SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Determination of nicotine and other minor alkaloids in international cigarettes by solid-phase microextraction and gas chromatography/mass spectrometry. 1243 Nicotine in cigarettes Analytical Chemistry (2003) 74 (19), 4878-4884. GC-MS Wu, W. J.; Ashley, D. L.; Watson, C. H.* Determination of the volatile constituents of Chinese Coriandrum sativum L. by gas chromatography-mass spectrometry with solid-phase microextraction. 1274 Chromatographia (2003) 57 (5-6), 357-361. 100 um PDMS, 250 C, 3 mGC-MS Deng, C. H.; Song, G. X.; Hu, Y. M.*; Zhang, X. M. 1314 Aroma dilution method using GC injector split ratio for volatile compounds extracted by headspace solid phase microextraction. Food Chemistry (2003) 83 (1), 151-158. Lee, Hyong Joo; Kim, Kyoung Heon; Kim, Tae Hwan; Kim, Young-Suk; Lee, Sang Mi; Oh, Sangsuk GC-O Flavor-protein binding: Disulfide interchange reactions between ovalbumin and volatile disulfides. Disulfide flavors from 1409 proteins Journal of Agricultural and Food Chemistry (2001), 49(9), 4333-4336. Mottram, Donald S.; Adams, Rachel L.; Brown, Helen M.; Parker, Jane K. Analysis of esters in wines 1559 Esters J.Chromatogr. A (2002) 963(1-2), 213-223 Various GC in wine Rodriguez-Bencomo, J.; Conde, J.; Rodriguez-Delgado, M.A.; Garcia-Montelongo, F.; Perez-Trujillo, J.P. Contribution of dimethyl sulfide to the aroma of Syrah and 1560 Dimethyl Grenache Noir wines and estimation of its potential in grapes headspace GC-MS sulfide in of these varieties wine J Agr Food Chem, 52, #23, 7084-7093 Segurel, M.; Razungles, A.; Riou, C; Salles, M; Baumes, R Hydrolysis of glycosidically bound volatiles from apple leaves 1561 Volaitles in (cv. Anna) by Aspergillus niger beta-glucosidase affects headspace GC-MS apple leaves the behavior of codling moth (Cydia pomonella L.) J Agril and Food Chem, 52, #26, 6212-6216 Wei, Shu; Reuveny, Haim; Bravdo, Ben-Ami; Shoseyov, Oded Genetic diversity of volatile components in Xinjiang Wild 2547 Volaitles in Apple (Malus sieversii) Headspace GC-MS apples Journal of Genetics and Genomics 34, #2, 171-179( FEB 2007) Chen, X.; Feng, T.; Zhang, Y.; He, T.; Feng, Jianrong; Zhang, Chunyu Monitoring seasonal variation in apple fruit volatile 1562 Volaitles in emissions in situ using SPME in situ GC apples Phytochemical Analysis, 14, No 4, 232-240 Hern, Alan; Dorn, Silvia Ester variability in apple varieties as determined 1563 Esters in by SPME-GC-MS PDMS fiber GC-MS apples J Agril and Food Chem, 52, #26, 8086-8093 Headspace Young, J. C.; Chu, C. L. G.; Lu, X. W.; Zhu, H. H. Potential of SPME-GC and chemometrics to detect 1564 Volaitles in adulteration of soft fruit purees. Headspace GC-FID stawberry vs J Agr Food Chem, 52, #3, 421-427 GC-MS a puree Reid, L.; Oapostrophe Donnell, C.; Downey, G. Development of headspace SPME-GC method for the 1565 Solvents in determination of solvent residues in edible oils various fibers GC-FID edible oils, and pharmaceuticals headspace GC-ECD pharmaceutics J. Chromatogr. A, 1071, #1-2, 119-124 Michulec, M.; Wardencki, W. Rapid determination of volatile constituents in safflower by microwave 2701 Volatiles in distillation and simultaneous SPME-GC-MS 65µm PDMS/DVB GC/MS safflower oil Annali di Chimica 97, #10, 1075-1084 (OCT 2007) headspace Yu, Yingjia; Yang, Bei; Zhou, T.; Zhang, H.; Shao, Luping; Duan, G. Identification of volatile compounds in structured lipid of Ambient temperature, unless otherwise indicated. 46
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1566 Volatiles in safflower oil using electronic nose and SPME-GC-MS headspace GC-MS safflower oil Agr Chem&Biotechnogy, 46, #4, 152-155 Shin, Jung-Ah; Lee, Jong-Ho; Lee, Ki-Teak Monoterpene and sesquiterpene hydrocarbons of virgin olive oil by . 2708 Terpenes headspace SPME coupled to gas chromatography/mass spectrometry headspace GC/MS in olive oil J. Chromatogr., A 1125, #1, 117-123 (2006-08-25) Vichi, S.; Guadayol, J.; Caixach, J.; Lopez-Tamames, E.; Buxaderas, S. Determination of halogenated solvents content in olive oil by two 2248 Halogenated completely automated headspace techniques coupled to GC-MS headspace GC/MS solvents in Analytica Chimica Acta (2005) 552 #1-2, 60-66 olive oil Arrebola, F. ; Gonzalez-Rodriguez, M.; Garrido Frenich, A.; Marin-Juan, A.; Martinez Vidal, J.; Characterization of olive paste volatiles to predict the sensory quality 2515 Volatiles from of virgin olive oil headspace GC/MS Virgin olive oil European J Lipid Sci Tech 109, #7, 663-672 (JUL 2007) Garcia-Gonzalez, Diego L.; Tena, Noelia; Aparicio, Ramon Effect of the matrix volatile composition in the headspace SPME 2300 Volatiles from analysis of extra virgin olive oil 65µm PDMS/DVB GC/MS Virgin olive oil Food Chemistry 94 #1, 143-150 (2006) headspace Contini, Marina; Esti, Marco Comparative study on volatile analysis of extra virgin 1567 Volatiles in olive oil by dynamic headspace and SPME 100µm PDMS GC-MS-TOF olive oils Food Chemistry, 90, #1-2, 69-79 65µm PDMS-DVB Kanavouras, A.; Kiritsakis, A.; Hernandez, R. J. headspace Application of SPME to virgin olive oil quality control 2738 Volatiles in J Chromatogr A, 1121, #1, 140-144 (2006-07-14) 65µm PDMS/DVB GC/MS olive oils Jimenez, A.; Aguilera, M. P.; Beltran, G.; Uceda, M. headspace 30 min @ 40°C Application of SPME in the analysis of volatile oils 1568 Volatiles in compounds in virgin olive oils. 100µm PDMS GC olive oils J Chromatogr A, 1028, #2, 321-324 15 min @ 45°C Jimenez, A.; Beltran, G.; Aguilera, M. P. headspace Analysis of virgin olive oil volatiles by a novel electronic 1569 Volatiles in nose based on a miniaturized SAW sensor array headspace SAW olive oils coupled with SPME enhanced headspace enrichment GC J AgriFood Chem, 52, #25, 7475-7479 Garcia-Gonzalez, D.; Barie, N; Rapp, M; Aparicio, R A chemical investigation by headspace SPME and 1570 Terpenes GC-MS of volatile and semi-volatile terpenes in headspace GC-MS in olibanum various olibanum samples Phytochemistry (Amsterdam), 66, #12,1499-1514 Hamm, S; Bleton, J; Connan, J; Tchapla, A 2450 Terpenes from Quantifying sesquiterpene and oxygenated terpene emissions from live vegetation using solid-phase microextraction fibers. 65µm PDMS-DVB GC-MS live branches J. Chromatogr., A 1161, #1-2, 113-120 (2007-08-17) headspace Bouvier-Brown, N. C.; Holzinger, R.; Palitzsch, K.; Goldstein, A. H. 10-45 min Simultaneous distillation-extraction of high-value volatile compounds 2522 Volatiles from from Cistus ladanifer L 85µm Polyacrylate GC-FID Rock-rose Anal. Chim. Acta 584, #2, 439-446 (Feb 19 2007) 60 min @ 40°C Alves, Arminda; Mendes, Adelio; Santos, Lucia; Teixeira, Salome headspace 20% NaCl Simultaneous determination of phytohormones in plant extracts 2479 Phytohormones using SPME and HPLC 50µm CW GC, HPLC from plants Chromatographia 66, #7/8, 515-520 (2007) Liu HongTao; Li YanFen; Luan TianGang; Lan ChongYu; Shu WenSheng Volatile profiling of Arabidopsis thaliana - Putative olfactory 2288 Volatiles from compounds in plant communication headspace GC/IMS plants Phytochemistry (Amsterdam) 66 #16, 1941-1955 (2005) Rohloff, Jens; Bones, Atle M. Evaluation of extracts and oils of mosquito (Diptera : Culicidae) 2202 Volatiles from repellent plants from Sweden and Guinea-Bissau headspace GC-MS plants J Medical Entomology 43, #1, 113-119 (2006) Jaenson, Thomas G. T.; Palsson, Katinka; Borg-Karlson, Anna-Karin Ambient temperature, unless otherwise indicated. 47
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