SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference SPME in Pretreatment of Environmental Samples Conditions Instrument 274 Huaxue Jinzhan 10 (1): 74-84(1998) Jia, J., He, Y., Huang, J. Direct SPME of Complex Aqueous Samples with Hollow 275 Aqueous samples Fiber Membrane Protection Anal. Commun. 33 (7): 219-221(1996) Zhang, Z., Poerschmann, J., Pawliszyn, J. The degradtion of humic substance using continuous 2838 Organics from photocatalysis systems GC humic material Sep. Sci. Technol. 43, #1, 93-112 (January 2008) Areerachakul, N.; Duangduen, C.; Kandasamy, J.; Vigneswaran, S. Partitioning of selected environmental pollutants into organic matter 2618 Organics from as determined by solid-phase microextraction GC humic material Chemosphere 66, #8, 1580-1589 (2007-01) Prosen, H.; Fingler, S.; Zupancic-Kralj, L.; Drevenkar, V. Bioavailability of PCBs from field-collected sediments: Application 2801 PCBs in sediment of Tenax extraction and matrix-SPME techniques GC Chemosphere 71, #2, 337-344 (MAR 2008) Trimble, Tricia A.; You, Jing; Lydy, Michael J. Availability of polychlorinated biphenyls in field-contaminated sediment 2631 PCBs in sediment Env Tox Chem 26, #9, 1940-1948 (SEP 2007) GC You, Jing; Landrum, Peter E.; Trimble, Tricia A.; Lydy, Michael J. Sorption of very hydrophobic organic compounds onto 693 Alkanes, PCBs,PAHs PDMS and dissolve humic organic matter. 1. Adsorption or 7um, 30um PDMS GC-MS in humic material partitioning of VHOC on PDMS coated SPME fibers- 20 min SIMS never-ending story stirring Environ Sci Technol 2000, 34, 3824-3830 Poerschmann, J., Gorecki, T., Kopinke, G. Sorption of hydrophobic organic compounds on nonpolar 844 Hydrophobic organics SPME fibres and dissolved humic organic matter long dash PDMS, polyacrylate GC-MS in humic material Part III: Application of the solubility parameter concept to interpret sorption on SPME fibre coatings J Microcolumn Separations (2000) 12(12), 603-612 Poerschmann, J. 923 Use of SPME for measuring oil-water partition coefficients and correlation with HPLC methods for lipophilicity J. Chromatogr A (1999) 864(2) 183-189 Pollein, P., Roberts, D. HPLC 276 Phenols, PAHs SPME for Determining Distribution of Chemicals in Aqueous Matrixes 100µm PDMS GC-MS in wastewater Anal. Chem. 69 (4): 597-600 (1997) 10 sec Zhang, A., Kopinke, G., Pawliszyn, J. stirring 277 Chlorinated organics Water Solubility and Octanol/Water-Partitioning of Hydrophobic Chlorinate Organic Substances Determined in water by Using SPME/GC Fresenius’ J. Anal. Chem. 360 (1): 52-57 (1998) Paschke, A., Popp, P. 278 Phenols Determination of Phenols by Solid-Phase Microextraction J. Chromatogr. A 767 (1+2): 171-175 (1997) 85µm polyacrylate GC-FID in water Bartak, P., Cap, L. Determination of Chlorophenols Using SPME and GC/MS 25°C, 60 min headspace pH 1, salt added 439 Chlorophenols Ann. Chim. (Rome) (1998), 88(9-10), 629-635 GC-MS in water Guidotti, M., Ravaioli, G. Determination of volatile organic compounds pollution sources in Ambient temperature, unless otherwise indicated. 154
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2617 Organics in Malaysian drinking water using multivariate analysis 100µm PDMS GC-MS drinking water Environ. Monit. Assess. 124, #1-3, 39-50 (January 2007) Abdullah, Pauzi; Soh, Shiau-Chian 2152 Organics in Evaluation of SPME as an alternative to the official method for the analysis of organic micro-pollutants in drinking water 65µm PDMS/DVB GC-MS drinking water J. Chromatogr. A, 1101, #1-2, 46-52 (2006) Guillot, Sophie; Kelly, Mary T.; Fenet, Helene; Larroque, Michel 30 min @ 60°C 777 Organics Solid phase extraction techniques for drinking water abstraction monitoring and investigation of pollution GC-MS in drinking water incidents J Water Supply Res and Tech (2000) 49(2), 103-109 Gardner, M.; Comber, S. ; Rogers, H. 944 Organics Determination of water contaminants at trace levels using large volume sampling techniques: Comparison of LVPTVI, in water LVOCI, and SPME. American Laboratory (2001) 33(11), 45-47 Trisciani, A.; Munari, F.; Anelli, L.; Castanho, J. 279 VOCs Pollution of Ground and Drinking Water with Volatile Organic Compounds, SPME and GC/MS Analysis GC-MS in water Toxicol. Environ. Chem. 55 (1-4): 73-81 (1996) Hassan, A., Benfenati, E., Facchini, G., Fanelli, R. 280 Trihalomethanes Determination of Trihalomethanes in Drinking Water by SPME-GC with Electron-Capture Detection GC-ECD in water Toxicol. Environ. Chem. 60(1-14): 39-45 (1997) Chen, M., Mao, I., Hsu, C. Determination of Chlorinated Acetic Acids in Drinking 281 Chloroacetic acid esters Water by in situ Derivatization and Solid Phase 30µm PDMS GC-ECD in water Microextraction 1 min Int. J. Environ. Anal. Chem. 66 (3): 215-224(1997) headspace Aikawa, B., Burk, R. Studies on the application of SPME for analysis of volatile stirring methanolic HCl added 510 Sulfur compounds in organic sulfur compounds in gaseous and liquid samples FPD-GC water, N2 & propane Chem. Anal. (Warsaw), 1999, 44(3A), 485-493 Wardencki, W., Namiesnik, J. 339 Geosmin, 2-MIB Rapid Analysis of Geosmin and 2-Methylisoborneol in Water Using SPME Procedures 100µm PDMS GC-MS in water Water Research Vol. 32, No. 7, 2140-2146 (1998 40°C, 30 min Lloyd, S., Lea, J., Zimba, P., Grimm, C. Analysis of 2-Methylisoboreneol and Geosmin in Catfish headspace, stirring salt added 362 2-MIB, geosmin by Microwave Distillation-SPME 100µm PDMS GC-MS in catfish J. Agri. Food Chem., 47, No. 1, pg. 164-169, 1999 40°C, 30 min Lloyd, S., Grimm, C. Determination of Geosmin and 2-Methylisoboreneol in Water headspace, stirring salt added 80µm 446 MIB & geosmin Using SPME and GC-Chemical Ionization/Electron Impact Carboxen/DVB/PDMS GC-MS in water Ionization Ion Trap MS 60°C, 30 min Analyst (Cambridge, U.K.) (1998), 123 (10), 2155-2160 headspace McCallum, R., Pendleton, P., Scumann, R., Trinh, M. stirring salt added 2778 Ozone in air Passive sampling of ambient ozone by SPME with on-fiber derivatization Analytica Chimica Acta: 610, #2, 149-155 (MAR 10 2008) 65µm DVB/PDMS GC-ECD Lee, I-Su; Tsai, Shih-Wei PFBHA & DPE derivatives @ 25°C Ambient temperature, unless otherwise indicated. 155
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