SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in soil Baciocchi, R.; Attina, M.; Lombardi, G.; Boni, M. R Determination of chlorophenols in soil using accelerated 60min. @ 20°C immersion, pH 1 719 Chlorophenols solvent extraction combined with SPME 85µm polyacrylate GC-MS in soil Anal. Chem. (2000), 72(3), 46-551 20min. @ 20°C Wennrich, L, Popp, P., Moeder, M. Headspace SPME for the determination of volatile and immersion, pH 2 satr NaCl 531 Volatiles and semivolatile pollutants in soils 100µm PDMS GC-MSD semivolatiles Talanta (1999), 48(2), 451-459 30 min @ 20°C in soils/water Llompart, M., Li, K., Fingas, M. headspace 532 PAHs, hydrocarbons Investigation by SPME and GC-MS of organic films on stone monuments GC-MS in pollutant crust Rapid. Commun. Mass Spectrom. (1999), 13(10), 895-900 Angelis, F., Di Tullio, A., Mellerio, G., Quaresima, R, Volpe, R 533 Aldehydes, acids Degradation of palmitic (Hexadecanoic) acid deposited on TiO2 coated self cleaning glass: kinetics of disappearance, from palmitic acid intermediate products and degradation pathways New J. Chem (1999), 23(4), 365-374 Romeas, V., Pichat, P., Guillard, C., Chopin, T., Lehaut, C. 534 PAHs in Interaction between natural organic matter (NOM) and polycyclic aromatic compounds, Comparison of 85µm polyacrylate GC-MS organic matter fluorescence quenching and SPME 30 min Fresenius'J. Anal. Chem. (1999), 364(4), 313-319 pH3, immersed Myung, S., Kim, M., Min, H., Yoo, E. Kim, K. alkyl formate derivative 172 Elemental analysis Elemental and Organometallic Analysis of Soil Using Glow-Discharge MS and GC-MS 100µm PDMS GC-MS of soil Rapid Commun. Mass Spectrom. 10: 341-346 (1996) 50°C, 10 min Barshick, C., Barshick, S., Mohill, M., Britt, P., Smith, D. salt added 174 Mercury species in Performance Improvements in the Determination of Mercury Species in Natural Gas Condensate Using Online GC-ICP natural gas condensate Amalgamation Trap or SPME with Capillary GC-Microwave- Induced Plasma Atomic Emission Spectrometry Analyst 121: 1055-1060 (1996) Snell, J., Frech, W., Thomassen, Y. 535 Organomercury SPME and GC-MIP-AED for the speciation analysis of organomercury compounds GC-MIP-AED in soil and water J. High Resolut. Chromatogr. (1999), 22(3), 181-182 Mothes, S., Wennrich, R. Headspace solid-phase microextraction (HS-SPME) for the 2314 BTEX in determination of BTEX in foundry molding sand 75µm Carboxen GC/MS sand Analytical Letters 38 #14, 2393-2405 (2005) headspace Dungan, Robert S. 239 BTEX, chlorinated The Determination of Volatile Organic Compounds in Soils Using SPME with Gas Chromatography-Mass Spectrometry 100µm PDMS GC-MS hydrocarbons J. High Res. Chromatogr. 19: 515-519 (1996) 5 min in soil James, K., Stack, M. headspace 197 VOCs in Environmental Analysis of Volatile Organic Compounds in Water and Sediment by GC overview water and sediment J.Chromatogr. A 733A 733: 119-141 (1996) (review) Kuran, P., Sojak, L. article 536 VOCs in Determination of VOC contamination in borehole sediments by headspace SPME-GC analysis sediment Fresenius' J. Anal. Chem 1999, 364(7), 645-647 water solution Dermietzel, Jurgen, Strenge, G. headspace Ambient temperature, unless otherwise indicated. 198
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 768 Tributyltin Determination of tributyltin by automated in-tube SPME with HPLC-ES-MS In-tube SPME LC-ES-MS in water J Anal At Spectrom (2001) 16(2), 159-165 Wu, J; Mester, Z; Pawliszyn, J. Supel-Q PLOT 720 Butyltin Determination of butyltin compounds in aqueous samples by GC w/FPD and headspace SPME after GC-FID in water in-situ hydride derivatization Aanl. Sci. 2000, 16(6), 585-588 Jiang, G, Liu, J. Determination of butyltin compounds in sediments NaBEt4 Japanese 771 Butyltin by headspace SPME and capillary GC w/FPD using quartz GC-FPD in sediment surface induced luninescence Fenxi Huaxue (20001) 29(2), 158-160 Liu, J; Jiang, G. KBH-4 in Chinese 721 Butyltin Determination of butyltin species in water and sediment by SPME-GC-FID GC-FID in water J.Chromatogr. A (2000), 873(1), 61-71 Millan, E., Pawliszyn, J. NaBEt4 Solid phase microextraction as a tool for trace 888 element speciation Spectrochim. Acta, Part B (2001) 56B(3), 233-260 Mester, Z.; Sturgeon, R.; Pawliszyn, J. 852 Butyltin Speciation of butyltin compounds in marine sediments with headspace SPME and gas chromatography: MS 100µm PDMS GC-MS in marine sediment Fresenius' J. Anal. Chem 2001, 369(6), 510-515 Cardellicchio, N.; Decataldo, A.; Di Leo, A.; Giandomenico, S. headspace NaBEt4 derivative 722 Butyl-, phenyltin SPME: a new procedure for the control of butyland phenyltin pollution in the environment by GC-FID 100µm PDMS GC-FID in water Analyst (Cambridge, UK) 2000, 125(2), 263-268 60 min, immersed Aguerre, S., Montigny, C, Lespes, G., Gaultier, M. NaBEt4 199 Organotin in humic organic Solid Phase Microextraction to Study the Sorption of Organotin Compounds onto Particulate and Dissolved 100µm PDMS GC-MS matter Humic Organic Matter 30 min Environ. Sci. Technol. 31: 3629-3636 (1997) Poerschmann, J., Kopinke, F., Pawliszyn, J. immersion 343 Methylmercury Development of a Technique for the Analysis of Inorganic Mercury salts in Soils by GC-MS 100µm PDMS, GC-MS derivative Intl. J. Mass Spectrometry 178 (1998) 31-41 65µm PDMS/DVB in soil Barshick, C., Barshick, S., Britt, P., Lake, D., Vance, M., 50°C, 5 min Walsch, E. Determination of methylmercury by SPME-ICP-MS: a new stirring, salt added methyl bis(dimethylgloximate) pyridinecobalt (III) 723 Methylmercury sample introduction method for volatile metal species ICP-MS derivative J. Anal. AT. Spectrom (2000) 15(7), 837-842 in soil Mester, Z., Lam, J., Sturgeon, R, Pawliszyn, J. Applications of Sorbent Extraction in Environmental Analysis 209 Chem. Anal. (Warsaw) 42 (3): 297-314 (1997) Gorlo, D., Namiesnik, J., Zygmunt, B. Coupled Subcritical Water Extraction with SPME for Ambient temperature, unless otherwise indicated. 199
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