SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Tacoma controls tastes and odours with ozone Conditions Instrument 2375 Odor compounds Water Science and Technology 55, # 5, 137-144 ( 2007) in water Carlson, M.; Chen, T.; McMeen, C.; Suffet, I. H.; Zhang, M 511 34 Odor compounds Headspace SPME for the determination of trace levels of taste and odor compounds in water samples 65µm DVB/PDMS GC-Ion trap in water Analyst (Cambridge, UK) 1999, 123(4), 459-466 40 min @ 20°C MS Bao, M., Mascini, M., Griffini, O., Burrini, D., Santianni, D., NaCl, stirring Barbieri, K. immersion/headspace 282 Chemical warfare On-Site Sample Work-Up Procedures to Isolate Chemical Warfare-Related Compounds, Using SPE & SPME Technology compounds Analytical Chemistry Associated with the Destruction of Chemical Weapons NATO ASI Ser., Ser. 1 13: 65-76 (1997) Alcaraz, A., Hulsey, S., Whipple, R., Andresen, B. 2349 Nerve agents Synthetic methods applied to the detection of chemical warfare nerve agents CURR. ORG. CHEM. 11, #3, 255-265 Giordano, B. C.; Collins, G. E Review article 116 Nerve agents Determination of Chemical Warfare Agents in Natural Water Samples by SPME 65µm PDMS/DVB GC-FID in water Anal. Chem. 69: 1866-1872 (1997) 30 min GC-MS Lakso, H., Ng, W. headspace saturated salt 762 Lewisite oxide Determination of Lewisite oxide in soil using SPME followed by GC w/FPD or Mass spectormetric detection 100µm PDMS GC-FPD/or in soil J. Chromatogr-A, 909 (2001) 13-28 20min. GC-MS Tomkin, B., Sega, G., Ho, C. agitated 1,3-propanedithiol derv. 560 Chemical warfare In-situ derivatisation of degradation products of chemical warfare agents in water by SPME and GC-MS analysis 65µm Carboxen/PDMS GC-MS agents in water J. Chromatogr-A, Feb 1999, 832(1+2), 173-182 20°C, Sng, M., Ng., W. Rapid Determination of Volatile Organic Compounds in N-methyl-N-(tert-butyl dimethylsilyl) trifluoroacetamide derivative 283 Volatiles Environmentally Hazardous Wastewaters, Using SPME in wastewater Anal. Chem. 358 (7-8): 833-837 (1997) James, K., Stack, M. 284 TNT, DNT salt Trace salt Signatures from World War II Unexploded Undersea Ordinance 65µm PDMS/DVB directly in seawater/ Environ. Sci. Technol. 32 (9): 1354-1358 (1998) 15 min into MS sediment Darrach, M., Chutjian, A., Plett, G. pH 8 agitation 285 Aromatic amines Determination of Aromatic Amines by SPME-GC-MS in Water Samples 65µm Carbowax/DVB GC-MS in water J. Chromatogr. A 791(1+2): 221-230 (1997) 30 min Muller, L., Fattore, E., Benfenati, E. SPME coupled with HPLC for the determination of stirring pH 7.6, salt added 65µm PDMS/DVB, CW- 578 Aromatic amines aromatic amines. TPR HPLC-UV in water Anal-Chem. 15 Jan 1999; 71(2): 310-318 Wu,-Y-C; Huang,-S-D 280nm 286 Volatiles Inter-Laboratory Studies for the Validation of SPME for the Quantitative Analysis of Volatile Organic Compounds 100µm PDMS GC-ECD in water Compounds in Aqueous Samples 30 min Anal. Chim. Acta 356 (2-3): 113-123 (1997) headspace & Nilsson, T., Ferrari, R., Facchetti, S. immersion Ambient temperature, unless otherwise indicated. 156
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Solid-phase micro-extraction of volatiles from water Conditions stirring Instrument 597 Volatiles (BTEX) using open cap vials 100µm PDMS GC-FID in water Chromatographia. May 1999; 49(9-10): 513-519 5 min. @ 25C Matisova,-E; Sedlakova,-J; Simon,-P; Welsch,-T stirred 287 VOCs, pesticides Capabilities for the Direct Determination of Triphenyland Triethylarsine in Water by SPME Followed by GC-A Carboxen/PDMS, GC-MS in water and air Amer. Environ. Lab, 9 (10): cover, 5-6 (1997) 100µm PDMS Mothes, S., Wennrich. R. various conditions 374 Organoarsenicals Determination of Organoarsenicals in the Environment by SPME-GC-MS 100µm PDMS GC-MS in water and soil J. Chromatogr. A 807 (1998) 253-263 10 min Szostek, B., Aldstadt, J. immersion methyl thioglycolate (derivative) 879 Organoarsenicals SPME method for GC w/MS and pulsed Flame photometric detection: studies of organoarsenical speciation 100µm PDMS GC-MS in water J. Chromatogr. A 918(2001) 169-175 10 min GC- PFPD Killelea, D., Aldstadt, J. immersion methyl thioglycolate (derivative) Speciation of organoarsenic compounds by poly(pyrrole)- 790 Organoarsenicals coated capillary in-tube SPME coupled with HPLC-EI-MS Polypyrrol capillary LC-EI-MS in water Analytica Chimica Acta (2000) 424(2), 211-222 Wu, J. C.; Mester, Z.; Pawliszyn, J. 815 Metal hydrides Sampling and determination of metal hydrides by SPME thermal desorption inductively coupled plasma MS Carboxen/PDMS, ICP-MS in water J. Analytical Atomic Spectrometry (2000) 15(11) 1461-1465 Mester, Z.; Sturgeon, R. E.; Lam, J. W Sodium Borohydride/HCl 2894 Disinfection Emerging technologies for identification of disinfection byproducts: GC/FT-ICR MS characterization of solvent artifacts GC/FT-ICR MS byproducts Environ Sci& Tech 41, #15, 5419-5425 (AUG 1 2007) in water Heffner, C.; Silwal, I.; Peckenham, J..; Solouki, T. 288 Iodinated volatiles SPME with Temperature-Programmed Desorption for the Analysis of Iodinated Disinfection Byproducts 85µm polyacrylate GC-ECD in water Anal. Chem. 70 (3): 638-644 (1998) 15 min Frazey, P., Barkley, R., Siever, R. immersion stirring 289 Chloroethers Determination of Chloroethers in Aqueous Samples, Using SPME GC-FID or MS in water Acta Hydrochim. Hydrobio. 25 (6): 329-334 (1997) Wennrich, L., Engewald, W., Popp, P. 513 Chloroethers GC trace analysis of haloethers in water: Comparison of different extraction techniques GC-FID or MS in water Int. J. Environ.Anal. Chem (1999), 73(1), 31-41 Wennrich, L., Engewald, W., Popp, P. 514 Aliphatic aldehydes Influence of extraction parameters and medium on efficiency of SPME sampling in analysis of aliphatic aldehydes 100µm PDMS GC-MSD in water/oil J. Chromatogr., A 1999, 845(1+2), 337-347 30 min @ 40°C Keszler, A., heberger, K. immersed/headspace 515 Glycerol ethers Improved extraction of glycerol ethers from water by SPME by Carboxen-PDMS coated fiber 75µm Carboxen/PDMS GC-FID in water Chromatogrophia, 1999, 50 (3/4), 155-159 25°C, sat. NaCl Ambient temperature, unless otherwise indicated. 157
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