SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Oxidatively derived volatile compounds in microencapsulated fish oil 2278 Volatiles in monitored by SPME PDMS/DVB GC-FID fish oil J Food Science 70 #7, C433-C440 (2005) headspace Jonsdottir, Rosa; Bragadottir, Margaret; Arnarson, Gudmundur Orn Determination of mono- to octachlorobiphenyls in 1934 Biphenyls fish oil using Florisil adsorption followed by 65µm PDMS-DVB GC-TOF-MS in fish oil headspace SPME-GC with TOF-MS headspace J. Chromatogr. Am 1085, #2, 278-284 Agustin, M.; Hong, S; Lee, K.; Park, H.; Ryu, Jae-Ch The comparison of SPME-GC and static headspace-GC 2805 Solvent residue in for determination of solvent residues in vegetable oils 85µm CAR/PDMS GC-FID vegetable oil Journal of Separation Science 31,#2, 364-371 (Feb 2008) headspace Ligor, Magdalena; Buszewski, Boguslaw Rapid validated method for the analysis of benzo a pyrene in vegetable 2700 Benzo-a-pyrene in oils by using SPME-gas chromatography-mass spectrometry. headspace GC-MS vegetable oil J. Chromatogr., A 1176, #1-2, 231-235 (2007) Purcaro, G.; Moret, S.; Conte, L. S. Determination of PAHs in vegetable oils using SPME-comprehensive 2453 PAHs in two-dimensional GC coupled with time-of-flight MS immersed GC-TOF-MS vegetable oil J. Chromatogr., A 1150, #1-2, 173-177 (2007-05-25) Wejnerowska, G.; Karczmarek, A.; Gaca, J Evaluation of spme conditions for the determination of PAHs 2868 PAHs in in aquatic species using gas chromatography 65µm PDMS-DVB GC-MS aquatic species Anal. Bioanal. Chem. 391, #4, 1419-1424 (June 2008) 75°C for 60 min Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; Vinas, P. headspace A headspace SPME procedure coupled with for the analysis of 2866 PAHs in volatile polycyclic aromatic hydrocarbons in milk samples 65µm PDMS-DVB GC-MS milk Anal. Bioanal. Chem. 391, #3, 753-758 (June 2008) 75°C for 60 min Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; Vinas, P. headspace Determination of 16 polycyclic aromatic hydrocarbons in milk and 2448 PAHs in related products using SPME-GC-MS 65µm PDMS-DVB GC-MS milk Anal. Chim. Acta 596, #2, 285-290 (2007-07-23) immersed Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M. ; Vinas, P. 60 min at 55°C Analysis of polycyclic aromatic hydrocarbons in solid matrixes by 2423 PAHs in solid-phase microextraction coupled to a direct extraction device 100µm PDMS GC-MS smoked meat Talanta 71, #2, 751-757 (2007-02-15) 65µm PDMS-DVB Martin, D.; Ruiz, J. 25°C for 60 min headspace Behaviour of polycyclic aromatic hydrocarbons in dissolved, 2720 PAHs in colloidal, and particulate phases in sedimentary cores GC-MS sediment Intl J Env Analyt Chem 87, #3, 211-225 (2007) King, A. J.; Readman, J. W.; Zhou, J. L. Electronic nose and SPME techniques to monitor phenanthrene 2782 Phenanthrene in biodegradation in soil headspace soil Sens Actuators, B Chem 131, #1, 63-70 (Apr 14 2008) De Cesare, F.; Macagnano, A.; Pantalei, S.; Zampetti, E. Comparison of techniques for estimating PAH bioavailability: uptake 2650 PAHs in in Eisenia fetida, passive samplers and leaching using various s GC soil olvents and additives. Environ Pollut 145, #1, 154-60 (2007 Jan) Bergknut, M.; Sehlin, E.; Lundstedt, S.; Andersson, P.; Haglund, P.; Tysklind, M. SPME and GC-MS for the determination of PAHs in 1935 PAHs in environmental solid matrices. 100µm PDMS GC-MS soil/seaweed Jl of Chromatographic Sci, 42, #6, 329-335 immersed liquid carrier Cam, D.; Gagni, S.; Lombardi, N.; Punin, M. SPME coupled with HPLC using on-line diode-array and 2266 Fenitrothion electrochemical detection for the determination of fenitrothion and HPLC in water its main metabolites in environmental water samples J. Chromatogr. A, 1094 #1-2, 70-76 (2005) Barrio,R.; Goicolea, M.; Sampedro, M.; Sanchez-Ortega, A.; Unceta,N. Ambient temperature, unless otherwise indicated. 138
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Sensitive method for the determination of roxarsone using Conditions Instrument 1936 Roxarsone w/ SPME multi-detector gas chromatography 65µm PDMS-DVB GC-MS in water J Chromatogr A, 1057, #1-2, 177-183 15min @ 70°C GC-PFPD Aldstadt III, Joseph H.; Roerdink, Aaron R. Speciation of volatile selenium species in plants using 1,3-propanedithiol derivatives 1937 Selenium GC-ICP-MS headspace GC-ICP-MS from plants Sepu, 22, #1, 16-19 Meija, J.; Montes-Bayon, M.; Caruso, J.; Leduc, D.; Terry, N. Analysis of sulfur & nitrogen odorants using SPME and GC-MS 1938 Sulfur & N2 Water Sci. Technol., 50, #4, 115-120 headspace GC-MS odorants in Chiu, P.C.; Dentel, S.K.; Hepner, S.; Turkmen, M. biomass Identification of metallic-smelling 1-octen-3-one and 1-nonen-3-one 2303 Odorants from from solutions of ferrous sulfate headspace GC FeSO4 solutions. J Ag Food Chem, 53, #21, 8325-8327 (2005) (1, 5, and 16 h) Lubran, Meryl B.; Lawless, Harry T.; Lavin, Edward; Acree, Terry E. 22° and 37°C Characterization of odors from limed biosolids treated 1939 Odors from with nitrate and anthraquinone headspace GC-MS biosolids J. Environ. Sci. Health, 40, #1, 139-149 Abu-Orf, M; Choi, H.; Kim, H.; McConnell, L.; Peot, C.; Ramirez, M. Contamination of toxic volatile and semi-volatile compounds 2214 Organics from from automobile materials automobile Bul Envn Contamination and Toxicology 76, #2, 301-305 (2006) materials Zhou, S.; Huang, J. X.; Kinkel, J.; Stark, W. Sampling and analysis of volatile organic pollutants emitted 1940 Organics by an industrial stack 85µm polyacrylate GC-MS in stack Anal. Chim. Acta, 524, #1-2, 51-62 headspace emmisions Campo, L.; Domeno, C.; Martinez-Garcia, Fca.; Nerin, C. Quantitative determination of volatile organic compounds in 1941 Volatile indoor dust using gas chromatography-UV spectrometry headspace GC-UV organics in Environ. Int., 31, #8, 1141-1148 dust Bornehag, C; Lagesson, V; Nilsson, A; Sundell, J; Tagesson, C Analysis of volatile components in concrete by 1942 Volatiles SPME-GC-Mass Spetrometry 50/30µm DVB/CAR GC-MS in concrete Zhipu Xuebao, 25, #4, 225-228 65°C, headspace Liao, K. Identification of volatile components in yunyan and yanmo 1943 Volatiles concrete by SPME -GC-MS headspace GC-MS in concrete Zhipu Xuebao, 25, #1, 32-37 Zhu, S. M.; Li, J.; Lin, P. Chlorophenols in leachates originating from different landfills 1944 Chlorophenols and aerobic composting plants headspace GC-FID from landfills J. Hazard. Mater., 124. #1-3, 107-112 Ozkaya, Bestamin GC analysis of organic marker compounds in fine particulate 2694 Organics matter using solid-phase microextraction 75µm Carboxen GC-MS from J Air Waste Manag Assoc. 57, #1, 53-58 (2007 Jan,) 30min headspace particulate Lin, Lin; Lee, Milton L; Eatough, Delbert J Qualitative analysis of organics in atmospheric 1945 Organics particulates by headspace SPME-GC/MS 100µm PDMS GC-MS from Atmos. Environ., 38, #40, 6917-6925 10min headspace particulate Khanal, O.; Shooter, D. Current trends in SPME techniques for the determination of 2653 Pesticides pesticides in food and environment Review from soil J Biochem Biophysical Methods 70, #2, 117-131 (MAR 10 2007) Pico, Yolanda; Fernandez, Monica; Ruiz, Maria Jose; Font, Guillermina Determination of pesticides and their degradation products 1946 Pesticides IN soil: Critical review and comparison of methods Review GC-MS from soil TrAC Trends Anal. Chem., 23, #10-11, 772-789 headspace SPME LC-MS Andreu, Vicente; Pico, Yolanda Coupled in-tube and on-fibre SPME for cleanup and preconcentration of Ambient temperature, unless otherwise indicated. 139
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