SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference
Improvement of the chemometric variety characterization of
Conditions Instrument
582 Aroma volatiles wines by improving the detection limit for aroma compound 85µm polyacrylate GC-EMIS
in wine J-High-Resolut-Chromatogr. Jun 1999; 22(6): 322-326 3 hr. , headspace
Weber,-J; Beeg,-M; Bartzsch,-C; Feller,-K-H;
De-la-Calle-Garcia,-D; Reichenbaecher,-M; Danzer,-M
NaCl added
459 Aroma volatiles
Determination of volatiles from red wines made
by carbonic maceration using SPME technique 100µm PDMS GC-EIMS
in wine Acta Aliment, 1999, 28(1), 95-101
Vas, G., Loerincz, G.
10 min headspace
2536 Aroma volatiles
A comparison of the volatiles compounds from Pinus massoniana
twigs extracted by SPME and steam distillation headspace GC/MS
from Pinus J Nanjing Forestry University (Natural Sciences Edition)
massoniana twigs 31, #1, 78-80 (2007)
Wang Yan; Ye JianRen
2634 Phenolic content
Determination of the alkyl- and methoxy-phenolic content in wood
extractives by micellar solid-phase microextraction and GC-MS headspace GC/MS
in wood Talanta 73, #3, 505-513 (SEP 30 2007)
Pino, Vernica; Ayala, Juan H.; Gonzalez, Venerando; Afonso, Ana M.
Induction of sesquiterpenoid production by methyl jasmonate
2295 Fragrances in aquilaria sinensis cell suspension culture headspace GC/MS
from woody J. Essent. Oil Res. (2005) 17 #2, 175-180
material Honda, G.; Ito, M.; Kiuchi, F.; Okimoto, K.; Shimada, Y.; Yagura, T.
2528 Aroma volatiles
Analysis of French and American oak chips with different toasting
degrees by headspace SPME-GC-MS Car/DVB 30/50µm GC/MS
from oak chips Journal of Chromatography A 1173, #1-2, 10-17 (2007)
Bozalongo, R.; Carrillo, J.; Fernandez-Torroba, M.; Tena, M.
headspace
Monitoring Toasting Intensity of Barrels by
559 Aroma volatiles Chromatographic Analysis of Volatile 100µm PDMS GC-FID
from toasted oak compounds from Toasted Oak Wood 30 min @ 22°C
J. Agric. Food Chem, 1999, 47, 4310-4318
Chatonnet, P., Cutzach, I., Pons, M., Dubourdieu, D. headspace
Application of SPME for determining residues of chlorpyrifos and
2663 Chlorpyrifos in chlorpyrifos-methyl in wine with gas chromatography (GC). headspace GC-ECD
wine J Institute of Brewing 113, #2, 213-218 (2007)
Anli, E.; Vural, N.; Vural, H.; Gucer, Y.
Assembly tests of "Nero d'Avola" with wines
460 Polyphenolics derived from an allocthonous cultivar: GC-MS
in red wine study of polyphenolic and aromatic profiles. headspace
Ind. Bevande (1999), 28(160), 119-126 Italian
Papucci, A, Monte, L., D'Agostino, S,
Aozzino, P., Avellone, G
Sample preparation optimization in wine and grapes. Dilution and
2885 Volatiles from sample/headspace volume equilibrium theory for headspace SPME headspace GC-MS
wine and grapes J Chromatogr A 1192, #1, 25-35 (May 23 2008)
Boss, Paul K.; Kalua, Curtis M.
Comprehensive two-dimensional gas chromatography with TOF-MS
2635 Monoterpenoids of monoterpenoids as a powerful tool for grape origin traceability headspace GC-ToF-MS
from white grapes J Chromatogr A 1161, #1-2, 292-299 (AUG 17 2007)
Rocha, S.; Coelho, E.; Zrostlikova, J.; Delgadillo, I.; Coimbra, M.
Distinction and identification of lignins based on their volatile
2763 Volatiles from headspace composition headspace GC-MS
ligins Talanta 75, #2, 594-597 (Apr 15 2008)
Delgadillo, Ivonne; Evtuguin, D.; Goncalves, V.; Rocha, S.
Monitoring ester formation in grape juice fermentations
775 Esters using SPME coupled with GC-MS 100µm PDMS GC-MS
Ambient temperature, unless otherwise indicated. 19