SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
1854 Fluoroacet- using GC-MS after SPME. 100µm PDMS GC-MS
amide in body J Chromatogr, B:802, #2, 239-245 25min @ 70°C
fluids Cai, X.; Zhang, D.; Ju, H. X.; Wu, G.; Liu, X. immersed
Sensitive methods for trace level analysis of
1855 Trichloro- trichloroethylene (TCE) in rat blood and tissues. headspace @ 55°C GC-MS
ethylene in Proc. 50th ASMS Conf. Mass Spectrom. Allied Top.
blood/tissues 2002, p629-630
Bartlett, Michael G.; Brown, Stacy D.; Bruckner, James V.;
Dixon, Amy M.; Muralidhara, S.
Photocatalytic oxidation of aqueous trichloroethylene using dye
2916 Trichloro- sensitized buoyant photocatalyst monitored via micro-headspace 100µm PDMS GC/ECD
ethylene in SPME-GC-ECD and MS headspace
water Microchemical Journal 88, #1, 38-44 (FEB 2008)
Alexander, Matt V.; Rosentreter, Jeffrey J.
Trace level determination of trichloroethylene in biological samples
2794 Trichloro- by headspace SPME-GC/negative chemical ionization MS 100µm PDMS GC-MS
ethylene in Rapid Communications in Mass Spectrometry 22, #6 797-806 (2008) headspace
biological samples Liu, Yongzhen; Muralidhara, S.; Bruckner, James V.; Bartlett, M.
Determination of trichloroethylene in biological samples by headspace
2770 Trichloro- SPME-GC-MS 100µm PDMS GC-MS
ethylene in J Chromatogr, B: 863, #1, 26-35 (2008) headspace
biological samples Liu, Yongzhen; Muralidhara, S.; Bruckner, James V.; Bartlett, M.
A study of the performance characteristics of immunoaffinity SPME
2457 Benzodiaze- probes for extraction of a range of benzodiazepines.
pines in J. Pharm. Biomed. Anal. 44, #2, 506-519 (2007-06-28)
blood Lord, H. L.; Rajabi, M.; Safari, S.; Pawliszyn, J.
Analysis of benzodiazepines from whole blood
1856 Benzodiaze- by SPME coupled to LC-MS-MS 50µm CW-TPR LC-MS-MS
pines in Proc. 50th ASMS Conf. Mass Spectrom. Allied Top.
whole blood 2002, p513-514
Grant, R; Incledon, B; Lord, H; Pawliszyn, Janusz
Application of the standard addition approach for the
1857 Benzene in quantification of urinary benzene headsapce GC-MS
urine J. Chromatogr. B, 818, #2, 293-299
Acampora, A.; Basilicata, P.; Miraglia, N;
Pieri, M.; Sannolo, N.; Soleo, L.
Determination of urinary ortho- and meta-cresol in
1858 Cresols in humans by headspace SPME-GC-MS 100µm PDMS GC-MS
urine J. Chromatogr. B, 817, #2, 309-317 headsapce
Campo, L.; Foa, V.; Fustinoni, S.; Mercadante, R.;
Scibetta, L.; Valla, C.
SPME and chiral HPLC analysis of ibuprofen in urine
1859 Ibuprofen J. Chromatogr.B, 818, #2, 285-291 65µm PDMS- DVB HPLC-UV
in urine Bonato, P.; Cesarino, E.; De Oliveira, A. immersion sampling
Stereoselective determination of the major ibuprofen
1860 Ibuprofen metabolites in human usrine by off-linecoupling SPME-HPLC 50µm CW-TPR HPLC
metabolites Anal. Chim. Acta, 538, #1, 25-34 immersion sampling
in urine De Oliveira, A;, DeSantana, Fo; Bonato, P
Simultaneous determination of barbiturates in human
1861 Barbiturates biological fluids by direct immersion SPME and GC-MS immersion sampling GC-MS
in blood/urine J. Chromatogr. B, 806, #1, 65-73 salt added
Arinobu, T.; Hattori, H.; Ishii, A.; Iwai, M.; Suzuki, O.;
Kumazawa, T., Noguchi, H., Noguchi, H.; Seno, H.
Monitoring of urinary acrolein concentration in
1862 Acrolein in patients receiving cyclophosphamide and ifosphamide headsapce GC-MS
urine J. Chromatogr. B, 806, #1, 59-63
Namera, A.; Sakura, N.; Takamoto, S.; Yashiki, M.
Headspace SPME and capillary GC-MS determination
1863 Rivastigmine of rivastigmine in canine plasma samples 65µm PDMS/DVB GC-MS
in plasma J. Chromatogr. B, 806, #2, 271-276 30min @ 100°C
Deng, Chunhui; Duan, Gengli; Huang, Taomin; Liu, Zhen; headspace
Sha, Yunfei; Yang, Bei NaOH/NaCO 3 buffer
Ambient temperature, unless otherwise indicated. 105