SPME Applications Guide - Overbrook Scientific

Recommendations

Info

(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Changes in the volatile profile of oats induced by processing Conditions headspace Instrument 894 Flavor compounds J. Agric. Food Chem. 49 (5): 2125-2130 (2001) 100µm PDMS GC-MS in oats Robards, Kevin; An, Min; Helliwell, Stuart; Sides, Alasdair SPME for the Analysis of Flavors 30SEC @ 25°c headspace 309 Flavors in Techniques for Analyzing Food Aroma, pp81-112, various fibers food products Food Sci. Technol., New York (1997) Harmon, A. & conditions 388 Volatiles in Analysis of Volatile Fragrance and Flavor Compounds by Headspace SPME Combined with Gas Chromatography/ 100µm PDMS GC-MS consumer products Mass Spectrometry 30 min J. Chem. Educ. 1999, 76(2), 245-248 Galipo, R., Canhoto, A., Walla, M., Morgan, S. headspace 760 Flavor volatiles Solid Phase Microextraction for the enantiometric analysis of Flavors in Beverages 85µm Polyacrylate GC-MS in beverages J. AOAC Intl, Vol. 84, No. 2, 2001, 479-485 60 min., headspace Ebeler, S., Sun, G., Datta, M., Stremple, P., Vicker, A. salt added 2771 Rose oxide Stereoselective formation of the varietal aroma compound rose oxide during alcoholic fermentation headspace GC/MS in white wine J. AOAC Intl, Vol.56, No. 4, 1371-1375 (FEB 27 2008) Koslitz, Stephan; Renaud, Lauren; Kohler, Marcel; Wuest, Matthias Monitoring of the principal carbonyl compounds involved in 2233 Carbonyls malolactic fermentation of wine by SPME and positive ion chemical 65um DVB GC/MS in wine ionization GC/MS analysis (PFBOA) J. Mass Spectrom. 40 #12, 1558-1564 (2005) derivatives Dalla Vedova, A.; Flamini, R.; Ongarato, S.; Panighel, A.Perchiazzi,N.; 5min @ 50C 2904 Carbonyls Analysis of carbonyl compounds via headspace SPME with on-fiber derivatization and GC-ion trap tandem MS determination GC-ITMS biological samples of their O-(2,3,4,5,6-pentafluorobenzyl)oxime derivatives PFBHA and foodstuffs, Anal. Chim. Acta 617, #1-2, 119-131 (Jun 9 2008) Bokuz, U.; Fischer, Ulrich; Ganss, S.; Kopp, B.; Potouridis, T.; derivatives 891 Volatile carbonyls Comparison of extraction techniques for GC determination of volatile carbonyl compounds in alcohols. GC-ECD in alcohols Fresenius' J.Anal Chem. (2001) 369(7-8) 661-665 Wardencki, W; Namiesnik, J; Orlita, J. PFBHA derivatives 903 Carbonyls Determination of carbonyl compounds in water by derivatization SPME and GC analysis GC in water J. Chromatography A 1998, 809, 1-2, 75-87 Bao,M., Pantani,F.,Griffini,O.,Burrini,D.,Santianni, D., Barbieri, K. Development of a dynamic headspace SPME procedure coupled to 2817 Organic content GC-qMSD for evaluation the chemical profile in alcoholic beverages various fibers GC-qMSD in alcoholic Analytica Chimica Acta 609, #1, 82-104 (FEB 18 2008) headspace beverage Rodrigues, F.; Caldeira, M.; Camara, J. S. Research on alcoholic beverages at Alko's control Lab 454 Organic content Kem.-Kemi, 1999, 26(2), 95-97 GC-MS in alcoholic Lehtonen, P. beverage Finnish Analysis of free fatty acids, higher alcohols and 455 Alcohols, esters, free esters in sake by headspace-SPME fatty acids Nippon Jozo Kyokaishi (1999), 94(3), 252-257 in Sake Utsunomiya, H. Japanese Solid-phase microextraction for the GC-MS determination of Ambient temperature, unless otherwise indicated. 14
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2867 Oxazole fungicide oxazole fungicides in malt beverages 100µm PDMS GC-MS(SIM) in malt beverages Anal. Bioanal. Chem. 391, #3, 1425-1431 (2008) 70µm CW-DVB Aguinaga, N.; Campillo, N.; Hernandez-Cordoba, M.; immersion Martinez-Castillo, N.;Vinas, Pilar 60°C, 30 min 312 Flavor volatiles in Headspace Gas Chromatography Profiles of Fruit-Flavored Malt Beverages, Using SPME 100µm PDMS GD-FID malt beverages J. Am. Soc. Brew. Chem. 55 (3): 112-118 (1997) 45°C, 45-60 min Constant, M., Collier, J. headspace 2906 Flavor volatiles in Optimisation of a complete method for the analysis of volatiles involved in the flavour stability of beer by SPME-GC-MS headspace GC-MS beer wort J. CHROMATOGR. A 1190, #1-2, 342-349 (May 9 2008) De Schutter, D.; Delvaux, F.; Delvaux, F.; Saison, D. PFBHA derivative 2422 Flavor volatiles in Optimisation of wort volatile analysis by headspace SPME in combination with gas chromatography and mass spectrometry headspace GC-MS beer wort J. CHROMATOGR. A 1179, #2, 75-80 (01 FEB 2008) De, Schutter D. P.; Saison, D.; Delvaux, F.; Derdelinckx, G.; Rock, J.; . Neven, H.; Delvaux, F. 313 Alcohols, esters Solid Phase Microextraction for the Analysis of Some Alcohols and Esters in Beer: Comparison with Static 85µm polyacrylate GC-FID in beer Headspace Method 50°C, 30 min J. Agric. Food Chem. 46 (4): 1469-1473 (1998) headspace Wasowicz, E., Kaminski, E., Jelen, H., Wlazly, K. salt added 2818 Dimethyl sulfide Laboratory inter-comparison of dissolved dimethyl sulphide (DMS) measurements using purge-and-trap and SPME GC-MS in water techniques during a mesocosm experiment Marine Chemistry 108, #1-2, 32-39 (JAN 1 2008) Vogt, M.; Turner, S.; Yassaa, N.; Steinke, M.; Williams, J.; Liss, P. headspace Headspace SPME for the analysis of dimethyl 456 Dimethyl sulfide sulfide from beer 65µm Carboxen/PDMS GC-FPD in beer J. Agric. Food Chem. 1999, 47(7), 2505-2508 15 min @ 30°C Scarlata, C. Ebeler, S. headspace 1.5gm NaCl Characterization of whiskIes using SPME with GC-MS 612 Volatiles in J.Chromatogr. A (2000) 896, 351-359 85µm polyacrylate GC-MS whiskies Fitzgerald, G., James, K., MacNamara, K., Stack, M. 35 min headspace Changes in volatile compounds of palm sap (Arenga pinnata) 2368 Volatiles in during the heating process for production of palm sugar headspace GC-MS palm sap Food Chemistry 102, # 4, 1156-1162 (2007) Ho, C. W.; Aida, W. M. Wan; Maskat, M. Y.; Osman, H. A headspace SPME method for the determination of some 953 Volatiles in secondary compounds of Brazilian sugar cane spirits by GC 85µm polyacrylate GC-FID sugar cane spirits J Agric Food Chem, 2001, 49, 3533-3539 25 min @ 60°C Nonato, E., Carazza, F., Silva, C. Carvalho, C., Cardeal, Z headspace 2.5g NaCl Determination of volatile fatty acid ethyl esters in raw spirits using 2765 Fatty acid ethyl SPME and GC headspace GC-FID esters in spirits Anal. Chim. Acta 613, #1, 64-73 (Apri 14 2008) Plutowska, Beata; Wardencki, Waldemar Characterization of rum using solid-phase microextraction with GC-MS 2732 Aroma volatiles Food Chemistry 104, # 1, 421-428 (2007) 100µm PDMS GC-MS in rum Pino, J. A 35 min @ 35°C headspace Comparison of two extraction methods for evaluation of volatile 2502 Aroma volatiles constituents patterns in commercial whiskeys. Elucidation of the 75µm Carboxen GC-MS in whiskeys main odour-active compounds Talanta 74, #1, 78-90 ( Nov 15 2007) Caldeira, M.; Camara, J.S.; Marques, J.C.; Perestrelo, R.; Rodrigues, F. headspace Ambient temperature, unless otherwise indicated. 15
Page 1 and 2: SPME Applications Guide The SPME Ap
Page 3 and 4: (New references added to the 7th ed
Page 13: (New references added to the 7th ed
Page 35 and 36: 1232 (New references added to the 7
Page 43 and 44: 1496 1499 1500 (New references adde
Page 65 and 66:
(New references added to the 7th ed
Page 67 and 68:
Page 69 and 70:
Page 71 and 72:
Page 73 and 74:
Page 75 and 76:
Page 77 and 78:
Page 79 and 80:
Page 81 and 82:
Page 83 and 84:
Page 85 and 86:
Page 87 and 88:
Page 89 and 90:
Page 91 and 92:
Page 93 and 94:
Page 95 and 96:
Page 97 and 98:
Page 99 and 100:
Page 101 and 102:
1485 1487 1503 1506 (New references
Page 103 and 104:
Page 105 and 106:
Page 107 and 108:
Page 109 and 110:
Page 111 and 112:
Page 113 and 114:
Page 115 and 116:
Page 117 and 118:
Page 119 and 120:
Page 121 and 122:
Page 123 and 124:
Page 125 and 126:
Page 127 and 128:
1381 (New references added to the 7
Page 129 and 130:
Page 131 and 132:
Page 133 and 134:
Page 135 and 136:
Page 137 and 138:
Page 139 and 140:
Page 141 and 142:
Page 143 and 144:
Page 145 and 146:
Page 147 and 148:
Page 149 and 150:
Page 151 and 152:
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Page 161 and 162:
Page 163 and 164:
Page 165 and 166:
Page 167 and 168:
Page 169 and 170:
Page 171 and 172:
Page 173 and 174:
Page 175 and 176:
Page 177 and 178:
Page 179 and 180:
Page 181 and 182:
Page 183 and 184:
Page 185 and 186:
Page 187 and 188:
Page 189 and 190:
Page 191 and 192:
Page 193 and 194:
1522 1531 1554 1551 (New references
Page 195 and 196:
Page 197 and 198:
Page 199 and 200:
Page 201 and 202:
Page 203 and 204:
Page 205 and 206:
Page 207 and 208:
Page 209 and 210:
Page 211 and 212:
Page 213 and 214:
Page 215 and 216:
Page 217 and 218:
Page 219 and 220:
Page 221 and 222:
Page 223 and 224:
Page 225 and 226:
Page 227 and 228:
Page 229 and 230:
Page 231 and 232:
SPME Literature Literature No. Titl
Page 233:
World Headquarters 3050 Spruce St.,
show all

SPME Applications Guide - Overbrook Scientific

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?