SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 412 Solventless Analytical Separation Method -- SPME/Microcolumn LC Chromatography (1998), 19(2), 6063 Jinno, K. HPLC 261 Fatty acid Derivatization/SPME: New Approach to Polar Analytes Anal. Chem. 69(2): 196-205 (1997) 85µm polyacrylate GC-FID methyl esters Pan, L., Pawliszyn, J. 2 hr in air and water headspace, pH 6 derivative: 1-pyrenyldiazomethane 819 Formaldehyde Solid phase analytical derivatization: enhancement of sensitivity and selctivity of analysis J.Chromatogr. A., 843, 19-27 Rosenfeld, J. On-fiber derivatization 553 9 references New Gas chromatographic approach to polar compounds by derivatization-SPME Bunseki, 1999 (7), 595-597 Takauchi, M. Japanese 262 Alcohol and ketones Strategies for the Analysis of Polar Solvents in Liquid Matrixes Anal. Chem. 70 (1): 19-27 (1998) Nafion fiber GC-ECD in water Gorecki, T., Martos, P., Pawliszyn, J. 10 min headspace, stirring 738 Phenanthrene, PCB Absorption of hydrophobic compounds into the poly(dimethylsiloxane) coating of SPME fibers: high 7µm PDMS GC-MS pentachlorobenzene partition coefficients and fluorescence 10min in water microscopy images Anal. Chem. (2000) 72(3), 459-464 Mayer, P., Vaes,W., Hermens, J. 739 Hydrophobic Nonequilibrium SPME for determination of the freely dissolved concentration of hydrophobic organic 7µm PDMS GC-ECD compounds (PCBs) compounds: matrix effects and limitations 0.5-60min @ 37°C in water Anal. Chem 2000, 72(13), 2802-2808 Oomen, A., Mayer, P., Tolls, J. 263 nC8 to nC14, Methodological Aspects of Headspace SPME. Application J. High Resolut. Chromatogr. 20 (4): 217-221 (1997) various fibers GC-FID neat Schafer, B. Hennig, P., Engewald, W. Headspace SPME. Dynamics and Quantitative Analysis Before 80°C, 5 min headspace 264 Phenol, alcohols Reaching a Partition Equilibrium 85µm polyacrylate GC-MS in water Anal. Chem. 69 (16): 3260-3266 (1997) 1-80 min at 25°C, Ali, J. 1-40 min at 80°C headspace, stirring 413 Tetraethyllead SPME as a Sample Introduction Technique for Radio Frequency Glow Discharge MS 30µm PDMS radio frequency in water Anal. Commun. (1997), 34(10), 275-277 5 min glow discharge Gorecki, T., Belkin, M., Caruso, J., Pawliszyn, J. headspace, stirred MS Effect of Sample Volume on Quantitative Analysis by SPME, 265 Part 1 - Theoretical Considerations Analyst (Cambridge) 122 (10): 1079-1086 (1997) Gorecki, T., Pawliszyn, J. Steady-state diffusion regime in solid-phase microextraction kinetics 2835 Theory Anal Chim Acta 609, #1, 113-119 (Feb 18 2008) ter Laak, Thomas L.; van Leeuwen, Herman P.; Benhabib, Karim Ambient temperature, unless otherwise indicated. 220
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Kinetics of SPE and SPME in thin adsorbent layer with Conditions Instrument 740 Theory saturated sorption isotherm J.Chromatogr. A (2000) 873(1), 39-51 Emenov, S, Koziel, J., Pawliszyn, J. 769 BTEX The use of polymeric fullerenes as a new coating for SPME Chromatographia (2000) 52(11/12), 803-809 GC-FID from water Xiao, C.; Liu, Z. ; Wang, Z.; Wu, C.; Han, H. headspace 266 Organics SPME as a Tool to Determine Membrane/Water Partition Coefficients and Bioavailable Concentrations in vitro 85µm polyacrylate GC-FID in water Systems 9-17 min Chem. Res. Toxicol. 10 (10): 1067-1072 (1997) Vae, W., et al. immersion, stirring 267 PAHs, phenols, Sol-Gel Coating Technology for the Preparation of SPME Fibers of Enhanced Thermal Stability Solgel coating GC-FID anilines Anal. Chem. 69 (19): 3889-3898 (1997) 30 min in water Chong, S. et al. stirring A review on SPME- HPLC as a novel tool for the analysis of 2231 Metallic species toxic metal ions review article HPLC Talanta 68 #3, 842-849 (2006) Kaur, Varinder; Malik, Ashok Kumar; Verma, Neelam 2150 Organometallic Applications of SPME for the determination of metallic and organometallic species headspace GC-FID J. Sep. Sci., 29, #3, 333-345 (2006) Kaur, Varinder; Malik, Ashok Kumar; Verma, Neelam NaBEt4 derivatives A new method for simultaneous determination of Co(II), Ni(II) and Pd(II) 2615 Co(II), Ni(II), Pd(II) as morpholine-4-carbodithioate complex by SPME-HPLC-UV system HPLC-UV in water Talanta 73, #3, 425-430 (Sep 30 2007) Kaur, Varinder; Malik, Ashok Kumar 2491 Co(II), Ni(II), Pd(II) A new approach for simultaneous determination of Co(II), Ni(II), Cu(II), and Pd(II) using 2-thiophenaldehyde-3-thiosemicarbazone (TPTS) . PDMS fiber HPLC-UV in water as reagent by SPME-HPLC Anal Chim Acta 603, #1, 44-50 (2007 Nov 5) Kaur, Varinder; Aulakh, Jatinder Singh; Malik, Ashok Kumar TPTS derivative 911 Organometalics Development of new SPME fibers by sol-gel technology for SPME-HPLC determination of organometals Analytica Chimica Acta 1999, 402(1-2) 67-69 Gabatu, T., Sutton, K., Caruso, J. Solgel coatings HPLC 741 BTEX, herbicides High-performance polyethylene glycol-coated SPME fibers using sol-gel technology PAG sol-gel fiber in water J. Chromatogr. A 893 (2000) 157-168 30°C, headspace Wang, Z., Xiao, C., Wu, C., Han, H. salt added, pH adjusted 554 Sol-gel method for the preparation of SPME fibers Anal. Lett., 1999, 32(8), 1675-1681 Zhou, Z., Wang, Z., Qu, C., Zhan, W., Xu, Y. Solgel coatings 268 BTEX Field-Portable SPME/Fast GC for Trace Analysis Field Anal. Chem. Technol. 1 (5): 277-284 (1997) 30µm PDMS GC-FID, -PID in soil Gorecki, T., Pawliszyn, J. 2 min, headspace, stirring 555 Optimization of the SPME device design for field applications Fresenius' J. Anal. Chem. 1999, 364(7), 610-616 Muller, L., Gorecki, T., Pawliszyn, J. varied coatings Ambient temperature, unless otherwise indicated. 221
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SPME Applications Guide - Overbrook Scientific

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