SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
in olive oil An application in the discrimination of virgin olive oils
according to the cultivar and area
Proceedings of the Phytochemical Society of Europe
(2000) Vol. 46, 211-220
Servili, M; Montedoro, G; Selvaggini, R; Taticchi, A
577 Dimetyl disulfide & Volatile reduced sulfur compounds in butter by SPME 85µm polyacrylate GC-EID
methanethiol J-Dairy-Res. Feb 1999; 66(1): 115-123 10 min. @ 30-35°C
in butter Shooter,-D; Jayatissa,-N; Renner,-N
338 Benzene, toluene Determination of benzene & toluene in vegetable HPLC
in vegetable oil oil by SPME/HPLC headspace
J. Commod. Sci. (1999), 38(1), 3-14
Giuffrida, R., Clasadonte, M., Zerbo, A.
606 Volatiles Headspace SPME use for the Characterization of volatile Carboxen/DVB/PDMS GC-FID
in vegetable oil compounds in vegetable oils of different sensory quality 20-60°C
J. Agric Food Chem, (2000), 48(6), 2360-2367 headspace
Jelen, H., Obuchowska, M., Zawirska-Wojtasiak, R.
885 Steroisomers Different stereoselectivity in the reduction of pulegone GC-MS
Pulegone enantiomers by Mentha species
Planta Medica (2001) 67(3) 260-262
Mosandl, A.; Beck, T.; Fuchs, S.
2724 Aldehydes in Determination of stale aldehydes in beer by headspace SPME and 65µm PDMS/DVB GC-MS
beer automatic precolumn derivatization. headspace
Fenxi Shiyanshi 26, #4, 38-41(2007) 60min @ 60°C
Wu, Q. -J.; Chen, H. -L.; Yang, Z. -X. PFBOA derivative in Chinese
2393 NDMA in Solid-phase microextraction of N-nitrosodimethylamine in beer 65µm PDMS/DVB GC-MS
beer Food Chemistry 107, #3, 1348-1352 (2008) headspace
Perez, D. M.; Alatorre, G. G.; Alvarez, E. B.; Silva, E. E.; Alvarado, J. F. J
2219 Aroma High gravity fermentations for low calories beer production GC
from Beers Journal of Biotechnology (2005) 118 Suppl. 1, S152
Piddocke, Maya; Sorensen, Thomas; Pedersen, Sven; Olsson, Lisbeth
2558 Flavors in Method optimization by SPME in combination with GC-MS for 75µm Carboxen GC-MS
beer analysis of beer volatile fraction headspace
J. Chromatogr., A 1121, #2, 145-153 (2006-07-21)
Pinho, O.; Ferreira, M.; Santos, L.
106 Flavors in Characterization of Beer Samples Using SPME-GC Analysis 100µm PDMS GC-FID
beer Supelco Reporter Vol. 16, #4, pg. 7
Vas, G.
10 min
2716 Sulfur compounds Comparison of headspace and direct single-drop microextraction headspace GC-FPD
in beer and headspace SPME for the measurement of volatile sulfur
compounds in beer and beverage by GC-FPD
J. Chromatogr. A. 1125, #1, 133-137 (2006-08-25)
Xiao, Q.; Yu, C. H.; Xing, J.; Hu, B.
607 Sulfur compounds Determination of sulfur compounds in beer using headspace 65µm Carboxen/PDMS GC-FPD
in beer SPME and GC analysis with pulsed FPD detector 32min @45°C
J. Chromatogr. A. (2000), 872(1+2), 203-213
Hill, P., Smith, R.
headspace
100 Flavors Characterization of Commercial Vodkas by SPME-GC/MS 100µm PDMS GC-MS
in vodka J. Sci. Food Agric. 70: 380-388 (1996)
Ng, L., Hupe, M., Harnois, J., Moccia, D.
1 hr
202 Methylcyclopendienyl Determination of Methylcyclopendienyl Manganese Tricarbonyl
manganese in Beverages by SPME
tricarbonyl Food Addit. Contam. 14 (3): 301-307 (1997)
in beverages Forsyth, D., Dusseault, L.
2538 Attractants of Onion aphid (Neotoxoptera formosana) attractants, in the headspace of headspace GC-MS
onion aphids Allium fistulosum and A-tuberosum leaves
J Applied Entomology 131, #1, 8-12 (FEB 2007)
Ambient temperature, unless otherwise indicated. 7