SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument antidepressants J. Anal. Toxicol. 31, #6, 313-320 (Jul-Aug 2007) in plasma Silva, B. J. G.; Queiroz, R. H. C.; Queiroz, M. E. C. 2507 Tricyclic Analysis of tricyclic antidepressant drugs in plasma by means of SPME-liquid chromatography-mass spectrometry 65µm PDMS/DVB LC-MS antidepressants J Mass Spectrometry 42, #10, 1342-1347 (OCT 2007) 30min @ 30°C in plasma Alves, C.; Santos-Neto, A.; Fernandes, C.; Rodrigues, J.; Lancas, F. direct extraction 64 Tricyclic Simple Extraction of Tricyclic Antidepressants in Human Urine by Headspace SPME 100µm PDMS GC-FID antidepressants Jpn. J. Forensic Toxicol. 13 (1): 25-30 (1995) 100°C, 15 min in urine Kumazawa, T., Lee, X., Tsai, M., Seno, H., Ishii, A., Sato, K. Detection of Tricyclic Antidepressants in Whole Blood by headspace stirring 95 Tricyclic Headspace SPME-Capillary GC 100µm PDMS GC-FID antidepressants J. Chrom. Sci. 35: 302-308 (1997) 100°C, 60 min in blood Lee, X., Kumazawa, T., Sato, K. Analysis of Tricyclic Antidepressant and that application headspace NaOH added 488 Tricyclic for fatal intoxication by Headspace SPME 100µm PDMS GC-MS antidepressants Jpn. J. Legal. Med. 52:69(1998) 45 min @ 120°C in urine, blood Watanabe,T., Namera,A., Yashiki,M., Iwasaki,Y., Kojima,T. headspace, NaOH 352 Tetracyclic Simple Analysis of Tetracyclic Antidepressants in Blood Using Headspace SPME and GC-MS 100µm PDMS GC-MS antidepressants J. Anal. Toxicology, Vol. 22 (5), 1998, 396-400 120°C, 45 min in blood Namera, A., Watanabe, T., Yahiki, M., Iwasaki, Y., Kojima, T. Direct coupling of microcolumn liquid chromatography headspace NaOH added 655 Antidepressant with in-tube SPME for the analysis of antidepressant drugs In-tube HPLC in urine Analyst (Cambridge UK) 2000, 125(5), 807-809 Saito, Y., Kawazoe, M, Jinno, K., Nayhashida, M. 227 Diazepam Solvent-Modified Solid-Phase Microextraction for the Determination of Diazepam in Human Plasma Samples 85µm polyacrylate GC-FID or FPD in serum by Capillary Gas Chromatography 4 min J. Chromatogr. B 689: 357-364 (1997) immersion Krough, M., Grefslie, H., Rasmussen, K. pH 5.5 1-octanol added 656 Amitriptyline SPME coupled with microcolumn LC for the analysis of amitriptyline in human urine HPLC in human urine Chromatographia, (2000 Sept.) 52(5-6) 309-313 Jinno, K., Kawazoe, M., Hayashida, M. 371 Benzophenone-3 Determination Benzophenone-3 and Metabolites in Water and Human Urine by SPME and Quadrupole Ion Trap GC-MS 65µm Carbowax/DVB GC-MS in water and urine Anal. Chimica Acta 371 (1998) 195-203 45 min Felix, T., Hall, B., Brodbelt, J. immersion 871 Benzoylecgonine Aqueous phase hexylchloroformate derivatization and SPME Determination of benzoylecgonine in urine by GC 100µm PDMS GC-MS in urine quadrupole ion trap mass spectrometry. J Forensic Sci (1999) 44(3) 527-534 Brodbelt, Jennifer S.; Hall, Brad J.; Parikh, Aashish R. Solid Phase Microextraction with Capillary GLC and NDPD for hexyl chloroformate derivative 168 Antidepressants the Assay of Antidepressant Drugs in Human Plasma 100µm PDMS GC-NDPD in blood J. Chromatogr. B 696: 217-234 (1997) 60 min Ulrich, S., Martens, J. immersion 657 Phenothiazines Determination of Phenothiazines in human body fluids by SPME and LC-tandem mass spectrometry 85µm Polyacrylate LC-MS urine, blood J.Mass Spec. (2000-9) 35(9) 1091-1099 60 min @ 40°C Seno, H., Kumazawa, T., Ishii, A., Hattori, H., pH 8 Ambient temperature, unless otherwise indicated. 118
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Nishikawa, M., Watanabe, K., Suzuki, O. stirring 142 Phenothiazines Detection of Some Phenothiazines by Headspace SPME and GC 100µm PDMS GC-FID urine, blood Jpn. J. Forensic Toxicol. 14: 30 (1996) 40 min @ 140°C Kumazawa, T., Seno, H.,, Ishii, A., Hattori, H., Sato, K., headspace Watanabe, K., Suzuki, O. NaCl added 947 Propranolol In-Tube Molecularly Imprinted Polymer SPME for the selective Determination of Propranolol Anal. Chem (2001) 73(11) 2383-2389 Mullett, Wayne M.; Martin, Paul; Pawliszyn, Janusz Quantification of plasma and urinary levels of furan in healthy individuals 2480 Furan FASEB Journal. 21, #6, A1066 (APR 2007) GC-MS in plasma, urine Jun, Hee-Jin; Chung, Mi Ja; Park, Young-Sik; Lee, Kwang-Geun; Lee, S. Application of (SPME) technique for the detection of 946 Carbofuran carbofuran in serum in seum J. Can. Soc. Forensic Sci(2001) 34(1), 23-26 Ameno, K.; Lee, S-K.; Ameno, S.; Kinoshita, H.; Kubota, T.; Zhang, X.; Ijiri, 908 Dinitroaniline Headspace SPME and GC determination of dinitroaniline herbiciede s in human blood, urine and environmental water 100µm PDMS GC-ECD in blood, urine J. Chromatogr. B. (1998), 714(2), 205-213 30 min @ 70°C and water Guan, F., Watanabe, K., Ishii, A., Seno, H., Kumazawa, T., headspace Hattori, H., Suzuki, O. NaSO4 2809 Pesticides Reliable identification of pesticides using linear retention indices as an active tool in GC-MS analysis J. Chromatogr. A.1186 (1-2), 430-433 (Apr 4 2008) Casilli, A.; Dugo, G.; Dugo, Paola; Mondello, L.; Salvatore, Angelo; Tranchida, Peter Quinto GC-MS 2636 Pesticides in Evaluation of the pesticide contamination of groundwater sampledl over two years from a vulnerable zone in Portuga GC-ECD ground water J Agri Food Chem 55, #15, 6227-6235 (2007) Goncalves, C. M.; Silva, J. C. G. E. da; Alpendurada, M. F GC-MS 2412 Phenylurea and Analysis of phenylurea and propanil herbicides by SPME-LC combined with post-column photochemically induced 60µm PDMS/DVB HPLC-PIF-FD propanil herbicides fluorimetry derivatization and fluorescence detection fluorimetry in ground water Anal. Chim. Acta 593, #2, 157-163 (2007-06-19) Mughari, A. R.; Parrilla Vazquez, P. ; Martinez Galera, M. derivatization 183 Herbicides SPME and GC-ECD Determination of Dinitroaniline Herbicides in Surface Water and Biological Fluids 100µm PDMS GC-ECD in water and Jpn. J. Forensic Toxicol. 15 (2): 151-153 (1997) 30 min @ 70°C water biological fluids Prosen, F., Watanabe, K., Ishii, A., Seno, H., Suzuki, O. Gas chromatographic determination of organochlorine and @ 90°C blood Na2SO4, headspace 860 Organochlorine & organophosphorus pesticides in human fluids using SPME GC/ECD/FPD organophosphorus Analytica Chimica Acta (2001) 433(2) 217-226 pesticides in biological fluids Hernandez, F.; Beltran, J.; Egea, S.; Lopez, F. J.; Pitarch, E. Detection of Organophosphate Pesticides in Human Body 66 Organophosphate Fluids by Headspace SPME and Capillary GC with 100µm PDMS GC-NPD pesticides Nitrogen-Phosphorus Detection 100°C, 20 min in urine, blood Chromatogrphia 42(3/4): 135-140 (1996) Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O. pH 3 with HCl 875 Organophosphorus Optimisation of SPME conditions for headspace analysis of organophophorus pesticides in whole blood pesticides in Z Zagadnien Nauk Sadowych, 42(2000) 47-59 whole blood Asri, K., Anderson, R. Ambient temperature, unless otherwise indicated. 119
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