SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Reliable characterization of coffee bean aroma 1645 Volatiles in profiles by automated headspace SPME-GC-MS with headspace GC-MS coffee beans the support of a dual-filter mass a dual-filter spectra library J. Sep. Sci., 28, #9-10, 1101-1109 Casilli, A, Costa, R; Dugo, G, Dugo, P; Festa, S; Mondello, L; Tranchida, P. Analysis of furan in foods by headspace SPME-GC-IT-MS 2401 Furan in J. Chromatogr., A 1146, #1,103-109 (2007-03-30) 75µm Carboxen GC-IT-MS food Altaki, M. S.; Santos, F. J.; Galceran, M. T. headspace Development and validation of a SPME-GC-MS method for the 2160 Furan in determination of furan in baby-food GC-MS baby-food J. Chromatogr. A, (2006) 1102, #1-2, 268-272 Bianchi, Federica; Careri, Maria; Mangia, Alessandro; Musci, Marilena Impact of ionizing radiation and thermal treatments on furan 2276 Furan in levels in fruit juice headspace GC-MS fruit juice J Food Science (2005) 70 #7, E409-E414 Fan, Xuetong Determination of furan levels in coffee using 1646 Furan in automated SPME-GC-MS headspace GC-MS coffee JAOAC Intl, 88, #2,574-576 Ho, I-Pin; Yoo, Seong-Jae; Tefera, Sebhat SPME-GC-MS and multivariate analysis 1647 Volatiles in for the characterization of roasted coffees headspace GC-MS roasted Talanta, 66, #1, 261-265 coffee Zambonin, C.; Balest, L.; De Benedetto, G.; Palmisano, F. Volatile composition of Gutierrezia sarothrae (broom snakeweed) 2212 Volatiles from as determined by steam distillation and SPME GC-MS broom J. Essent. Oil Res.18 #2, 121-125 (2006) GC-FID snakeweed Estell, R.; Fredrickson, E.; Lucero, M.; Morrison, A.; Richman, D. A direct liquid, non-equilibrium SPME application 1648 Essential oils for analysing chemical variation of single peltate 100µm PDMS fiber GC-MS from leaves trichomes on leaves of Salvia officinalis immersed Phytochemical Analysis, 15, #3, 198-203 Grassi, P.; Novak, J.; Steinlesberger, H.; Franz, C. GC-olfactometric characterization of aroma active 1649 Aroma from compounds in sun-dried and vacuum-dried tarhana Headspace GC-FID Tarhana European Food Res &Tech, 218, #6, 573-578 Goemen, D; Gurbuz, O; Rouseff, R; Smoot, J.; Dagdelen, A Lactic acid fermentation of Brassica rapa: 1650 Aroma from chemical and microbial evaluation of a typical headspace GC-FID fermentation Italian product (brovada) process European Food Res &Tech, 218, #5, 469-473 Maifreni, Michela; Marino, Marilena; Conte, L Monitoring acetaldehyde concentrations during micro-oxygenation of . 2687 Acetaldehyde red wine by headspace SPME with on-fiber derivatization headspace GC-FID in red wine J Agr Food Chem 55, #14, 5620-5625 (2007) PFBH derivative Carlton, W. K.; Gump, B.; Fugelsang, K.; Hasson, A. S. Determination of haloanisoles in paper samples for food packaging 2728 Haloanisoles from by solid-phase microextraction and gas chromatography DVB/CAR 50/30µm GC-MS packaging Microchim. Acta 159, #3-4, 229-234 (2007) headspace Martendal, E.; Budziak, D.; Debastiani, R.; Carasek, E. 30min @ 70°C Comparison of stir bar sorptive extraction and SPME to determine 2792 Haloanisoles and halophenols and haloanisoles by GC-iontrap MS halophenols Talanta 75, #3, 753-759 (May 15 2008) headspace GC-iontrap MS in water Alonso, G.; Maggi, L.; Mazzoleni, V.; Salinas, M..; Zalacain, A. Multiple headspace solid-phase microextraction for eliminating matrix 2686 Haloanisoles and effect in the simultaneous determination of haloanisoles and DVB/CAR 50/30µm GC-MS/MS halophenols volatile phenols in wines headspace in wine J. Chromatogr., A 1166, #1-2, 1-8 (2007) Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M. Ambient temperature, unless otherwise indicated. 56
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Optimisation of a headspace SPME with on-fiber derivatisation method 2407 Haloanisoles and for the direct determination of haloanisoles and halophenols in wine. 85µm polacrylate GC-ECD halophenols J. Chromatogr., A 1143, #1-2, 26-35 (2007-03-02) 60min @ 70°C in wine Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M. headspace MSTFA derivative Study of chloroanisoles assay and TCA assay validation in wine and 2289 Trichloroanisole cork stoppers soaked in dilute alcohol solution using headspace GC-MS/ from wine & cork SIDA-HSSPME-GC-MS/EI-SIM EI-SIM stoppers J Intl des Scie de la Vigne et du Vin 39 #3, 137-147 (2005) Chatonnet, P.; Labadie, Dominique; Boutou, S. Matrix effect during the application of a rapid method using HS-SPME 2542 2,4,6-trichloro followed by GC-ECD for the analysis of 2,4,6-TCA in wine and cork soaks Headspace GC-ECD anisole in Food Chemistry 105, #2, 681-690 (2007) cork Vlachos, P.; Kampioti, A.; Kornaros, M.; Lyberatos, G. Relationship between sensory and instrumental 1651 2,4,6-trichloro analysis of 2,4,6-trichloroanisole in wine and cork Headspace GC-ECD anisole in stoppers wine/cork Anal. Chim. Acta, 513, #1, 291-297 Antico, E.; Garcia Regueiro, J.A.; Guerrero, L.; Insa, S.; . Juanola, R.; Salvado, V.; Subira, D Determination of fluoride in toothpaste using headspace SPME-GC-FID 2452 Floride in J. Chromatogr., A 1150, #1-2, 173-177 (2007-05-25) 75µm Carboxen GC/FID toothpaste Wejnerowska, G.; Karczmarek, A.; Gaca, J. Headspace TMCS derivative Assay of stability, free and total concentration of 1652 Chlloro- chlorhexidine in saliva by solid phasemicroextraction headspace GC hexidine in J Pharma and Biomed Analysis, 37, #5, 1015-1024 saliva Musteata, Florin Marcel; Pawliszyn, Janusz Improving headspace-SPME of 3-isobutyl-2- 1653 Pyrazines methoxypyrazine by experimental design with regard headspace GC-MS in wine to stable isotope dilution GC-MS analysis of wine saturated salt Anal. Chim. Acta, 513, #1, 223-227 Lucchese, Y.; Nepveu, F.; Prouteau, C.; Renard, R.; Schneider, R.;Vaca-Garcia, C. Determination of terpenes in tequila by SPME-GC-MS 2575 Terpenes in J. Chromatogr., A 1134, #1-2, 291-297 (2006-11-17) 100µm PDMS GC-MS tequila Pena-Alvarez, A.; Capella, S.; Juarez, R.; Labastida, C. 30min @ 25°C headspace, sat salt Optimization of SPME methods for GC-MS 1654 Terpenes in determination of terpenes in wine 100µm PDMS GC-MS wine J Sci of Food and Agr, 85, #7, 1227-1234 15min @ 20°C Pena, R.; B, Julia; Herrero, C; Garcia-Martin, S. immersed 25% NaCl Comparative study of sampling systems combined with gas sensors 2677 Volatiles in for wine discrimination headspace GC Spanish wine Sens. Actuators B, Chem. (Switzerland) 126, #2, 616-23 (1 Oct. 2007) Lozano, J.; Santos, J.P.; Gutierrez, J.; Horrillo, M.C. Sensory profiling of aroma in Greek dry red wines using rank-rating 2692 Volatiles in and monadic scoring related to headspace composition headspace GC Greek wine European Food Res. and Technology 225, #5-6, 749-756 (SEP 2007) Koussissi, Elisabeth; Paterson, Alistair; Piggott, John R. A survey of Saccharomyces populations associated with wine 2845 Volatiles in fermentations from the Apulia region (South Italy) headspace GC wine yeast Annals of Microbiology 57, #4, 545-552 (2007) Tofalo, R.; Torriani, S.; Chaves-Lopez, C.; Martuscelli, M.; Paparella,Antonello; Suzzi, Giovanna Comparative study of aromatic compounds in young red wines from 2614 Aromatic volatiles cabernet sauvignon, cabernet franc, and cabernet gernischet headspace GC in red wines varieties in China. J Food Sci 72, #5, C248-52 (2007 Jun) Zhang, M; Xu, Q; Duan, C; Qu, W; Wu, Y Factors influencing sensory quality in red wines of the variety 2419 Volatiles in Aghiorghitiko (Vitis vinifera L.) from Nemea headspace GC-MS red wine Eur. Food Res. Technol. 226, #4, 745-753 (February 2008) Koussissi, Elisabeth; Paraskevopoulos, Yiannis; Paterson, Alistair Ambient temperature, unless otherwise indicated. 57
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