SPME Applications Guide - Overbrook Scientific

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1530 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Residual solvents in cocaine Forensics Gas chromatographic-mass spectrometric analysis of residual solvent trapped into illicit cocaine exhibits using head-space solid-phase microextraction Journal of Chromatography B (2002) 772(2), 249-256 headspace GC-MS Chiarotti, Marcello; Marsili, Remo; Moreda-Pineiro, Antonio 748 Review The use of SPME-GC in forensic analysis J. Chromatogr. Sci. (2000), 38(7), 297-306 Furton, K., Wang, J., Hsu, Y. Walton, J, Almirall, J. 500 Gasoline The detection and analysis of ignitable liquid residues extracted from human skin using SPME-GC 100µm PDMS GC-FID on skin Almirall, J., Wang, J., Lothridge, K, Furton, K. Characterization of SPME-GC for the analysis of gasoline tracers 15 min headspace 2733 Gasoline volatiles in different microenvironments. 75µm Carboxen GC-FPD in varied matries J Air Waste Manag Assoc 57, #3, 355-65 (2007 Mar) 10min Ceballos, Diana; Zielinska, Barbara; Fujita, Eric; Sagebiel, John air samples SPME samping of fire debris resideus in the presence of 2385 Fire debris radionuclide surrogate metals headspace GC-MS from surrogate Journal of Chromatography A 2007-03-23 22°C metals Duff, M., Crump, S., Keisha M. 2630 Ignitable liquids Forensic application of GC-differential mobility spectrometry with two-way classification of ignitable liquids from fire debris headspace GC-MS in fire debris Anal. Chem. 79, #17, 6752-6759 (Sep 1 2007) Harrington, Peter B.; Lu, Yao 85 Accelerants A Simple, Inexpensive, Rapid, Sensitive and Solventless Technique for the Analysis of Accelerants in Fire 100µm PDMS GC-FID in fire debris Debris Based on SPME 40°C, 20 min J. High Res. Chromatogr. 18: 625-629 (1995) Furton, K., Bruna, J., Almirall, J. headspace 105 Gasoline, kerosene Forensic Application of the SPME Method to the Analysis of Gasoline and Kerosene 100µm PDMS GC-NPD in fire debris Kaneko, T., Nakada, M. 22°C for 1 hr, or 80°C for 5 min headspace Multivariate pattern recognition of petroleum-based accelerants by 2430 Accelerants SPME-GC with flame ionization detection. headspace GC-FID Identification Anal. Chim. Acta 589, #2, 247-254 (2007-04-25) Bodle, E. S.; Hardy, J. K. 114 Accelerants Novel Method for Analysis of Gasoline from Fire Debris Using Headspace Solid Phase Microextraction 100µm PDMS GC-FID in fire debris J. Forensic Sci. 41: 12-22 (1996) Furton, K., Almirall, J., Bruna, J. 40°C, 20 min The Recovery of Accelerants in Aqueous Samples from Fire 115 Accelerants Debris Using SPME 100µm PDMS GC-FID in liquid residue Science & Justice 36 (4): 283-287 (1996) 20 min @ 40°C Almirall, J., Furton, K., Bruna, J. 143 Accelerants Determination of Liquid Accelerants in Arson Suspected Fire Debris Using Headspace SPME 100µm PDMS GC-FID in fire debris Anal. Commun. 33: 129 (1996) Steffen, A., Pawliszyn, J. A comprehensive sample preparation scheme for a 15 min @ 70°C headspace 594 Accelerants accelerants in suspect arson cases. GC, GC-MS in fire debris J-Forensic-Sci. May 1999; 44(3): 504-515 Ren,-QL; Bertsch,-W Immersion mode SPME ECD/GC and TEEM-GC/MS for analysis of Ambient temperature, unless otherwise indicated. 128
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2269 TNT in sand explosives buried in sand Immersion GC-ECD Proc SPIE Int Soc Opt Eng (2005) 5794 #II, 1272-1280 GC/MS Baez, B.; Briano, J.; Castro, M..; Correa, S.; De Echevarria, M. Hernandez-Rivera, S. 2270 TNT in sand Transport of explosives II: Use of Headspace-SPME/GC-ECD and TEEM GC/MS for detection of TNT vapors from sand buried samples Headspace GC-ECD Proc SPIE Int Soc Opt Eng (2005) 5794 #II, 1263-1271 Baez, B.; Briano, J.; Castro, M..; Correa, S.; De Echevarria, M. Hernandez-Rivera, S. GC/MS SPME sampling of high explosive resideus in the presence 2383 Explosive residue of radionuclides and radioneclide surrogate metals J Radioanalytical and Nuclear Chemistry -2007-04-13 Duff, M., Crump, S., Robert, R., Beals, D. Bioconcentration factor hydrophobicity cutoff: An artificial 2675 PAHs in phenomenon reconstructed aquatic worm ENVIRON. SCI. TECHNOL. 41, #21, 7363-7369 (01 NOV 2007) Jonker, M. T. O.; Van, Der Heijden S. A. 668 TNT, 2,4-DNT, RDX Development of field screening methods for TNT, 2,4-DNT, and RDX in soil. in soil Talanta, 39: 419-28 (1992) T Jenkens, et al 812 RDX, HMX Detection of the cyclic nitramine explosives hexahydro 1,3,5-trinitro-1,3,5-triazine (RDX) and octahydro-1,3,5,7- 65µm PDMS/DVB GC-MS in soil tetranitro-1,3,5,7-tetrazine (HMX) and their degradation 20MIN @55°c LC-MS products in soil environments J Chromatog A (2001) 909(1), 53-60 Hawari, J; Beaudet, S; Groom, C.; Halasz, A; Paquet, L PFBHA derivative 344 explosives Trace Analysis of explosives in Seawater Using SPME and GC-Ion Trap Mass Spectrometry 65µm Carbowax/DVB GC-MS in salt water Anal. Chem., Vol. 70, No. 14, July 15, 1998, pg. 3015-3020 60 min Barshick, S., Griest, W. immersion stirring Solid-phase microextraction coupled to GCfor the determination 2394 2,3-dimethyl-2,3- of 2,3-dimethyl-2,3-dinitrobutane as a marking agent for explosives headspace GC dinitrobutane Talanta 72, #4, 1581-1585 (2007-06-15) 30 sec @ 22°C from ammonium nitrate Li, X. J.; Zeng, Z. R.; Zeng, Y. Application of a SPME-IMS detection system for explosives detection 2284 Explosives Proc SPIE Int Soc Opt Eng Vol 5778 #2, 667-672 (2005) headspace GC/IMS in open areas. Almirall, Jose R.; Furton, Kenneth G.; Perr, Jeannette M. Discrimination of smokeless powders by headspace SPME-GC-MS 2285 Odors from and SPME-GC-ECD, and the potential implications upon training headspace GC-MS smokeless canine detection of explosives GC-ECD powders Proc SPIE Int Soc Opt Eng Vol 5778 #2, 638-643 (2005) Almirall, Jose R.; Furton, Kenneth G.; Harper, Ross J. 2370 Explosives SPME-HPLC: A new approach to the analysis of explosives J. HAZARD. MATER. 14, # 3, 691-697 (2007) Gaurav; Kaur, V.; Kumar, A.; Malik, A. K.; Rai, P. K. 65µm CW/DVB HPLC 669 Explosives Application of SPME to the recovery of explosives and ignitable liquid residues from forensic specimens 65µm Carbowax/DVB GC-ECD from solids, water J. Chromatogr A, 885(2000) 419-432 25 min, 25% NaCl HPLC Furton, K., Almirall, J., Bi, M., Wang, J., Wu, L. immersion stirring 592 explosives An improved interface for coupling SPME to HPLC applied to the analysis of explosives 50µm Carbowax/TPR HPLC-UV Ambient temperature, unless otherwise indicated. 129
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