SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
in water Toxicol. Lett. 2000, 112-1113, 273-282
Parkerton, T, Sone, M., Letiski, D.
643 Methadone
SPME in the determination of methadone in human
saliva by GC-MS 100µm PDMS
in saliva J. Anal Toxicol (2000), 24(2), 93-96
Dos Santos Lucas, A., Bermejo, A.,
Fernandez, P., Tabernero, M
30 min
29 Methadone
Gas Chromatographic Analysis of Methadone in Urine Samples
after Solid Phase Microextraction 100µm PDMS GC-MS
in urine J. Microcolumn Sep. 6: 577-581 (1994) 15 min
Chiarotti, M., Marsili, R.
Use of SPME for the determination of methadone and
immersion
pH 7.7
644 Methadone, EDDP EDDP in human hair by GC-MS 100µm PDMS GC-MS
in human hair Forensic Sci. Int (2000) 107(1-3), 225-232
Luca, A., Bermejo, A., Tabernero, M., Fernadez, P.,
Strano-Rossi, S.
30 min, immersed
563 Methadone, EDDP
Use of SPME for the determination of Methadone and
its main metabolite, EDDP, in plasma by GC-MS 100µm PDMS GC-MS
in plasma J. Anal. Toxicol. 24, 66-69 (2000) 30 min immersion
Bermejo, A., Seara, R., dos Santos Lucas, A.,
Tabernero, M., Fernandez, P., Marsili, R.
1:4 delution @ pH 9
474 Anorectics
SPME and GC analysis of anorectic compounds in
human urine GC-MS
in urine J.Microcolumn Sep. 1997, ((4), 249-252
Chiarotti, M. Strano-Rossi, S., Marsili, R.
Analysis of tetramethylene disulfotetramine in foods using SPME
2891 Tetramethylene gas chromatography-mass spectrometry 70 μm CW/DVB GC/MS
disulfotetramine J. Chromatogr. A 1192, #1, 36-40 (May 23 2008) headspace
in foods De Jager, Lowri S.; Diachenko, Gregory W.; Perfetti, Gracia A.
Determination of tetramethylenedisulfotetramine in human urine with
2715 Tetramine GC-flame thermionic detection coupling with direct immersed SPME 85µm polyacrylate GC-FPD
in human urine Forensic Sci. Int. 159, #2-3, 168-174 (2006-06-02)
Zeng, D.; Chen, B. ; Yao, S. Z.; Ying, J. Y.
immersed
Rapid detection of tetramethylenedisulfotertramine
645 Tetramine in human blood by SPME-GC 100µm PDMS GC-FPD
in blood Anal. Chim. Acta (2000), 404(2), 329-334
Luan, T., Li, G., Zhao, M., Zhang, Z.
SPME-GC-MS method for the determination of
930 Anesthetics inhalation anesthetics in urine 50:30µm DVB/Carboxen/ GC-MS
in urine J. Chromatogr. B (1999), 732(1) 115-125 PDMS
Poli, D., Bergamaschi, E., Maini, P., Andreoli, R., Mutti, A.
Detection of Ten Local Anesthetics in Human Blood Using
20min headspace
10% NaCl
65 Anesthetics Solid Phase Microextraction and Gas Chromatography 100µm PDMS GC-FID
in human blood Jpn. J. Forensic Toxicol. 13 (2): 182-188 (1995) 100°C, 40 min
Kumazawa, T., Lee, X., Sato, K., Seno, H., Ishii, A., Suzuki, D.
Extraction of Local Anesthetics from Human Blood
headspace
perchloric acid added
144 Anesthetics by Direct Immersion-SPME 100µm PDMS GC-FID
in blood Chromatographia 43: 59-62 (1996) 40 min
Kumazawa, T., Sato, K., Seno, H., Ishii, A., Suzuki, O. immersion
342 Anesthetics
Simple Analysis of Local Anesthetics in Human Blood Using
Headspace SPME and GC-MS-Electron Impact Ionization 100µm PDMS GC-MS
in human blood Selected Ion Monitoring 120°C, 45 min
J. Chromatog. B, 709 (1998), 225-232 headspace
Watanabe, T., Namera, A., Yaskiki, M., Iwasaki, Y., Kojima, T. NaOH added
Ambient temperature, unless otherwise indicated. 110