SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
essential oils Lopez, P.; Sanchez, C.; Batlle, R.; Nerin, C.
Determination of microbial volatile organic compounds from
2217 Volatile organics Staphylococcus pasteuri against Tuber borchii using SPME-GC-MS GC-MS
in bacteria Rapid Communications Mass Spectrometry 19 #22, 3411-3415 (2005)
Barbieri, E.; Gioacchini, A. M.; Zambonelli, A.; Bertini, L.; Stocchi, V.
2372 poly(3-hydroxy
Use of headspace solid-phase microextraction for the quantification
of poly(3-hydroxybutyrate) in microbial cells headspace GC-FID
-butyrate) J. Chromatogr., A 1154, #1-2, 34-41 (2007-06-22)
in microbial cells Monteil-Rivera, F.; Betancourt, A.; van Tra, H.; Yezza, A.; Hawari, J
811 Volatile hydrocarbon
Development of a method for the application of SPME
to monitor biodegradation of volatile hydrocarbons GC-FID
from bacterial during bacterial growth on crude oil 45min @ 30°C
growth J Indus Microb & Biotech (2000) 25(3), 155-162
Van Hamme, J. D.; Ward, O
headspace
Solid-phase microextraction of volatile compounds from the chopped leaves of
three species of Eucalyptus.
Volatile compounds
1054 from Eucalyptus. Journal of Agricultural and Food Chemistry (2003) 51 (9), 2679-2686.
Pawliszyn, Janusz; Caramao, Elina B.; Christensen, Eva; Zanin, Kelen D.; Zini,
Claudia A.
Sampling and sample preparation for analysis of aromas and fragrances.
1082 Aromas and fragrances Trends in Analytical Chemistry (2003) 22 (3), 160-169.
Augusto, Fabio; Leite e Lopes, Alexandre; Zini, Claudia Alcaraz
Localization and speciation of selenium and mercury in Brassica
2169 Selenium, mercury juncea - Implications for Se-Hg antagonism headspace GC-ICP-MS
in plants J Anal At Spectrom 21, #4, 404-412 (2006) GC-TOFMS
Caruso, J.; Meija, J.; Mounicou, S.; Shah, M.; Shann, J.; Vonderheide,A.
Simultaneous monitoring of volatile selenium and sulfur species from Se
accumulating plants (wild type and genetically modified) by gas chromatography
mass spectrometry and gas chromatography-inductively coupled plasma mass
spectrometry using solid-phase microextraction for sample introduction.
Selenium and sulfur
1092 from plants. Analytical Chemistry (2002) 74 (22), 5837-5844.
Meija, J.; Montes-Bayon, M.; Le Duc, D. L.; Terry, N.; Caruso, J. A.*
GC-ICP MS
Use of solid-phase micro-extraction as a sampling technique in the
determination of volatiles emitted by flowers, isolated flower parts and pollen
1120 Volatiles from flowers Journal of Chromatography A (2003) 1000 (1-2), 229-233.
Cioni, Pier Luigi; Flamini, Guido; Morelli, Ivano
2598 Volatile organics
Enantiomeric purity of (+/-)-methyl jasmonate in fresh leaf samples
and commercial fragrances headspace GC/MS.
from Jasminum J. Sep. Sci.30, #13, 2117-2122 (August 2007)
leaves Blanch, Gracia P.; Ruiz del Castillo, Maria Luisa
Composition and antimicrobial activity of Anemopsis
2220 Volatiles californica leaf oil GC
from califonica leaf J Ag Food Chem, 53, #22, 8694-8698 (2005)
Medina, A.; Lucero, M.; Holguin, F.; Estell, R.; Posakony, J.;
Simon,J.; O'Connell, M
The composition of dalea formosa oil determined by steam
2228 Volatile organics distillation and SPME 100um PDMS GC-FID and
in dalea J. Essent. Oil Res. 17 #6, 645-647 (2005) GC/MS.
formosa oil Estell, Rick E.; Lucero, Mary E.; Sedillo, Ruth L.
Identification and quantification of methyl jasmonate in leaf volatiles of
Arabidopsis thaliana using solid-phase microextraction in combination with gas
chromatography and mass spectrometry.
Ambient temperature, unless otherwise indicated. 80