SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
fruit juices pesticide residues in fruit juices by SPME-LC-MS 60µm PDMS/DVB
J. Chromatogr., A 1147, #2, 135-143 (2007-04-20)
Sagratini, G.; Manes, J.; Giardina, D.; Damiani, P.; Pico, Y.
90 min @ 20 C
2408 Pesticides in
Fast screening of pesticide residues in fruit juice by SPME
Food Chemistry 107, #3, 1314-1325 (2008) GC-MS
fruit juices Cortes-Aguado, S.; Sanchez-Morito, N.; Arrebola, F. J.;
Frenich, A. G.; Vidal, J. L. M
10 min
2498 Pesticides in
Screening method for the determination of parts per trillion levels
of pesticide residues in vegetables combining SPME-GC-MS 65µm PDMS/DVB GC-MS
vegetables Anal. Lett. 40, #13-15, 2886-2914 (2007-12) 10 min @ 20 C
Cortes Aguado, S.; Sanchez-Morito, N.; Garrido Frenich, A.;
Martinez Vidal, J. L.;
immersed
Validation of a SPME method for the
462 Organophosphorus determination of organophosphorus pesticides 100µm PDMS GC-FPD
pesticides in in fruits and fruit juice 3 min
fruit/fruit juices J. Chromatogr. A (1999), 843(1), 35-42 immersed
Simplicio, A, Vilas Boas, L.
SPME-HPLC-MS applied to the analysis of insecticides in honey.
2358 Insecticides in Food Addit Contam 25, #1, 59-69 (2008 Jan ) HPLC-MS
honey Blasco, C; Font, G; Picoo, Y
Determination of organophosphorus pesticides in honeybees
929 Organophosphorus after solid phase microextraction 85µm Polyacrylate GC-NPD
pesticides in J. Chromatogr. A (2001), 922(1-2) 257-265 45min @ 25°C
honeybees Fernandez, M., Padron, C., Marconi, L., Colombo, R. Ghinie, S. immersed
Sabatini, A, Girotti, S. stirred
463 Organochlorine &
A Systematic Approach to Optimize SPME
determination of Pesticides in Ethanol/Water
organophosphorus mixtures used as Food Simulates
in water/ethanol Anal. Chem. (1999), 71(13), 2417-2422
Batlle, R, Sanchez, C., Nerin, C.
616 Volatiles
Evidence for selectivity of absorption of volatile organics
compounds by PDMS SPME fiber 30µm PDMS GC-MS
in water J. Chromatogr. A,(2000) 885, 457-464 60min
Niedziella, S., Rudkin, S., Cooke, M. headspace
317 Aroma volatiles
Analysis of Aroma Release During Microwave Heating
J. Agric. Food Chem. 45 (11): 4388-4392 (1997) 60µm Carbowax/DVB GC-FID
in water traps Roberts, D., Pollien, R. 10 min
435 Aroma volatiles
SPME Associated with Microwave Assisted Extraction of
Food Products
in food products J. High Resolut. Chromatogr. (1997), 20(4), 213-216
Wang, Y., Bonilla, M., McNari, H., Khaled, M.
immersion, stirring
2400 1-naphthlamine
Application of microwave-assisted desorption/headspace SPME as
pretreatment step in the gas chromatographic determination of 65µm PDMS/DVB GC-FID
from silica gel 1-naphthylamine in silica gel adsorbent
Talanta 71, # , 1993-1997 (2007-03-30)
Yan, C. T.; Jen, J. F.; Shih, T. S.
headspace
2870 Volatiles from
Analysis of volatile compounds of Iberian dry-cured loins with
different intramuscular fat contents using SPME-DED headspace GC/MS
dry-cured Meat Science 79, #1, 172-180 (MAY 2008)
2583 Volatiles from
Effect of salt content and processing conditions on volatile compounds
formation throughout the ripening of Iberian ham headspace GC/MS
dry-cured Eur. Food Res. Technol. 225, #5-6, 677-684 (September 2007)
Iberian ham Andres, Ana I.; Cava, Ramon; Muriel, Elena; Ruiz, Jorge; Ventanas, S.
318 N-nitrosamines
Rapid Semi-Quantitative Estimation of N-Nitrosodibulylamine
and N-Nitrosodibenzylamine in Smoked Hams by SPME 85µm polyacrylate GC-thermal
Ambient temperature, unless otherwise indicated. 21