SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />
Analyte / Extraction<br />
Matrix Literature Reference Conditions Instrument<br />
2777 Malathion bait<br />
Malathion bait consumption and mortality of Anastrepha suspensa<br />
(Diptera : Tephritidae)<br />
Annals of the Entomological Society of America 101, #2, 418-429<br />
Nigg, H.; Schumann, R.; Rouseff, R.; Smoot, John M.; Fraser,<br />
headspace GC-MS<br />
103 Malathion<br />
Rapid Analysis of Malathion in Blood Using Head Space<br />
Solid Phase Microextraction and Selected Ion Monitoring 100µm PDMS GC-MS<br />
in blood Forensic Sci. Int. 88: 125-131 (1997) 90°C, 5 min<br />
Namer, A., Yashiki, M., Nagasawa, N., Iwasaki, Y.,<br />
Kojima, T.<br />
headspace<br />
489 Parathion<br />
Rapid analysis of parathion in biological samples using<br />
headspace <strong>SPME</strong> and GC-MS GC-MS<br />
in blood Clin. Chem. Lab. Med. 1999, 37(6), 639-642<br />
Musshoff, F., Junker, H., Madea, B<br />
headspace<br />
136 Carbamate in<br />
Determination of Some Carbamate Pesticides in Human Body<br />
Fluids by Headspace <strong>SPME</strong>/GC 100µm PDMS GC-NPD<br />
urine, serum Jpn. J. Forensic Toxicol. 14 (3): 199-203 (1996) 70°C, salt<br />
Seno, H., Kumazawa, T., Ishii, A., Nishif, M. headspace<br />
797 Amino pesticides<br />
Separation methods for amino group-possessing pesticides<br />
in biological samples. 100µm PDMS GC-FID, NPD<br />
in biological samples J Chromatogr B (2000) 747(1&2), 241-254 30min @ 95°C, salt<br />
Kumazawa, T; Suzuki, O. headspace<br />
490 Arylamide Herbicides<br />
Simple Analysis of Arylamide Herbicides in Serum using<br />
Headspace <strong>SPME</strong> and GC-MS 100µm PDMS GC-MS<br />
in Serum 6th Indo Pacific Congress on Legal Medicine and 45 min @ 90°C<br />
Forensic Science. 770-773(1998)<br />
Namera,A., Watanabe,T., Yashiki,M., Iwasaki,Y., Kojima,T.<br />
headspace, NaCl<br />
107 Diazepams in<br />
Solid-Phase Microextraction/Liquid Chromatography (<strong>SPME</strong>/LC)<br />
for Drug Analysis in Biological Fluids 85µm polyacrylate HPLC-UV,<br />
biological fluids Chromatography (1997), 18(4), 244-245,<br />
Jinno, K<br />
30°C, 3 hr 200nm<br />
658 Drugs<br />
<strong>SPME</strong> of drugs from biological matrices<br />
J. Chromatogr. A 885(2000) 445-455 review article<br />
in biological fluids Snow, N.<br />
234 Drugs in<br />
Analysis of Drugs and Poisons in Legal Medicine<br />
J. Mass Spectrom. Soc. Jpn. 44: 321-333 (1996) 100µm PDMS & GC-MS<br />
biological fluids Suzuki, O., Seno, H., Ishii, A.<br />
Confirmation of Volatiles by <strong>SPME</strong> and GC-MS in the<br />
85µm polyacrylate<br />
headspace<br />
NaCl, Na2SO4,<br />
108 Volatiles Investigation of Two Traffic Fatalities 85µm polyacrylate GC-MS<br />
in urine J. Anal. Toxicol. 1997, 21(4), 286-290 60°C, 10 min<br />
Brewer, W., Galipo, R., Morgan, S., Habben, K. headspace<br />
564 Tetarchoroethylene<br />
Tetrachloroethylene and trichloroethylene fatality:<br />
case report and simple headspace <strong>SPME</strong>-capillary 100µm PDMS GC-ECD<br />
trichloroethylene in GC determination in Tissues 1 min headspace<br />
tissue, urine, serum J. Anal.Toxicol, 24 (1), 22-26, (2000)<br />
Dehon, B., Humbert, L., Devisme, L., Stievenart, M., Mathieu, D.<br />
Houdret, N., Lhermitte, M.<br />
60°C<br />
2783 steroidal<br />
<strong>SPME</strong> followed by on-fiber derivatization of solasodine and<br />
solanidine aglycones of steroidal glycoalkaloids 60µm CW/DVB GC/MS<br />
glycoalkaloids J. Liq. Chromatogr.Relat. Technol. 31, #8, 1132-1146 (Jan 2008) immersion<br />
Eanes, Ritchie C.; Tek, Neslihan TMSI derivative<br />
2239 Steroid<br />
<strong>SPME</strong> with on-fiber silylation for simultaneous determinations<br />
endocrine disrupting chemicals and steroid hormones by GC-MS 85µm polyacrylate GC/MS<br />
Ambient temperature, unless otherwise indicated. 120
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