products Analyzed by SPME-GC-Mass Selective Detection 100µm PDMS GC-MS products J. Chromatogr. Sci. 34: 213 (1996) 5 min in water Coleman III, W. A Study of the Behavior of Polar and Nonpolar SPME Fibers immersion stirring 207 Alkyl & alkoxy aroma & J. Chromatogr. Sci. 35 (6): 245-258 (1997) 100µm PDMS GC-MSD flavor compounds Coleman, W. 5 min in water immersion & headspace stirring, salt added 730 Inorganic anions SPME of inorganic anions based on polypyrrole film Analyst (Cambridge, UK), 2000, 125(3), 391-394 Polypyrrole film Ion Chrom. in water Wu, J., Yu, Z, Lord, H., Pawliszyn, J. 764 Volatile organics Preparation and appplication of polypyrrole films in SPME J. Chromatogr. A (2001) 909(1) 37-52 Polypyrrole film In-tube GC-FID PAHs, amines Wu, J., Pawliszyn, J. 20min. LC-UV in water/air mixture headspave 163 Mercury, SPME Combined with Electrochemistry Anal. Commun. 33(10): 361-364 (1996) 10µm gold on GC-MS mercury compounds Guo, F., Gorecki, T., Irish, D., Pawliszyn, J. carbon steel electrode in water 5 min gas phase sampling Ambient temperature, unless otherwise indicated. 215
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