SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />
Analyte / Extraction<br />
Matrix Literature Reference Conditions Instrument<br />
Namera, A., Yashiki, M., Kojima, T., Fukunaga, N. and conditions<br />
337 Acylcarnitines<br />
Determination of Urinary Acylcarnitines by ESI-MS Coupled<br />
with <strong>SPME</strong> ESI-MS<br />
in urine J. Mass Spectrom. 32 (11): 1195-1204 (1997)<br />
Mioder, M., Loster, H., Hraschuh, R., Popp, R.<br />
499 Methylxanthines<br />
Extraction of methylxanthines from human body fluids<br />
by <strong>SPME</strong> 65µm Carbowax/DVB GC-NPD<br />
in blood/urine Anal. Chim. Acta., 1999, 387(1), 53-60 1 hr @ 40°C<br />
Kumazawa, T., Seno, H., Lee, X., Ishii, A. 1ml of 1M HCl04<br />
414 Organic acid esters<br />
Urinary Organic Acid Screening by <strong>SPME</strong> of the Methyl Esters<br />
J. Chromatogr. B: Biomed Sci. Appl. (1998), 713(2), 427-432 85µm polyacrylate GC-FID, -MS<br />
in urine Liebich, H., Gesele, E., Woll, J.<br />
Validation of negligible depletion <strong>SPME</strong> as a tool to<br />
20 min<br />
immersion w/stirring<br />
trimethyloxonium<br />
tetrafluoroborate<br />
667 Semivolatile determine tissue/blood partition coefficient for semivolatiles<br />
in tissue/blood and nonvolatile organic chemicals<br />
Toxicol. Appl. Pharmacol. (2000), 166(2), 138-144<br />
Garicano, E., Vaes, W., Hermens, J.<br />
415<br />
New Mass Spectrometric Methods for the Fast Analysis<br />
of Biomedical-Relevant Substances<br />
CLB Chem. Labor Biotech. (1998), 49(11), 414-420<br />
Volmer, D.<br />
GC-MS<br />
417 Verpamil &<br />
<strong>SPME</strong>-HPLC Determination of Verpamil and Norverpamil<br />
Enantiomers in Urine HPLC<br />
norverapamil J. Mass Spectrom. (1997), 32(11), 1195-1204<br />
in urine Asafu-Adjaye, E., Shiu, G.<br />
971 Pesticides in water<br />
Pesticide toxicity assessment using an electrochemical biosensor.<br />
Analytical and Bioananalytical Chemistry (2002) 373(8), 696-703<br />
Farre, M.; Goncalves, C.; Lacorte, S.; Barcelo, D.; Alpendurada, M.F.<br />
GC-MS<br />
Absorption through porcine skin exposed to various doses of jet fuel marker<br />
components determined with GC-FID using head space <strong>SPME</strong> fiber.<br />
1034 Jet fuel in porcine skin. Toxicological Sciences (2003) 72 (S-1), 383.<br />
1050 PAH<br />
Xia, X. R.; Riviere, J. E.; Muhammad, F.; Monteiro-Riviere, N. A.; Baynes, R. E.<br />
Determination of selected monohydroxy metabolites of 2-, 3- and 4-ring<br />
polycyclic aromatic hydrocarbons in urine by solid-phase microextraction and<br />
isotope dilution gas chromatography-mass spectrometry.<br />
Journal of Chromatography, B: Analytical Technologies in the Biomedical and<br />
Life Sciences (2002) 778 (1-2), 157-164. GC-MS<br />
Smith, C. J.; Walcott, C. J.; Huang, W. L.; Maggio, V.; Grainger, J.; Patterson,<br />
D. G., Jr.<br />
1294<br />
Biomimetic solid-phase microextraction to predict body residues and toxicity of<br />
chemicals that act by narcosis.<br />
Environmental Toxicology and Chemistry (2002) 21(2), 229-234<br />
Leslie, Heather A.; Busser, Frans J. M.; Hermens, Joop L. M.; Kraak, Michiel H.<br />
S.; Oosthoek, Annelies J. P.<br />
GC-MS<br />
1349<br />
Fatty acid ethyl esters in hair as markers of alcohol consumption. Segmental<br />
hair analysis of alcoholics, social drinkers, and teetotalers.<br />
Fatty acid ethyl esters<br />
in hair Clinical Chemistry (2001) 47(12), 2114-2123.<br />
Auwaerter, V.; Sporkert, F.; Hartwig, S.; Pragst, F. *; Vater, H.; Diefenbacher,<br />
A.<br />
GC-MS<br />
Ambient temperature, unless otherwise indicated. 126