SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument soymilk J of Food Science 72, #7, S481-S486 (SEP 2007) Yuan, S. H.; Chang, S. K. C. Quantification of naltrexone and 6,beta-naltrexol in plasma and milk using gas chromatography-mass spectrometry. Application to studies in the lactating sheep. Naltrexone, 6,beta- 1413 naltrexol Journal of Chromatography B (2001) 761(1), 85-92. Ilett, Kenneth F.; Bencini, Roberta; Chan, Chooi Fen; Chiswell, Gregory M.; GC-MS in milk Dusci, Leon J.; Hackett, L. Peter Monitoring and fast detection of mycotoxin-producing fungi based on headspace solid-phase microextraction and headspace sorptive extraction of the volatile metabolites. 1225 Journal of Chromatography, A (2003) 985 (1-2), 127-135. GC-MS Demyttenaere, J. C. R.; Morina, R. M.; Sandra, P. 1159 Phthalates from toys Determination of bis(2-ethylhexyl) phthalate of plastic toys leached in stimulant saliva by gas chromatography with solid-phase microextraction Fenxi Ceshi Xuebao (2003) 22 (2), 34-36. Yang, Z. J.; Zhang, W. Y.; Pan, K. Y.; Yu, J. X.; Wu, C. Y.; Wang, C. Y. PDMS-fullerene GC 1210 Volatile fatty acids in rumen. Characterizing volatile fatty acids and other gases in a rumen closed in vitro fermentation system using solid phase microextraction Transactions of the American Society of Agricultural Engineers (2003) 46 (2), 585-588. Chirase, Norbert K.; Koziel, Jacek A.; Spinhirne, Jarett P. DVB/Carboxen/PDMS GC-MS 2798 Crude oil A comparison of results obtained using liquid injection and headspace SPME for crude oil analysis by GC-MS J of Chrom Sci. 46, #4, 332-338 (APR 2008) D'Auria, Maurizio; Racioppi, Rocco; Velluzzi, Vincenzina headspace GC-MS Volatile hydrocarbon biodegradation by a mixed-bacterial culture during growth on crude oil. 1412 Volatile hydrocarbons Journal of Industrial Microbiology & Biotechnology (2001) 26(6), 356-362. Van Hamme, J. D.; Ward, O. P 1311 Production of flavoured volatile organic compounds (VOCs) by Candida oleophila GK10: Optimisation using factorial design and response surface analysis Enzyme and Microbial Technology (2003) 33 (5), 668-675. Buzzini, Pietro; Davoli, Paolo; Martini, Alessandro; Pagnoni, Ugo Maria GC-MS 2791 Bromocyclen Enantioselective determination of the organochlorine pesticide bromocyclen in spiked fish tissue using SPME-GC-ECD and ICP-MS GC-ECD in fish tissue Talanta 75, #3, 710-716 (May 15 2008) ICP-MS 1443 Organochlorine pesticides in fish 1456 1468 Pheremones in mouse urine Sufentanil in human plasma Blanco-Gonzalez, E.; Fidalgo-Used, N.; Montes-Bayon, M.; Sanz-Medel, A Solid-phase microextraction as a clean-up and preconcentration procedure for organochlorine pesticides determination in fish tissue by gas chromatography with electron capture detection Journal of Chromatography A (2003) 1017(1-2), 35-44 GC-ECD Blanco-Gonzalez, Elisa; Centineo, Giuseppe; Fidalgo-Used, Natalia; Sanz- Medel, Alfredo Identification of pheromones in mouse urine by head-space solid phase microextraction followed by gas chromatography-mass spectrometry. Journal of Chromatography B (2003) 796(1), 55-62 85um Carboxen PDMS GC-MS Kayali-Sayadi, M. N.; Bautista, Jose M.; Polo-Diez, L. M.; Salazar, Ignacio Solid-phase microextraction of human plasma samples for determination of sufentanil by gas chromatography-mass spectrometry. Therapeutic Drug Monitoring (2002) 24(6), 768-774 Ambient temperature, unless otherwise indicated. 100 65um PDMS DVB, 10mins, immersion GC-MS
1485 1487 1503 1506 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Boulieu, Roselyne; Bolon, Magali; Dufresne, Christelle; Paradis, Chantal Conditions Instrument Volatiles in live biological samples Pheremones from Lepidoptera Organic compounds in elephant urine C9-C20 hydrocarbons in shellfish Applications of solid-phase microextraction to chemical analysis of live biologica samples. Trends in Analytical Chemistry (2002) 21(6-7), 428-438 Augusto, Fabio; Valente, Antonio Luiz Pires Lepidoptera (Sesamia nonagrioides (Lefebvre) (Lepidoptera Noctuidae)) by solid-phase microextraction Redia (2001) 84, 7-18 Rotundo, Giuseppe; Germinara, Giacinto Salvatore; De Cristofaro, Antonio Implementation of SPME and GC-MS to identify organic compounds in African elephant urine. Abstracts of Papers American Chemical Society (2002) 223(1-2), CHED 234 dwin, Thomas E.; Dowdy, Nichole C.; Rasmussen, L. E. L. Determination of petroleum contamination in shellfish using solid phase microextraction with gas chromatography-mass spectrometry. 100µm PDMS, 20mins, 120 degrees C, headspace GC-MS Analytical and Bioanalytical Chemistry (2002) 373(3), 147-152 100um PDMS GC-MS Stack, Mary A.; James, Kevin J.; O'Connell, Sharon Systemic availability and pharmacokinetics of thymol in humans. 1519 Thymol in humans Journal of Clinical Pharmacology (2002) 42(7) 731-737 LC-MS-MS Veit, Markus; Abel, Gudrun; Brinkhaus, Benno; Derendorf, Hartmut; Graefe, Eva-Ulrike; Kohlert, Claudia; Maerz, Reinhard W.; Schindler, Gernot 2201 Volatile organics Quantification of 31 volatile organic compounds in whole blood using SPME-GC-MS headspace GC-MS in blood J. Chromatogr. B Anal. 832, #2, 292-301 (2006) Ashley, D.; Blount, B.; Cardinali, F.; Chambers, D.;Kobelski, R.; McElprang, David O.; Morrow, John C. Optimization of solid-phase microextraction conditions for gas chromatographic determination of ethanol and other volatile compounds in blood. 1529 Ethanol in blood Journal of Chromatography B (2002) 773(1), 75-82 Zuba, Dariusz; Parczewski, Andrzej; Reichenbacher, Manfred 65um Carbowax DVB, 60 degrees C, 10mins, stirring, NaCl addtion, headspace GC-FID 2361 Hydroxychloro- Stereoselective determination of hydroxychloro-quine and its major . metabolites in human urine by SPMEand HPLC 60µm PDMS-DVB HPLC quine metabolites J. Sep Sci 3, #15, 2351-2359 (Oct-2007) 40 min at 25°C in human urine Moraes del Oliveira, A/; Sueli Bonato, P. Determination of naproxen in human urine by SPME coupled LC pH 11 10% NaCl 2272 Naproxen J Pharma Biomedical Analysis, 39, #3-4, 643-647 (2005) 50µm CW/TPR LC in human urine Aresta, Antonella; Palmisano, Francesco; Zambonin, Carlo G. 1532 Quantitation of 2-chlorovinylarsonous acid in human urine by automated solidphase microextraction-gas chromatography-mass spectrometry. 2-chlorovinylarsonous acid in human urine Journal of Chromatography B (2002) 772(1), 147-153 Calafat, Antonia M.; Ashley, David L.; Wooten, Joe V. GC-MS 1533 Fluoroacetic acid in biological samples Headspace solid-phase microextraction with 1-pyrenyldiazomethane on-fibre derivatization for analysis of fluoroacetic acid in biological samples. Journal of Chromatography B (2002) 772(1), 45-51 Ambient temperature, unless otherwise indicated. 101 85um Carboxen PDMS Stableflex, on-fiber derivatization with 1-pyrenyldiazomethane
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