SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
1552 Chlorophenols in water Journal of Chromatography A (2002) 947(2), 155-165 Various fibers compared HPLC-ELCD
1354
Aldehydes in drinking
water
Galceran, M. T.; Santos, F. J.; Sarrion, M. N.
Determination of aldehydes in drinking water using
pentafluorobenzylhydroxylamine derivatization and solid-phase microextraction
Journal of Chromatography A (2002) 943(1), 1-13
Ventura, Francesc; Cancho, Beatriz; Galceran, Ma. Teresa
65um DVB PDMS, onfiber
derivatization with
PFBHA
GC-ECD
1156 Chlorophenols
Solid-phase microextraction liquid chromatography/tandem mass spectrometry
for the analysis of chlorophenols in environmental samples.
Rapid Communications in Mass Spectrometry (2002) 17 (1), 39-48.
Sarrion, M. N.; Santos, F. J.; Moyano, E.; Galceran, M. T.*
Carbowax/TPR LC-TMS
1166
Simultaneous mercury and tin speciation in environmental samples by GC-
MIP/AES after preconcentration by solid phase microextraction
Mercury and tin in
environmental
samples. Journal De Physique. IV : JP (2003) 107 (II), 1423. PDMS GC-MIP/AES
Carrera, R.; De Diego, A.; Delgado, A.; Madariaga, J.; Sanz, J.; Zuloaga, O.
1074 Tributyltin
Improvement of measurement precision of SPME-GC/MS determination of
tributyltin using isotope dilution calibration.
Analytical Chemistry (2002) 74 (21), 5606-5613.
Bancon-Montigny, C.; Maxwell, P.; Yang, L.; Mester, Z.; Sturgeon, R. E.
GC-MS
Determination of methylphosphonic acid in water by SPME-GC
1952 Methyl Fenxi Ceshi Xuebao, 23, #1, 106-108 GC
phosphoric Yuan, L.; Xu, D. N.
acid in wate
Electrochemically controlled (EC) SPME based
1953 Nickle-cadmium on over oxidized sulfonate polypyrrole sulfortated polypyrrole ETAAS
from water Talanta, 67, #1,, 245-251 coated fiber
Ertas, N; Pekmez, K; Sahin, Y; Tamer, U Udum, Y.; immersed
Yildiz, A.
Risk assessment of domestic and industrial effluents
1954 Industrial unloaded into a freshwater environment GC-MS
effluent in Ecotoxicology & Environmental Safety, 61, #3, 380-391
freshwater Di Marzio, W.; Saenz, M.; Alberdi, J.;
Tortorelli, M.; Silvana, G.
Low part per trillion determination of reactive
1955 Alkanethiols alkanethiols in wastewater by in situ derivatization- N-ethylmaleimide GC-MS
in wastewater SPME followed by GC/MS derivatives
Anal. Chem., 77, #18, 6012-6018 immersion sampling
Alzaga, R.; Bayona, J.M.; Garcia-Jares, C.;
Llompart, M.; Salgado-Petinal, C.
2876 Alcohol
Sediment toxicity of a rapidly biodegrading nonionic surfactant:
Comparing the equilibrium partitioning approach with GC-MS
ethoxylates in measurements in pore water
marine sediment Env Sci & Tech. 42, #11, 4215-4221 (Jun 1 2008)
Droge, Steven T. J.; Hermens, Joop L. M.; Postma, Jaap F.
Analysis of freely dissolved alcohol ethoxylate homologues in various
2443 Ethoxylates seawater matrixes using solid-phase microextraction headspace GC
in seawater Anal. Chem. 79, #7, 2885-2891 (2007-04-01)
Droge, S. T.; Sinnige, T. L.; Hermens, J. L. M.
Determination of total chromium in seawater by
1956 Chromium in isotope dilution sector field ICPMS using GC s PDMS fiber ICPMS
seawater sample introduction TFA derivatives
Anal. Chem., 76, #13, 3510-3516 headspace
Abranko, L; Mester, ; Sturgeon, .; Yang, L
Ambient temperature, unless otherwise indicated. 171