SPME Applications Guide - Overbrook Scientific

Recommendations

Info

(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2707 Selegiline human body fluids by headspace SPME-GC-MS headspace GC/MS in human blood J. Chromatogr., B: 844, #2, 283-291 (2006-12-05) Kuriki, A.; Kumazawa, T. ; Lee, X. P,; Hasegawa, C.; Kawamura, M.; Suzuki, O.; Sato, K. 2456 Paeonol in plasma Fast determination of paeonol in plasma by headspace SPME followed by gas chromatography-mass spectrometrY Anal. Chim. Acta 585, #1, 76-80 (2007-02-28) Dong, L.; Deng, C. H.; Wang, J. Y.; Shen, X. Z. headspace GC/MS 2425 Fluoxetine and SPME-LC determination of fluoxetine and norfluoxetine in plasma using a heated liquid flow through interface 65µm PDMS/DVB LC-MS norfluoxetine in J. Chromatogr., B: 847, #2, 217-223 (2007-03-01) plasma Fernandes, C.; dos Santos Neto, A.; Rodrigues, J.; Alves, C.; Lancas, F. 1392 Drugs in plasma Application of solid-phase micro-extraction technology to drug screening and identification. Annals of Clinical Biochemistry (2001) 38(5), 541-547. Mosaddegh, M. H.; Richardson, T.; Stoddart, R. W.; McClure, J. Polyacrylate, carbowax/D GC-MS 1470 Amphetamine-like drugs 1497 Residual solvents in pharmaceuticals Simultaneous detection of amphetamine-like drugs with headspace solid-phase microextraction and gas chromatography-mass spectrometry. Journal of Chromatography B (2002) 780(1), 183-192 GC-MS Macchia, Teodora; Chiarotti, Marcello; Gentili, Stefano; Marsili, Remo; Torresi, Alessio High-speed gas chromatographic analysis of solvents in pharmaceuticals using solid phase microextraction Journal of Pharmaceutical and Biomedical Analysis (2002) 29(3), 507-518 Raghani, A. R. 50/30um DVB/Carboxen PDMS, 65um PDMS DVB 2769 citalopram, Simultaneous determination of citalopram, fluoxetine and their main metabolites in human urine samples by SPME-LC HPLC-UV fluoxetine in J Pharma and Biomedical Analysis 46(4), 763-770 (MAR 13 2008) human urine Unceta, Nora; Gomez-Caballero, Alberto; Sanchez, Alicia; Millan, S.; Carmen Sampedro, M.; Aranzazu Goicolea, M.; Salles, J.; Barrio, R. Determination of delorazepam in urine by solid-phase microextraction coupled to high performance liquid chromatography. 1514 Delorazepam in urine Journal of Pharmaceutical and Biomedical Analysis (2002) 28(5), 965-972 Zambonin, Carlo Giorgio; Aresta, Antonella; Monaci, Linda 50um Carbowax TPR, 60um PDMS DVB HPLC-UV Rapid screening of 2-"fluorine-18"-fluoro-2-deoxy-D-glucose infusions for volatile organic compound contaminants by solid phase microextraction with gas chromatography-selective ion monitoring mass spectrometry (SPME-GC- SIMMS). 1201 Applied Radiation and Isotopes (2003) 58 (2), 193-200. Kanu, A. B.; Dixon, M.; Zu, Y. Y.; Bailey, J.; Gillies, J. M.; Zweit, J.; Thomas, C. L. P.* 1280 Determination of trace retinoic acid by capillary electrophoresis-solid-phase microextraction with direct UV detection. Journal of Chromatographic Science (2003), 41 (6), 301-304). Fang, M.; Xu, G. W. CE Study of multiple SPME combined off-line w/HPLC 1827 Pharmaceuticals Application in analysis of pharmaceuticals in urine 100µm PDMS & HPLC in urine Anal. Chim. Acta, 516, #1-2, 197-204 85µm polyacrylate Aikaterini Lontou, M.; Gondova, T.; Michopoulos, F.; immersed Sucha, M.; Theodoridis, G. salt added Biological 2205 Phosphoric acid Determination of phosphoric acid triesters in human plasma using SPME and GC coupled to inductively coupled plasma MS 65µm DVB/PDMS GC-MS triesters in J. Chromatogr. A, 1103, #2, 329-336 (2006) immersion human plasma Shah, Monika; Meija, Juris; Cabovska, Baiba; Caruso, Joseph A. 30min @40°C Ambient temperature, unless otherwise indicated. 94 GC
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument deproteinization 2204 Proteomics Sample preparation techniques for mass spectrometry in proteomics using recently developed highly selective materials Current Proteomics 2 #4, 269-285 (2005) Huck, Christian W.; Bakry, Rania; Bonn, Guenther K. MS Evaluation of SPME for the study of protein binding in human 638 Anesthetics plasma samples 60µm Carbowax/DVB NPD in plasma J. Chromatogr. Sci. (2000), 38(10), 458-464 32°to 40°C Abdel-Rehim, M., Calsson, G., Bielenstein, M., Arvidsson, T., pH 6.4-9.4 Blomberg, L. Influence of albumin on sorption kinetics in SPME: Consequences 2613 Pyrene diffusion for chemical analyses and uptake processes serum albumin Anal. Chem. 79,#18, 6941-6948 (Sep 15 2007) Hermens, Joop L. M.; Kramer, Nynke I.; Van Eijkeren, Jan C. H. Application of SPME in the investigation of protein binding of 2227 Drugs in pharmaceuticals HPLC serum albumin J. Chromatogr. B 830 #2, 238-244 (2006) Theodoridis, Georgios Measurement of the Free Concentration Using SPME: 99 Aniline, nitrobenzene, Binding to Protein 85µm polyacrylate GC-MS 4-n-pentylphenol, J. Anal. Chem. 68: 4463-4467 (1996) 24°C, 9-14 min 4-chloro-3methylphenol Vaes, W., Ramos, E., Verhaar, H., Seinen, W., Hermens, J. stirring in bovine serum albumin K2PO4 buffered Modeling bovine serum albumin binding of flavor compounds (alcohols, 2843 Flavor compounds aldehydes, esters, and ketones) as a function of molecular properties headspace GC bovine serum Journal of Food Science 73, #1, S56-S63 (JAN-FEB 2008) Tan, Y.; Siebert, K. J. Quantification of solute-solute interactions using negligible-depletion 2888 Estradiol in SPME: Measuring the affinity of estradiol to bulk organic matter organic matter Environ. Sci. Technol. 42, #8, 2886-2892 (Apr 15 2008) Escher, Beate I.; Neale, Peta A.; Schafer, Andrea I. The binding constant of estradiol to bovine serum albumin. An 2320 Estradiol from upper-level experiment utilizing tritium-labeled estradiol and headspace GC bovine serum liquid scintillation counting albumin J Chem Educ 83 #2, 294-295 (2006) Adhyaru, Bhavin; Liang, Peihong; Pearson, Wright L.; Williams, K. Solid Phase Microextraction of Biopolymers, Exemplified 140 Protein in with Adsorption of Basic Proteins onto a Fiber Coated 85µm polyacrylate HPLC-UV bovine serum albumin with Polyacrylic Acid 5-240 sec J. Microcolumn Sep. 8: 1 (1996) Liao, J., Zeng, C., Hjerten, S., Pawliszyn, J. immersion Sorbent preconcentration procedures coupled to capillary 2899 Review article electrophoresis for environmental and biological applications Anal. Chim. Acta 616, #1, 1-18 (May 26 2008) Aguilar, Carme; Borrull, Francesc; Calull, Marta; Puig, Patricia 411 Proteins Optimization of SPME-Capillary Zone Electrophoresis-MS for High Sensitivity Protein Identification capillary zone Electrophoresis (1998), 19(13), 2338-2347 electrophoresis- Figeys, D., Ahang, Y., Aebersold, R. MS Bio-compatible in-tube SPME capillary for the direct extraction and HPLC determination of drugs in human serum. 988 Drugs in human serum J.Chromatogr. A (2002) 963(1-2), 325-334 HPLC Ambient temperature, unless otherwise indicated. 95
Page 1 and 2:
SPME Applications Guide The SPME Ap
Page 3 and 4:
(New references added to the 7th ed
Page 5 and 6:
Page 7 and 8:
Page 9 and 10:
Page 11 and 12:
Page 13 and 14:
Page 15 and 16:
Page 17 and 18:
Page 19 and 20:
Page 21 and 22:
Page 23 and 24:
Page 25 and 26:
Page 27 and 28:
Page 29 and 30:
Page 31 and 32:
Page 33 and 34:
Page 35 and 36:
1232 (New references added to the 7
Page 37 and 38:
Page 39 and 40:
Page 41 and 42:
Page 43 and 44: 1496 1499 1500 (New references adde
Page 45 and 46: (New references added to the 7th ed
Page 93: (New references added to the 7th ed
Page 101 and 102: 1485 1487 1503 1506 (New references
Page 127 and 128: 1381 (New references added to the 7
Page 145 and 146:
Page 147 and 148:
Page 149 and 150:
Page 151 and 152:
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Page 161 and 162:
Page 163 and 164:
Page 165 and 166:
Page 167 and 168:
Page 169 and 170:
Page 171 and 172:
Page 173 and 174:
Page 175 and 176:
Page 177 and 178:
Page 179 and 180:
Page 181 and 182:
Page 183 and 184:
Page 185 and 186:
Page 187 and 188:
Page 189 and 190:
Page 191 and 192:
Page 193 and 194:
1522 1531 1554 1551 (New references
Page 195 and 196:
Page 197 and 198:
Page 199 and 200:
Page 201 and 202:
Page 203 and 204:
Page 205 and 206:
Page 207 and 208:
Page 209 and 210:
Page 211 and 212:
Page 213 and 214:
Page 215 and 216:
Page 217 and 218:
Page 219 and 220:
Page 221 and 222:
Page 223 and 224:
Page 225 and 226:
Page 227 and 228:
Page 229 and 230:
Page 231 and 232:
SPME Literature Literature No. Titl
Page 233:
World Headquarters 3050 Spruce St.,
show all

SPME Applications Guide - Overbrook Scientific

Create successful ePaper yourself

Delete template?

Save as template?