SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Optimization of SPME for the GC-MS analysis of
2041 Organic persistent organic pollutants varios fibers GC/MS
pollutants J AOAC Int, 87, #4, 1021-1027
from water Alpendurada, M.; Gago-MARTINEZ, A; Nogueiras, M,
Prado, Juan; Rellan, Satvdra;Vetter, Walter
Use of headspace SPME to characterize odour
2042 Amines, fatty compounds in subsurface flow constructed wetland headspace GC/MS or GC/NPD
acids, alky- for wastewater treatment
sulfides in Water Sci. Technol., 49, #9, 89-98
wastewater Aguirre, P.; Bayona, J.M.; Garcia, J.; Huang, Y.;
Mujeriego, R.; Ortiz, L.
Development of a simple and sensitive method for the
2043 Odourous characterization of odorous waste gasemissions by 75µm Carboxen GC/MS or GC/FID/O
compounds means of SPME-GC-MS/olfactometry headspace
from waste Waste Manage., 25, #9, 872-879
gas Jans, M.; Kleeberg, K.K.; Liu, Y.; Schlegelmilch, M.;
Stegmann, R.; Streese, J.
Comparison of strategies for extraction of high
2044 PAHs in molecular weight PAHs from drinking waters immersion sampling HPLC-FLD
drinking water J Agr Food Chem, 52, #23, 6897-6903
Garcia-Falcon, M. S.; Perez-Lamela, M.;
Simal-Gandara, J.
Determination of PAHs in water by SPME-HPLC
2045 PAHs in Analytical Sciences, 20, #10, 1383-1388 35min immersed extract HPLC-FLD
water Chen, H. W. added 1.5M sodium
monochloroacetate
Determination of organochlorides in water using
2046 organochlorides solid-phase microextraction coupled to GC 65µm PDMS-DVB GC
in water Am Lab, 34. #17, 12-14 45sec @ 50°C
Huang, Min-Jia; Li, Ju-Bai; Liang, Bing; Ou, Qing-Yu
SPME measurement of parent and alkyl PAHs in
2047 PAHs in milliliter sediment pore water samples and immersion sampling GC/ MS
water determination of K' values
Environ. Sci. Technol,.39, #8,2795-2803
Grabanski, C.; Hawthorne, S.; Kreitinger, J..; Miller, D.
Coupling of SPME with MCC/UV-IMS as a tool for rapid on-site
2048 Organics in detection of groundwater and surface water contamination headspace UV-IMS
groundwater Anal. Bioanal. Chem., 382, #8, 1842-1847
Baumbach, J.I.; Klockow, D.; Walendzik, G.
Simultaneous picogram determination of "earthy-musty" odorous
2292 Trichloroanisoles compounds in water using SPME-GC-MS coupled with initial cool DVB/CAR 50/30µm GC/MS
and gesomin in programmable temperature vaporizer inlet headspace
water J. Chromatogr. A 1098, #1-2, 7-13 (2005)
Hu, Ruikang; Yang, Zhaoguang; Zhang, Lifeng
Detection of 2,4,6-trichloroanisole in chlorinated water at
2049 2,4,6-Trichloro- nanogram per litre levels by SPME-GC-ECD 100µm PDMS GC-ECD
anisole in Anal. Bioanal. Chem., 382, #2, 341-346 headspace
chlorinated Da Silva, Joaquim C. G. Esteves; Pinheiro, Paula B. M.
water
SPME and headspace derivatization of clenbuterol followed
2050 Clenbuterol by GC-FID and GC-SIMMS quantification 85µm polyacrylate GC-FID, GC-MS
in water Anal. Bioanal. Chem., 375, #3, 460-464 HMDS derivative
Engelmann, M.D.; Hinz, D.; Wenclawiak, B.W. headspace
Use of SPME-GC-ECD for the determination of energetic
2051 Explosives chemicals, in marine samples 65µm CW/DVB GC-ECD
in water J Chromatogr A, 1066, #1-2, 177-187 30% salt added
Monteil-Rivera, Fanny; Beaulieu, Chantale; Hawari, J.
SPME ion mobility spectrometer interface for explosive
2051 Explosives and taggant detection headspace Ion mobility
in water J Sep Science, 28, #2, 177-183 spectrometry
Perr, Jeannette M.; Furton, Kenneth G.; Almirall, J.
2052 Explosives
Determination of explosives in environmental water samples
by SPME-liquid chromatography 50µm CW-TPR HPLC-UV
in water J. Chromatogr. A, 1048, #2, 213-221
Beaulieu,C.; Deschamps,S.; Hawari,J.;
immersed
Ambient temperature, unless otherwise indicated. 181