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SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference<br />

Determination of dichlorvos by online microwave-assisted extraction coupled to<br />

headspace solid-phase microextraction and gas chromatography-electroncapture<br />

detection.<br />

Conditions Instrument<br />

1148 Dichlorvos Journal of Chromatography, A (2002) 976 (1-2), 349-355.<br />

Chen, Y. I.; Su, Y. S.; Jen, J. F.*<br />

GC-ECD<br />

Analysis of polar pesticides in water and wine samples by automated in-tube<br />

solid-phase microextraction coupled with high-performance liquid<br />

chromatography-mass spectrometry.<br />

Polar pesticides in<br />

1152 water and wine. Journal of Chromatography, A (2002) 976 (1-2), 357-367.<br />

Wu, J. C.; Tragas, C.; Lord, H.; Pawliszyn, J. *<br />

ESI-MS<br />

1172<br />

1177<br />

1192<br />

Oxidation residues of<br />

herbicides<br />

Pesticides in water<br />

samples.<br />

Atrazine and<br />

organophosphorus<br />

pesticides in soil<br />

Determination of oxadiazon residues by headspace solid-phase microextraction<br />

and gas chromatography-mass spectrometry<br />

Journal of Chromatography A (2002) 946(1-2), 239-245<br />

Araujo, Lilia; Navalon, Alberto; Prieto, Avismelsi; Vilchez, Jose Luis<br />

Solventless sample preparation for pesticides analysis in environmental water<br />

samples using solid-phase microextraction-high resolution gas<br />

chromatography/mass spectrometry (<strong>SPME</strong>-HRGC/MS)<br />

Journal of Environmental Science and Health - Part B Pesticides, Food<br />

Contaminants, and Agricultural Wastes (2003) 48 (4), 417-428. Various<br />

Lancas, Fernando M.; Souza, Dalva A.<br />

Solid-phase microextraction method for the determination of atrazine and four<br />

organophosphorus pesticides in soil samples by gas chromatography.<br />

Journal of Chromatography A (2001) 939(1-2), 13-21 GC-MS<br />

Camara, C.; Bouaid, A.; Fernandez, P.; Gonzalez, M. J.; Ramos, L.<br />

1219 DDT<br />

On-fiber photodegradation after solid-phase microextraction of p,p '-DDT and<br />

two of its major photoproducts, p,p '-DDE and p,p '-DDD.<br />

Journal of Chromatography, A (2003) 985 (1-2), 175-183.<br />

Llompart, M.; Lores, M.; Lourido, M.; Sanchez-Prado, L.; Cela, R.<br />

GC-MS<br />

Determination of organophosphorus insecticide residues by solid-phase<br />

microextraction coupled with gas chromatography-mass spectrometry.<br />

Organophosphorous<br />

1299 insecticide residues. Sepu (2003), 21 (3), 273-276.<br />

Shuai, Q.; Yang, W.; Zheng, Y. J.; Zheng, C. G.<br />

PDMS or polyacrylate. GC-MS<br />

1309<br />

Solid-phase microextraction coupled with high-performance liquid<br />

chromatography for the determination of phenylurea herbicides in aqueous<br />

samples<br />

Phenylureas herbicides<br />

in aqueous samples. Journal of Chromatography, A (2003) 1012 (1), 57-66.<br />

Huang, Shang-Da; Lin, Hsin-Hang; Sung, Yu-Hsiang<br />

PDMS-DVB, CW-TPR HPLC<br />

Pesticide vapours in confined atmospheres. Determination of dichlorvos by<br />

<strong>SPME</strong>-GC-MS at the mg m-3 level.<br />

Dichlorvos in<br />

1316 pesticides. Journal of Environmental Monitoring (2003) 5 (4), 574-577.<br />

Sanusi, Astrid; Montury, Michel; Ferrari, Federico; Millet, Maurice<br />

PDMS GC-MS<br />

2440 Acaricides<br />

GC-MS determination of acaricides from honey after a new fast<br />

ultrasonic-based <strong>SPME</strong> sample treatment 85µm polyacrylate GC-MS<br />

from honey Talanta 71, #5, 1906-1914 (2007-03-30)<br />

Rial-Otero, R. ; Gaspar, E. M.; Moura, I.; Capelo, J. L.<br />

30 min<br />

1355 Pesticides in honey.<br />

A solid-phase microextraction-gas chromatography-mass spectrometry<br />

approach for antivarroa acaricides and pesticide residues in honey.<br />

Chromatographia (2001) 54 (3-4), 241-246.<br />

Volante, M.; Galarini, R.; Miano, V.; Cattaneo, M.; Pecorelli, I.; Bianchi, M.;<br />

Marinoni, M. T.; Cossignani, L.; Damiani, P<br />

100 um PDMS GC-MS<br />

Ambient temperature, unless otherwise indicated. 191

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