SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Sediment dilution method to determine sorption 2109 Organic coefficients of hydrophobic organic chemicals Immersed extract from GC chemicals in Environ. Sci. Technol., 39. #11, 4220-4225 sediment in water sediment Busser, F; Hermens, J.; Klamer, H.; Mayer, P; Ter Laak, T 2698 Dioxin congeners Microbial dehalogenation of trichlorinated dibenzo-p-dioxins by a Dehalococcoides-containing mixed culture is coupled to headspace GC-MS from cultures carbon isotope fractionation Environ. Sci. Technol.41, #22, 7744-7751 (15 NOV 2007) Ewald, E. -M.; Wagner, A.; Nijenhuis, I.; Richnow, H. -H.; Lechner, U. Simple device for the SPME screening of 2110 PCDDs/PCDF polychlorodibenzo-p-dioxins and polychlorodibenzo- 100µm PDMS GC-MS in soil furans in heavily contaminated soil samples. headspace Analytica Chimica Acta, 527, #2, 157-162 sonicated Chia, K. J.; Lee, T. Y.; Huang, S. D.* Air 725 Organic vapors Application of SPME for determination of organic vapors in gaseous matrices review article in gaseous matrices J. Chromatogr. A, 885(2000) 405-418 Namiesnik, J., Zygmunt, B., Jastrzebska, A. 846 Solvent vapors Solvent vapour monitoring in work space by SPME J Hazardous Materials (2001) 83(1-2), 83-91 100µm PDMS in air Li, K.; Fingas, M.; Goldthorp, M.; Lambert, P.; Santilli, A.; Whiticar, S. 75µm Carboxen/PDMS Diffusive sampling of methylene chloride with SPME 2563 Methylene chloride J. Chromatogr., A 1137, #2, 138-144 (2006-12-29) 85µm Carboxen/PDMS GC-ECD in air Chen, C. Y.; Hsiech, C. M.; Lin, J. M. diffuse sampling 2460 Volatiles Characterization of sorption mechanisms of SPME with volatile organic compounds in air samples using a linear solvation energy relationship approach 100µm PDMS GC in air J. Chromatogr. A 1179, #1, 24-32 (25 JAN 2008) Prikryl, P.; Sevcik, J. 85µm polyacrylate 726 Volatiles Airflow Rate in the Quantitation of Volatiles in Air Streams by Solid Phase Microextraction 100µm PDMS GC-FID in air Anal. Chem 2000, 72, 3949-3955 Bartelt, R., Zilkowski, B. 30 min 727 Volatile organic Sorbent trapping of volatile organic compounds from air J. Chromatogr. A, 885 (2000) 120-151 75µm Carboxen/PDMS GC-FID in air Harper, M. review article 758 Volatile organic Air sampling with porous SPME fibers compounds Anal. Chem. 2000, 72, 5178-5186 75µm Carboxen/PDMS GC-FID in air Koziel, J., Jia, M., Pawliszyn, J. Air sampling and Analysis of Volatile Organic compounds 65µm DVB/PDMS 5-10 sec air sampling 754 Volatile organic with Solid Phase Microextraction 100um PDMS GC-FID in air J. Air & wasteManage. Assoc 51: 173-184 Koziel, J., Pawliszyn, J. 55 BTEX Analysis of Environmental Air Samples by Solid Phase microextraction and GC/Ion Trap Mass Spectrometry 100µm PDMS GC-MS in air Environ. Sci. Technol. 29: 693-701 (1995) 3 min Chai, M., Pawliszyn, J. gas sampling 226 Petroleum Estimation of Air-Coating Distribution Coefficients for SPME Using Retention Indexes from Linear Temperature-Programmed 100µm PDMS, GC-FID hydrocarbons Capillary Gas Chromatography. Application to the Sampling 30µm PDMS in air and Analysis of Total Petroleum Hydrocarbons in Air Anal. Chem. 69: 402-408 (1997) 30-480 min Ambient temperature, unless otherwise indicated. 204
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Martos, P., Saraullo, A., Pawliszyn, J. Conditions Instrument 375 Formaldehyde Sampling and Determination of Formaldehyde Using SPME with On-Fiber Derivatization 65µm PDMS/DVB GC-MS derivatives Anal. Chem. 198, 70, 2311-2320 10-150 sec in air Martos, P., Pawliszyn, J. Determination of Amines in Air and Water Using Derivatization gas sampling PFBHA derivatives 110 Amines Combined with SPME 65µm Carbowax/DVB GC-FID in air J. Chromatogr. A 773: 249-260 (1997) 30 min Pan, L., Chong, M., Pawliszyn, J. Evaluation of SPME for sampling of volatile organic sulfur gas sampling DPTFA derivatives 539 Thiol and sulfides compounds in air for subsequent GC analysis with 75µm Carboxen/PDMS GC-AED in air samples atomic emission detection J. Chromatogr., A 1999, 848(1+2), 305-315 Haberhauer-Troyer, C., Rosenberg, E., Grasserbauer, M 540 Sulfur compounds Studies on the application of SPME for analysis of volatile organic sulfur compounds in gaseous and liquid samples 100µm PDMS FPD-GC in water/ N2 & Chem. Anal. (Warsaw), 1999, 44(3A), 485-493 10 min propane Wardencki, W., Namiesnik, J. Calibration of Solid-Phase Microextraction for Air Analyses 233 C5-C11 hydrocarbons, Based on Physical Chemical Properties of the Coating 30µm & 100µm PDMS GC-FID BTEX Anal. Chem. 69: 206-215 (1997) 15-450 sec in air Martos, P., Pawliszyn, J. gas sampling On Calibration of SPME-GC-MS system for analysis of 541 Chlorobenzen and organic air contaminants using gaseous standard mixtures Optimization of sampling GC-MS p-xylene Chem. Anal. (Warsaw) (1999), 44(2), 201-213 in air Namiesnik, J., Gorlo, D, Wolska, L, Zygmunt, B. SPME in environmental analysis 2851 Review article Anal. Bioanal. Chem. 386, #4, 1059-1073 (Oct 2006) Ouyang, Gangfeng; Pawliszyn, Janusz Standard-free kinetic calibration for rapid on-site analysis by SPME 2903 PAHs J. Sep. Sci.31, #6-7, 1167-1172 (April 2008) GC-MS Cai, Jibao; Li, Hui; Ouyang, Gangfeng; Pawliszyn, Janusz; Zhang, Xu 2297 PAHs Calibration of SPME for quantitative analysis by gas chromatography J. Chromatogr. A, 1097, #1-2, 9-16 (2006) Chen, Yong; Ouyang, Gangfeng; Pawliszyn, Janusz; Setkova, Lucie GC 308 Organic vapors Calibration Procedure for SPME-GC Analysis of Organic Vapors in Air in air Talanta 44 (9): 1543-1550 (1997) Gorlo, D., Wolska, L., Zygmunt, B., Namiesnik, J. 756 Organic vapors Diffusion-Based Calibration for SPME Analysis of Aqueous samples Carboxen/PDMS in air Anal. Chem. 2001, 73 (1), 13-18 DVB/PDMS Sukola, K., Koziel, J., Augusto, F., Pawliszyn, J. 10sec. Passive sampling Determination of absolute amount extracted by SPME 828 different approaches under examination J.Microcolumn Separations (2000) 12(10), 550-557 Tuduri, L.; Desauziers, V.; Fanlo, J. L 757 Aerosols, particulate Sampling and Analysis of Airbourne Particulate matter and aerosols using In-Needle Trap and SPME fiber devices 7um PDMS GC-MS Ambient temperature, unless otherwise indicated. 205
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