SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2844 Organics organic micropollutants from aqueous samples and analysis by GC-MS DVB/Cab (30/50 μm) GC-MS in water Anal. Chim. Acta 618, #1, 61-69 (Jun 16 2008) Gupta, Manju; Jain, Archana; Pillai, Aradhana K.K.V.; Verma, K. Target and nontarget screening of organic micropollutants in water by 2339 Organics SPMEs combined with GC-TOF-MS in water Anal Chem Vol. 79, # 24 9494-504 (2007 Dec 15) GC-TOF-MS Hernandez, F.; Portoloes, Tania; Pitarch, Elena; Loopez, F. 2846 PAHs in SPME followed by HPLC with fluorimetric and UV detection for the determination of polycyclic aromatic hydrocarbons in water 65µm PDMS/DVB LC-UV water Analytical Letters 41, #1, 119-136 (2008) 60 min @ 70°C Ricardo Lucio-Gutierrez, J.; de la Luz Salazar-Cavazos, Maria; Waksman de Torres,Noemi H.; Castro-Rios, Rocio immersion 2397 PAHs in Determination of PAHs in aqueous samples by microwave assisted headspace SPME-GC-FID 65µm PDMS/DVB GC-FID water Talanta 72, #4, 1269-1274 (2007-06-15) Wei, M. -C.; Jen, J. -F. 30 min @ 20°C SPME-GC-MS analysis of PAHs Towards the European 2345 PAHs in Union water directive 2006/0129 EC 65µm PDMS/DVB GC-MS water J Chromatogr A 1176, #1-2 , 48-56 (2007 Dec 28) immersion GC-MS-MS Fernoandez-Gonzoalez, V; Concha-Graona, E; Muniategui-Lorenzo, S; Loopez-Mahoa, P; Prada-Rodroguez, D Predicting PAH bioaccumulation and toxicity in earthworms exposed to 2543 PAHs in manufactured gas plant soils with solid-phase microextraction earthworms Env Science & Tech 41, #21, 7472-7478 (NOV 1 2007) Jonker, T. O.; van der Heijden, S.; Kreitinger, J.; Hawthorne,S. 2596 Organics Characterization of an urban landfill soil by using physicochemical . analysis and solid phase microextraction (SPME)-GC/MS 65µm PDMS/DVB GC-MS from soil Env. Monitoring Assessment 127, #1-3, 337-351 (APR 2007) headspace Banar, Mufide; Ozkan, Aysun; Vardar, Cigdem 15 min @ 50°C SPME to predict bioavailability and accumulation of organic 1947 Organics micropollutants in terrestrial organisms after exposure 30µm PDMS GC-MS from soil to a field-contaminated soil headspace Environ. Sci. Technol., 38, #18, 4842-4848 10 days exposure Barendregt, A; Fleuren, R; Hermens, J.; Jager, T; Sinnige, T.; Van Der Wal, Leon; Van Gestel, Cornelis A. M. SPME coupled to GC-MS for determining PAH-micelle 1948 PAHs in micelle partition coefficients 85µm polyacrylate GC-MS micelles Anal. Chem., 76, #15, 4572-4578 100µm PDMS Alfonso, Ana M.; Ayala, Juan H.; Gonzalez, V; Pino, V. Implementation of new methods to characterise 1949 Odors from atmospheres in piggeries headspace GC-MS pig sheds Int. J. Environ. Anal. Chem., 84, #9, 647-659 Begnaud, F.; Berdague, Jean-Louis; Lebost, J.; Murat, C.; Peres, C. In-tube solid-phase microextraction and online 1950 Organics in coupling with high-resolution GC. 5 M X 0.53mm ID GC water LC-GC Europe, 17, #3, 144-151 1.2µm PDMS Wang, H. W.; Liu, W. M.; Guan, Y. F. Characterization of volatile organic compounds on 1951 Odor from airborne dust in a swine finishing barn 75µm Carboxen GC swine Trans. Am. Soc. Agric. Eng., 47, #4, 1231-1238 100µm PDMS facilities Jeon, I.J.; Maghirang, R.G.; Razote, E.B.; Seitz, L.M headspace Water 778 Volatile organics Solid Phase Microextraction of volatile organic compounds in environmental applications 100µm PDMS GC in environmental Am Laboratory (2001)33(4), 18-20 85µm Polyacrylate samples Van Longenhove, H; Dewulf, J. 15 min. 858 Organic pollutants SPME - a convenient tool for the determination of organic pollutants in environmental matrices Ambient temperature, unless otherwise indicated. 140
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in environment Crit. Rev. Anal. Chem (2001) 31(1) 1-18 Zygmunt, Bogdan; Jastrzebska, Anna; Namiesnik, Jacek 2670 Toluene from Characterisation of absorptive sampling with SPME fibres in the EUPHORE photoreactor GC air Talanta 72, #5, 1757-1766 (JUL 31 2007) Alvarez E., Gomez Experimental confirmation of the dicarbonyl route in the photo-oxidation 2601 Carbonyl product of benzen and toluene photo-oxidation Env Sci Tech 41, #24, 8362-8369 (DEC 15 2007) BTEX Alvarez, E. Gomez; Viidanoja, J.; Munoz, A.; Wirtz, K.; Hjorth, J. PFBHA derivatives Rapid analysis of tile industry gaseous emissions by ion mobility 2717 Volatile emissions spectrometry and comparison with SPME-GC-MS GC-MS industrial gaseous J. Environ. Monit. 8, #12, 1219-1226 (2006-11-28) Pozzi, R.; Bocchini, P.; Pinelli, F.; Galletti, G. C. Comparative application of SPME fibre assemblies and semi-permeable 2710 Semivolatile membrane devices as passive air samplers for semi-volatile chlorinated organic compounds. A case study on the landfill "Grube Antonie" in 65µM CW/DVB GC chlorinated Bitterfeld, Germany passive air sample organics in air Environmental Pollution 144; # 2; 414-422 (2006-11-15) Paschke, A.; Vrana, B.; Popp, P.; Schueuermann, G. Modelling of toluene SPME for indoor air sampling. 2602 Toluene from Anal Bioanal Chem 388, #1, 147-56 (2007 May) 75µm Carboxen GC air samples Mocho, Pierre; Larroque, Virginie; Desauziers, Valoerie 1 BTEX compounds, The Application of Chemically Modified Fused Silica Fibers in the Extraction of Organics from Water Matrix uncoated fiber GC-FID PCBs, solvents Samples and Their Rapid Transfer to Capillary Columns 1 min in water Water Pollution Research J. Canada 24: 179 (1989) Belardi, R., Pawliszyn, J. 2678 VOCs Development of a simple, accurate SPME-based method for assay of VOCs in column breakthrough experiments headspace GC in water CHEMOSPHERE 66, #1, 18-29 (2006) Salaices, Avila M. A.; Breiter, R.; Mott, H. 5 min Multiple solid-phase microextraction: Theory and applications. 2682 Review article Trends Anal. Chem 26, #3, 206-214 (2007-03) Tena, M. T.; Carillo, J. D. Developments in multiple headspace extraction 2685 Review article J. Biochem. Biophys. Mehods 70, #2, 229-233 (10 MAR 2007) Hakkarainen, M. Sorbent- and liquid-phase microextraction techniques and membrane- 2789 Review article assisted extraction in combination with GC analysis: A review Anal. Chim. Acta 614, #1, 27-37 (Apr 28 2008) Hyotylainen, Tuulia; Riekkola, Marja-Liisa 3 VOCs Solid Phase Microextraction for the Direct Analysis of Water: Theory and Practice 100µm PDMS GC-FID in water LC-GC 10: 656-661 (1992) 2-5 min Arthur, C., Potter, D., Buchholz., K, Motlagh, S., Pawliszyn, J. salt added 4 VOCs, PCBs, Practical and Theoretical Aspects of Solid Phase Microextraction for the Direct Analysis of Groundwater 100µm PDMS GC-FID solvents in water Proceedings 15th Annual EPA Conference-Analysis 5-14 min of Pollutants in Environment, Norfolk, VA, May 1992 Arthur, C., Buchholtz, K., Motlagh, S., Killam, L., Pawliszyn, J. salt added Ambient temperature, unless otherwise indicated. 141
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