SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
in serum Anal. Chim. Acta, 538, #1-2, 49-56
Chou, Chi-Chi; Lee, Maw-Rong
Comparison and classification of methamphetamine seized in Japan
2800 Methyl and Thailand using GC with liquid-liquid extraction and SPME GC-FID
amphetamine Forensic Science International 175, #2-3, 85-92 (MAR 5 2008)
Kuwayama, K.; Inoue, H.; Phorachata, J.; Kongpatnitiroj, K.;
Puthaviriyakorn, V.; Tsujikawa, K.; Miyaguchi, H.; Kanamori, T.;
Iwata, Yuko T.;Kamo, Naoki; Kishi, Tohru
Excretion of unchanged volatile organic compounds (toluene,
2836 Volatile organics ethylbenzene, xylene and mesitylene) in urine as result of headspace GC
in human urine experimental human volunteer exposure
Intl Archives of Occupational Environ. Health 81, #4, 443-449 (2008)
Janasik, Beata; Jakubowski, Marek; Jalowiecki, Piotr
Quantitative analysis of benzene, toluene,
1835 BTX solvents and xylenes in urine by headspace SPME headspace GC-MS
in urine J Chromatogr A, 1027, #1-2, 37-40
Alkalde, T; Peralba, M; Zini, C; Caramao, E.
SPME w/ on-fiber derivatization for the determination of
1836 PCB metabolite hydroxy-polychlorinated biphenyl compounds in urine 65µm PDMS-DVB GC/MS
in urine Anal. Chim. Acta, 539, #1-2 55-60 60min @ 90°C
Hong, Jee Eun; Lee, Won; Park, Song-Ja; Pyo, Heesoo BSTFA derivative
headspace
Single drop microextraction or SPME-GC-MS
1837 Iodine in for the determination of iodine in pharmaceuticals, iodate derivatives GC
various iodized salt, mil powder and vegetables
matrices involving conversion into 4-iodo-N,N-dimethylaniline
J Chromatogr A, 1023, #1, 33-39
Das, P; Gupta, M; Jain, A; Verma, K.
Determination of quinalphos in blood and urine by direct SPME
2315 Quinalphos in combined with GC-MS 100µm PDMS GC/MS
blood J. Chromatogr. B 832 #1, 162-168 (2006) direct
Barroso, M.; Cruz, A.; Gallardo, E.; Lopez-Rivadulla, M.;
Margalho, C.; Vieira, D.N
Investigations on the medico-legal relevance of spirits containing
2290 Thujone thujone with special regard to toxicological-analytical aspects headspace GC/MS
in blood Blutalkohol 42 #4, 263-271 (2005) (German)
Kroner, L.; Padosch, S.; Lachenmeier, D.; Madea, B.
Monitoring of drugs and metabolites in whole blood
1838 Diazipenes in by restricted-access SPME coupled to LC-MS restricted access LC-MS
biological fluid J Chromatogr A, 1025, #1, 85-92 coated fibers
Walles, M.; Mullett, W. M.; Pawliszyn, J. headspace
An accurate and sensitive method for determination
1839 Methyl methylmercury in biological specimens 100µm PDMS ICP-MS
mercury from using GC-ICP-MS with solid phase microextraction methyl, ethyl, phenyl
biological J Anal At Spectrom, 19, #12, 1546-1551 derivatives
specimens Christopher, S.J.; Davis, W. Clay; Day, Rusty D.; microwave extraction
Long, S.E.; Schantz, Michele M.; Vander Pol, Stacy S.
Sampling and analysis of volatile organic compounds
1840 Volatiles in in bovine breath by SPME-GC-MS 50/30µm DVB/CAR GC-MS
bovine breath J Chromatogr A, 1025, #1, 63-69 15min @ 22°C
Spinhirne, J.; Koziel, J.; Chirase, N. headspace
High-throughput analysis of phthalate esters in
1841 Phlated esters human serum by direct immersion SPME followed 85µm polyacrylate GC-MS
in serum by isotope dilution-fast GC/MS direct immersion
Anal. Bioanal. Chem., 380,#2, 275-283
Colon, Ivelisse; Dimandja, Jean-Marie D.
Development of pressurized hot water extraction
1842 Ligustilides followed by headspace SPME-GC-MS determination headspace GC-MS
in Chinese ligustilides in Ligusticum chuanxiong and Angelica sinensis
medicines J. Sep. Sci., 28, #11, 1237-1243
Deng, Chunhui; Ji, Jie; Wang, Xiaochuan; Zhang, X
1843 Benzene
Urinary benzene determination by SPME/GC-MS:
A study of variables by fractional factoria 1 min @ 15°C GC-MS
from urine design and response surface methodology headspace
Ambient temperature, unless otherwise indicated. 103