SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 31 VOCs, chloropesticides and Narrow Bore Capillary Columns 100µm PDMS GC-MS in water J High Res. Chromatogr. 18(8): 495-499 (1995) 15 min Shirey, R. stirring saturated salt 47 BTEX compounds Determination of BTEX Compounds in Water by Solid-Phase Microextraction and Raman Spectroscopy 100µm PDMS GC-FID in water Anal. Chem. 67(3): 600-605 (1995) Wittkamp, B., Tilotta, D. 681 Volatiles A new method for the rapid determination of volatile substances: the SPME-direct method Part 1: Apparatus and working conditions Sens, Acatuators, B. (2001) B72 (2) 184-187 Bene, A., Fornage, A., Luisier, J., Pichler, P., Villettaz, J. 830 Methyl, ethylmercury Direct hydride derivatization of methyl- and ethylmercury chlorides in acqueous solution with KBH4 GC-MS chlorides J Environ Sci (China) (2000) 12(3) 275-278 in water Jiang Gui-bin; He Bin 2582 Methylmercury Methylmercury determination in biota by SPME matrix effect evaluation J Chromatogr A 1174, #1-2, 2-6 (2007 Dec 7) headspace GC-Py-AFS derivatives in biological matrix Carrasco, Luis; Doez, Sergi; Bayona, Josep M Determination of Methymercury in Fish and River Water NaBEtr derivative 48 Methylmercury Samples Using in situ Sodium Tetraethylborate 100µm PDMS GC-MS derivatives Derivatization Followed by SPME and GC-MS 10 min in water and fish J. Chromatogr. 696: 113-122 (1995) stirring Cai, Y., Bayona, J. headspace 407 Organomercury SPME and GC-MIP-AED for the Speciation Analysis of Organomercury Compounds 100µm PDMS GC-MIP-AED in water and soil J. High Resol. Chromatogr. 1999, 22 (3) 181-182 25°C Mothes, S., Wennrich, R. Solid Phase Microextraction of Metal Ions 50 min (immersion) 20 min (headspace) 18 Bismuth III Microchim. Acta 112: 41-6 (1993) bare, or 100µm PDMS UV / VIS in water Otu, E., Pawliszyn, J. Speciation of dimethylarsinic acid and monomethyl- 60 min immersion 460nm 682 Dimethylarsinic acid arsonic acid by SPME-GC-ion trap MS 100µm PDMS GC-MS arsonic acid J. Chromatogr.A 2000, 873(1), 129-135 Mester, Z., Pawliszyn, J. 40min @ 20°C thioglycol methylate derv. 96 Organo Hg, Sn, Pb Sensitive, Simultaneous Determination of Organomercury Lead, and Tin Compounds with Headspace SPME 100µm PDMS ICP-MS in water Capillary GC Combined with Inductively Coupled Plasma MS 10 min Anal. Chem. 69: 1604-1611 (1997) headspace Moens, L., DeSmaele, T., Dams, R., VanDen Broeck, P., stirring Sandra, P. SPME-GC-glow discharge-optical emission detection for pH 5.3 NaBEtr derivative 873 Tin & lead tin and lead speciation GC-OES in water J Anal At Spectrom (2001) 16(4), 376-381 Orellana-Velado, N.G.; Pereiro, R.; Sanz-Medel, A Speciation of organotins in environmental samples by NaBEtr derivative 796 Organo Sn SPME-GC: comparison of four specific detectors: FPD, PFPD in water J. Anal. At. Spectrom (2001) 16(3), 263-269 MIP-AES Aguerre, S; Lespes, G; Desauziers, V; Potin-Gautier, M ICP-MS 2764 Organotin and Optimisation of the headspace-SPME for organomercury and organotin compound determination in sediment and biota 30 µm PDMS MIP-AES organomercury in J. Sep. Sci. 31, #4, 768-774 (March 2008) Headspace sediments de Diego, A.; Delgado, A.; Madariaga, Juan M.; Prieto, Ailette; 3-24 min@ 20-90°C Ambient temperature, unless otherwise indicated. 146
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Usobiaga, Aresatz; Zuloaga, Olatz NaBEtr derivative 2244 Organotin in Organotin speciation in Bizerte lagoon (Tunisia) Science of the Total Environment 349, #1-3, 211-222 (2005) headspace GC-PFPD marine sediments Mzoughi, N.; Lespes, G.; Bravo, M.; Dachraoui, M.; Potin-Gautier, M. Preconcentration and Determination of Sn- and Pb-Organic NaEt4B derivatives 153 Organo Sn, Pb Species in Environmental Samples by SPME and GC-AED GC-AED in water Fresenius’ J. Anal. Chem. 354: 587-91 (1996) Tutschiku, S., Mothes, S., Wennrich, R. Determination of Organotin Compounds in Water Samples 215 Organotin by Solid-Phase Microextraction (SPME) and GC-MS GC-MS in water Ann. Chim. (Rome) 87: 497-504 (1997) Guidotti, M., Vitali, M. 152 Methyltin Rapid Determination of Methyltin Compounds in Aqueous Samples Using SPME and Capillary GC Followed by 100µm PDMS GC-FPD in water in situ Derivatization with Sodium Tetraethylborate 29°C, 2-35 min J. High Res. Chromatogr. 18: 767 (1995) headspace Morcillo, Y., Cai, Y., Bayona, J. Determination of Tetraethyllead and Inorganic Lead in Water stirring NaBEtr derivative 161 Lead derivatives by SPME-GC 100µm PDMS GC-MS in water Anal. Chem. 68: 3008 (1996) 10 min Gorecki, T., Pawliszyn, J. headspace 683 Lead derivatives Determination of Tetraethyllead by SPME-thermal desorption quartz furnace atomic absorption spectrometry AA in water J. Anal. At. Spectrom. 2000, 15(16), 705-709 Sandra Fraguairo, M, AlavapMoreno, F., Isela, B. 10 min, headspace Rapid Determination of Butyl, Phenyl and Cyclohexyl Tin 23 Organotin compounds Compounds in Aqueous Samples Using SPME and 100µm PDMS GC-FPD in water Capillary Gas Chromatography Following in situ Derivatization 30 min with Sodium Tetraethylborate immersion CID-CSIC Jordi Girona, 18-26, E-8034, Barcelona, Spain stirring Morcillo, Y., Cai, Y., Porte, C., Bayona, J. NaBEt4 derivative 503 Organo-tin, -lead, Determination of organometallic compounds in surface water and sediment samples with SPME-CGC-ICPMS 100µm PDMS GC-ICPMS -mercury Mikrochim. Acta (1999), 130(4), 241-251 10 min in water De Smaele, T., Moens, L., Sandra, P., Dams, R. headspace 235 Rare earth elements Separation of Cerium from Other Rare-Earth Elements with Application to Samarium-Neodymium and Lanthanum- Cerium Chronometry Nucl. Instrum. Methods Phys.Res.Sect.B 117: 201-208 (1996) Rehkaemper, M., Gaertner, M., Galer, S., Goldstein, S. 2742 Selenite and Comparison of two derivatizing agents for the simultaneous. determination of selenite and organoselenium species immersed vs GC-MS organoselenium by GC and atomic emission . headspace (20min) J. Chromatogr. A 1165, #1-2, 191-199 (Sep 21 2007) piazselenol Campillo, N.; Penalver, R.; Hernandez-Cordoba, M.; Perez-Sirvent, C.; Martinez-Sanchez, M. -J. derivative 580 Selenite, selenate Selective determination of selenite and selenate using SPME and GC-MS GC-MS in water J-High-Resolut-Chromatogr. Jul 1999; 22(7): 414-416 35 min, agitation Guidotti,-M; Ravaioli,-G; Vitali,-M Compound-specific nitrogen and carbon isotope analysis of piazselenol derivative immersed 2752 Nitroaromatics nitroaromatic compounds in aqueous samples using SPME-GC/IRMS GC/IRMS in water ANAL. CHEM. 79, #6, 2386-2393 (15 MAR 2007) Berg, M.; Bolotin, J.; Hofstetter, T. B. Ambient temperature, unless otherwise indicated. 147
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