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SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference Conditions<br />

stirring<br />

Instrument<br />

390 Organophosphorus<br />

<strong>SPME</strong> for quantitative analysis of organophosphorus<br />

Pesticides in Environmental Water Samples 100µm PDMS, GC-NPD<br />

pesticides J. Chromatogr. A 808 (1998) 257-263 85µm polyacrylate<br />

in water Beltran, J., Lopez, F., Hernandez, F.<br />

<strong>SPME</strong> for the determination of systemic and non-volatile<br />

30 min<br />

stirring, salt added<br />

706 Pesticides pesticides in river water using GC with NPC and ECD 100µm PDMS GC-NPD<br />

in water J. Chromatogr. A 893(2000) 347-358 15min ECD<br />

Sampedro, M.; et al immersed<br />

868 Herbicides<br />

Determination of herbicides in natural waters using (<strong>SPME</strong>)<br />

and GC coupled with flame thermionic and MS detection GC-MS<br />

in water Int. J. Environ. Anal. Chem (2000) 78(3-4), 223-240<br />

Lambropoulou, D.; Konstantinou, I; Albanis, T.<br />

707 Nitrogen herbicides<br />

Use of <strong>SPME</strong> for the Quantitative determination of<br />

Herbicides in soil and water samples Carbowax DVB GC-MS<br />

in water Anal. Chem. 2000, 72, 2313-2322 30 min SIM mode<br />

Hernandez, F., Beltran, J., Lopez, F, Gaspar, J. salt added, stirred<br />

28 Nitrogen herbicides<br />

Solid Phase Microextraction of Nitrogen-Containing<br />

Herbicides 85µm polyacrylate GC-NPD<br />

in water J Chromatogr. 704: 163-172 (1995) 50 min<br />

Boyd-Boland, A., Pawliszyn, J. immersion<br />

pH 2, salt added<br />

53 Triazine herbicides<br />

Automated Determination of S-Triazine Herbicides<br />

Using Solid-Phase Microextraction 100µm PDMS GC-NPD<br />

in water J. Chromatogr. 705: 305-312 (1995) 15 min (manual)<br />

Barnabas, I., Dean, J., Fowlis, I., Owen, S.<br />

Determination of Triazine Herbicides in Environmental Samples<br />

3 min (automated)<br />

immersion<br />

177 Triazine herbicides J. Chromatogr. 733: 295-335 (1996) (review) 100µm PDMS GC-NPD<br />

Dean, J., Wade, G., Barnabas, I.<br />

Validation of <strong>SPME</strong> for the Analysis of Triazine Herbicides<br />

10 min<br />

immersion (water)<br />

111 Triazine herbicides at ppt Level in Aqueous Samples Carbowax/DVB GC-NPD,<br />

in water J. Chromatogr. A. 795 (1998) 371-376 30 min GC-MS<br />

Nilsson, T., Ferrari, R., Basta, R., Dellavedova, P. immersion, stirring<br />

salt added<br />

708 Urea herbicides<br />

Indirect analysis of urea herbicides from environmental<br />

water using solid phase microextraction 85µm polyacrylate GC-NPD<br />

in water J. Chromatogr. A. 890 (2000) 303-312 immersed<br />

Berrada, H., Font,G., Molto, J. sat. salt, pH 4<br />

Depletion <strong>SPME</strong> for the evaluation of fiber-sample partition<br />

2162 Pesticides coefficients of pesticides headspace GC-MS<br />

J. Chromatogr. A, 1102, #1-2, 51-59 (2006)<br />

Zimmermann, Thomas; Ensinger, Wolfgang J.; Schmidt, Torsten C.<br />

231 Pesticides<br />

Minimization of Solvent Consumption in Pesticide<br />

Residue Analysis overview<br />

J. Chromatogr. A 754: 43-47 (1996)<br />

Wan, H., Wong, M.<br />

article<br />

838 Chlorinated<br />

Determination of chlorine-containing pesticides in aqueous<br />

media by solid-phase microextraction method<br />

pesticides Zh. Prikl. Khim (2000) 73(11), 1877-1882<br />

in water Stolyarov, B. V.; Boiko, V. V<br />

156 Organochlorine<br />

Online Determination of Organochlorine Pesticides in Water<br />

by <strong>SPME</strong> and GC-ECD 100µm PDMS GC-ECD<br />

pesticides J. High Res. Chromatogr. 19(5): 24756 (1996) 20 min<br />

Ambient temperature, unless otherwise indicated. 186

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