SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Jezova, V.; Skladal, J.; Eisner, A.; Bajerova, P.; Ventura, K. Pedersen-Bjergaard, S. Conditions Instrument Measurement of octanol-air partition coefficients using solid-phase microextraction ( SPME ): Application to hydroxy alkyl nitrates. 1400 Hydroxy alkyl nitrates. Atmospheric Environment (2001) 35(33), 5843-5854. Rudich, Yinon; Shragina, Lea; Treves, Keren Application of low-temperature glassy carbon films in solid-phase microextraction 1429 Aromatic hydrocarbons Anal. Chem. (2001) 73(24), 5841-5851. GC-FID Giardina, M.; Olesik, S.V. 1430 Atomic spectrometry update. Industrial analysis: Metals, chemicals and advanced materials J Anal At Spectrom (2001) 16(12), 1446-1469. Fairman, B.; Goodall, P.; Hinds, M.W.; Nelms, S.M.; Penny, D.M. ICP-MS 1435 VOC's Application of the polysilicone fullerene coating for solid-phase microextraction in the determination of semi-volatile compounds Journal of Chromatography A (2001) 927(1-2), 121-130. Han, S.; Wang, Z.; Wu, C.; Xiao, C.; Xing, J. PDMS GC-FID 1507 Aliphatic carboxylic acids Solid-phase microextraction and on-line methylation gas chromatography for aliphatic carboxylic acids. Analytical and Bioanalytical Chemistry (2002) 373(1-2), 64-69 Various fibers compared GC-MS Danielson, Neil D.; Cho, Seong R.; Liu, Yaqian Effect of masking agents on the emission of VOCs from asphalt. 1502 VOCs from asphalt Abstracts of Papers American Chemical Society (2002) 223(1-2), CHED 451 Smith, Crystal; Hardee, John Determination of impurities in industrial caprolactam produced 2213 Impurities in from toluene by SPME and GC-MS GC-MS caprolactam J. Appl. Polym. Sci.100 #4, 3141-3144 (2006) Li, Na; Zou, Jiankai Capillary extractors for left dbl quote negligible depletion right dbl quote sampling of benzene, toluene, ethylbenzene and xylenes by in-tube solid-phase microextraction. 1227 BTEX Journal of Chromatography, A (2003) 985 (1-2), 85-91. Nardi, L. 1099 Method for determining chlorohydrocarbon residues in dry cleaning fabrics with gas chromatography-mass spectrometry. Chlorohydrocarbon in dry cleaning fabrics. Sepu (2002) 20 (6), 573-576. Chen, J. 100 um PDMS GC-MS 1257 Formic acid Quantitation of formate by solid-phase microextraction and gas chromatography mass spectrometry utilizing a " 13 C"formate internal standard. Journal of Chromatography, A (2003) 986 (2), 313-317. Kim, J. K.; Shiraishi, T.; Fukusaki, E.; Kobayashi, A. * GC-EIMS Before the injection - Modern methods of sample preparation for separation Review techniques 1119 Review article Journal of Chromatography A (2003) 1000 (1-2), 3-27. Smith, Roger M. Derivatization - solid-phase microextraction techniques and its application to analysis of organic compounds. 1269 Review Fenxi Huaxue (2003) 31 (4), 496-500. Luan, T. G.; Zhang, Z. X. Ambient temperature, unless otherwise indicated. 228
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument A field guide to instrumentation: modern sample preparation methodology. 1. Automated SPE. 1371 Review Inside Laboratory Management (2001) 5(5), 14-18. Sherma, J.; Larkin, J. D.; Larkin, F. H. A new thermal desorption SPME system for hand-held 2310 volatile organic ion mobility spectrometry headspace GC/MS Anal. Chim. Acta 559 #2, 159-165 (2006) Grigoriev, A.; Liu, Xinyu; Lynds, Paul; Nacson, S.; Pawliszyn, J. Thermal desorption SPME inlet for differential 2124 BTX solvents mobility spectrometry differential mobility in water Appl Spectrosc, 59, #6, 754-762 spectrometry De Harrington, Peter B.; Rainsberg, Matthew R. A review on SPME-HPLC analysis of pesticides 2125 pesticides Crit. Rev. Anal. Chem., 35, #1,71-85 in-tube HPLC various Aulakh, J.; Kaur, V; Malik, A.; Schmitt-Kopplin, P matrices Kinetic Calibration Using Dominant Pre-equilibrium Desorption for 2399 PAH standards On-Site and in Vivo Sampling by Solid-Phase Microextractio in water Anal Chem 80. #2, 481-90 (2008 Jan 15) Zhou, Simon Ningsun; Zhao, Wennan; Pawliszyn, Janusz On-fiber standardization technique for solid-coated SPME 2427 Carbamate Anal. Chem. 79, #3, 1221-1230 (2007-02-01) 50µm Carbowax/TPR, pesticide Zhou, S. N. S.; Zhang, X.; Ouyang, G. F.; Es-haghi, A.; Pawliszyn, J. 2398 Pre-loaded Preparation and application of in-fibre internal standardization SPME Analyst (Cambridge, U. K.) 132, #3, 256-261 (2007-03-15) headspace GC standard on fiber Zhao, W. N.; Ouyang, G. F.; Pawliszyn, J. Flow-through system for the generation of standard aqueous solution 2183 PAH standards of polycyclic aromatic hydrocarbons in water J. Chromatogr. A, 1105, #1-2,176-179 (2006) Chen, Yong; Ouyang, Gangfeng; Pawliszyn, Janusz System for the generation of standard gas mixtures 2126 Volatiles & of volatile and semi-volatile organic compounds fo headspace GC seimivolatiles calibrations of SPME and other sampling devices in air J Chromatogr A, 1025, #1, 3-9 Koziel, Jacek; Martos, Perry.; Pawliszyn, J Origin of carbons in sulfur-containing aroma compounds from the 2191 Sulfur compd Maillard reaction of xylose, cysteine and thiamine headspace GC-MS from Mailard Food Sci. Technol. 40, #8, 1309-1315 (Oct. 2007) reaction Cerny, C. Small alpha -Mercaptoketone formation during the 2127 Sulfur compd Maillard reaction of cysteine and C13 ribose headspace GC-MS from Mailard J Agrl Food Chem, 52, #4, 958-961 reaction Cerny, C.; Davidek, T. * Role of the solvent glycerol in the Maillard reaction of D-fructose 2163 Volatiles from and L-alanine headspace GC-MS D-fructose and J Ag Food Chem, 54, #2, 574-577 (2006) 130 C L-alanine Cerny, Christoph; Guntz-Dubini, Renee SPME based on polypyrrole films with different counter ions 2128 Review Anal. Chim. Acta, 520, #1-2, 257-264 polypyrrole Pawliszyn, Janusz; Wu, Jingcun Coupling of dynamic headspace sampling and SPME 2129 Review Chromatographia, 60, #11-12, 687-691 headspace GC Silva, R. C.; Aguiar, P. M. S.; Augusto, F. * Extraction techniques 2130 organics from Anal. Bioanal. Chem., 372, #1, 39-40 comparison w/SFE, GC water Camel, Valerie microwave, pressure solvent Methyl benzoate as a marker for the detection of mold in indoor Ambient temperature, unless otherwise indicated. 229
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