SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />
Analyte / Extraction<br />
Matrix Literature Reference Conditions Instrument<br />
475 Nereistoxin in<br />
Simple and Sensitive Analysis of Nereistoxin and its<br />
Metabolites in Human Serum using Headspace 65µm DVB/PDMS GC-MS<br />
human serum <strong>SPME</strong>-GC-MS 30 min @ 70°C<br />
J. Chromatographic Science 37(3):77-82(1999) NaCl added,<br />
Namera,A., Watabe,T., Yashiki,Y., Kojima,T., Urabe,T. headspace<br />
419 Lidocaine<br />
Direct <strong>SPME</strong> Combined with Gas and Liquid Chromatography<br />
for the Determination of Lidocaine in Human Urine GC, HPLC<br />
in urine Chromatographia (1998), 47(11/12), 678-684<br />
Koster, E., Hofman, N., DeJong, G .<br />
646 Lidocaine<br />
Determination of lidocaine in plasma by direct <strong>SPME</strong><br />
combined with GC 65µm PDMS/DVB GC<br />
in plasma J. Chromatogr., B. Biomed Sci. Appl (2000), 739(1), 175-182 10 min<br />
Koster, E., Wemes, C., Morsink, J., deJong, G.<br />
Evaluation of <strong>SPME</strong> in combination with GC as a tool<br />
immersed<br />
salt added<br />
647 Lidocaine for quantitative bioanalysis Carbowax-DVB GC-NPD<br />
in plasma J. Microcolumn Sep. 2000, 12(5), 308-315<br />
Abdel-Rehim, M., Bielenstein, M, Arvidsson, T. pH 9<br />
420 Organochlorine<br />
Determination of Persistent Organochlorine Compounds in<br />
Blood by <strong>SPME</strong> Extraction and GC-ECD GC-ECD<br />
compounds Fresenius' J. Anal. Chem. (1998), 361(2), 192-196<br />
in blood Roehrig, L., Puettmann, M., Meisch, H.<br />
141 Chloroethers<br />
Determination of Chloroethenes in Environmental Biological<br />
Samples Using GC Coupled with <strong>SPME</strong><br />
in biological samples Chromatographia 42(5/6): 313-17 (1996)<br />
Xu, N., Vandegrift, S., Sewe, G.<br />
67 Solvent thinners<br />
Simple Analysis of 5 Thinner Components in Human-Body<br />
Fluids by Headspace <strong>SPME</strong> 100µm PDMS GC-FID<br />
in urine, blood J. Legal Medicine 107: 310-313 (1995)<br />
Lee, X., Kumazawa, T., Sato, K.<br />
Improved extraction of thinner components from human<br />
80°C, 5 min<br />
headspace<br />
877 Solvent thinners body fluids by headspace <strong>SPME</strong> with a Carboxen/PDMS 65µm Carboxen/PDMS<br />
in urine, blood coated fiber<br />
Leg. Med. 1(1999) 231-237<br />
Lee, X., Kumazawa, T., Kondo, K., Furuta, S., Sato, K.<br />
648 Volatile organics<br />
Determination of volatile organic compounds in blood<br />
by headspace <strong>SPME</strong>-GC 100µm PDMS GC-FID<br />
in blood Weosjemg Uamkoi 2000, 29(1), 37-39<br />
Hao, S., Kang, J., Zhou, S, Cui, J., Qi, Q., Han, K.<br />
10 min<br />
649 Volatile organics<br />
The use of <strong>SPME</strong> in conjunction with benchtop quadropole MS<br />
for the analysis of volatile organic compounds in human 100µm PDMS GC-MS<br />
in blood blood at low ppt. Levels<br />
J. Chromatogr. Sci. (2000), 38(2), 49-54<br />
Cardinali, F., Ashley, D., Wooten, J., McCraw, J., Lemire, S.<br />
10 min, headspace<br />
795 Benzene<br />
Urinary benzene as a biomarker of exposure among<br />
occupationally exposed and unexposed subjects. GC-MS<br />
in urine Carcinogenesis (Oxford) (2001) 22(2), 279-286<br />
Rappaport, S; Bechtold, W; Dosemeci, M; Fustinoni, S<br />
Guilan, Li; Hayes, R<br />
2386 Organochlorine<br />
Determination of organochlorine pesticides and PCBs in human<br />
serum using headspace <strong>SPME</strong>-GC-ECD 100µm PDMS GC-ECD<br />
pesticides, PCBs J. Chromatogr., B: 846, #1, 298-305 (2007-02-01) 50min @ 85°C<br />
in human serum Lopez, R.; Goni, F.; Etxandia, A.; Millan, E. headspace<br />
Ambient temperature, unless otherwise indicated. 111
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