SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Sex and developmental stage of carob flowers
1818 Fragrance affects composition of volatiles headspace GC-MS
from Carob J Horticultural Sci & Biotechnology, 79, #5, 689-692
flower Custodio, L.; Nogueira, J. M. F.; Romano, A.
Direct extraction of volatiles of rice during cooking using SPME
2690 Volatiles from Cereal Chemistry 4, #5, 423-427 (2007)
cooked rice Zeng Zhi; Zhang Han; Chen JieYu; Zhang Tao; Matsunaga, R.
Determination of flavour profile in Iranian fragrant rice samples
2476 Volatiles from using cold-fibre SPME-GC-TOF-MS 100um PDMS GC-TOF-MS
scented rice Flavour and Fragrance J. 22, #5, 377-391 (SEP-OCT 2007) headspace
Ghiasvand, Ali Reza; Setkova, Lucie; Pawliszyn, Janusz
Rapid discrimination of scented rice by SPME, mass spectrometry,
2418 Volatiles from and multivariate analysis used as a mass sensor headspace GC-MS
scented rice J. Agric. Food Chem. 55, #4, 1077-1083 (2007-02-21)
Laguerre, M.; Mestres, C.; Davrieux, F.; Ringuet, J.; Boulanger, R.
SPME-GC and olfactory analysis of the scent and
1819 Essential oils fixative properties of the essential oil of Rosa headspace GC-FID and GC-MS
from Chinese damascena L. from China
rose oil Flavour and Fragrance J, 20, #1, 7-12
Jirovetz, Leopold; Buchbauer, Gerhard; S, A;
Balinova, A.; Guangjiun, Z.; Xihan, Ma
Comparison of odorous volatile compounds from fourteen
1820 Volatiles from different commercial composts using SPME. headspace GC
compost Trans. Am. Soc. Agric. Eng., 48, #1, 315-320
Kim, H.; McConnell, L.L.; Millner, P.
Why are some floral nectars scented?
1821 Nectar odors Ecology (Washington D C), 85, #6, 1486-1494 headspace GC-MS
from flowers Raguso, Robert A.
Quality assessment of Flos Chrysanthemi Indici from
1822 Volatiles different growing aras in China by SPME-GC-MS 65µm PDMS-DVB GC-M
from China J. Chromatogr. A, 1047, #2, 281-287 30min @ 60°C
medicine Chen, J; Deng, C; Fu, D; Sha, Y; Shen, S Zhang, X headspace
SPME-GC-MS analysis of volatile compounds in compounded
1823 Volatiles Chinese medicinal prescription, Xiao-Cheng-Qi-Tang 100µm PDMS GC-MS
from China Journal of Pharma Biomed Analysis, 36, #2, 381-385 20min @ 90°C
medicine Sha, Yunfei; Shen, Shun; Duan, Gengli stirring, headspace
Application of HS-SPME and GC-MS to characterization of
1824 Volatiles from volatile compounds emitted from osmanthus flowers 65µm CW/DVB GC-MS
osmanthus Annali di Chimica, 94, #12, 921-927 10 min @ 22°C
flowers Deng, Chunhui; Song, Guoxin; Hu, Yaoming headspace
An evaluation of SPME for analysis of odorant
1825 Odors from emissions from stored biosolids cake 75µm Carboxen GC-MS
biosolids Water Res., 38, #17, 3800-3808 headspace
Parker, W.J.; Visan, M.
Effects of petroleum spray oils on oviposition behaviour and
1826 Volatiles from larval survival of Helicoverpa armigera Hubner (Lepidoptera headspace GC
maize plants Noctuidae) and Ostrinia nubilalis Hubner (Lepidoptera:Pyralidae)
Intl J of Pest Mgmt, 51, #2, 111-119
Mensah, Robert; Frerot, Brigitte; Al Dabel, Faiza
Pharmaceuticals
147 Volatiles in
Application of Head-Space SPME for the Analysis of
Volatile Metabolites GC-MS
biological fluids J. Microbiol. Methods 25: 245 (1996)
Milsson, T., Larsen, T., Montanarella, L., Madsen, J.
338 Solvents in
Determination of Residual Solvents in Pharmaceuticals
with Automated SPME 100µm PDMS GC-FID
pharmaceutical Chem. N. Z. 61 (4): 10-12 (1997) 15 min
products Penton, Z. headspace
149 Components
Analysis of Components in Crude Drugs by Headspace
SPME Method
Ambient temperature, unless otherwise indicated. 91