SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference
Biotransformation of (R)-(+)- and (S)-(-)-limonene by
Conditions Instrument
895 Volatile metabolites fungi and the use of SPME for screening.
from limonen Phytochemistry (Oxford) (2001) 57(2) 199-208
Demyttenaere, J.; De Kimpe, N; Van Belleghem, K
2730 Volatile
Fungal biotransformation of monoterpenes found in
agro-industrial residues from orange and pulp industries into : headspace GC
metabolites from aroma compounds screening using SPME
monoterpenes Food Sci Biotech 16, #1, 37-42 (2007)
Marostica, M. R., Jr.; Onoyama Mota, N.; Baudet, N.; Pastore, G. M.
802 Volatile metabolites
Biotransformation of geraniol, nerol and citral by sporulated
surface cultures of Aspergillus niger and Penicillium sp.
in penicillium fungi Phytochemistry (2000) 55(4), 363-373
Demyttenaere, J.,del Carmen Herrera, M.; De Kimpe, N
393 Volatiles in
Use of Digital Aroma Technology and SPME GC-MS to Compare
Volatile Compounds produced by Bacteria Isolated from 100µm PDMS GC-MS
bacteria on poultry Processed Poultry 37°C, 30 min
J. Sci Food Agric. 1998, 78, 343-348
Arnold, J., Senter, S.
headspace
664 Volatiles in
Evaluation of SPME for the Isotopic Analysis of volatile
compounds produced during fermentation by lactic 70µm Carboxen/PDMS GC-C-IRMS
lactic acid bacteria acid bacteria 10 min
J. Agric Food Chem. 2000, 48, 2222-2227 headspace
Goupry, S., Rochut, N., Robins, R., Gentil, E. salt added
570 Fatty acid esters
Headspace SPME with l-pyrenyldiazomethane in-fiber
derivatization for analysis of fecal short-chain fatty acids 85µm polyacrylate GC-EMIS
in faeses J-Chromatogr,-B:-Biomed-Appl. 25 Jun 1999; 730(1): 113-122 15 min
Mills,-GA; Walker,-V; Mughal,-H
Determination of Cannabinoids in Water and Human Saliva by
1-pyrenyldiazomethane
derivative
335 Cannabinoids SPME and Quadrupole Ion Trap GC-MS 30µm PDMS GC-MS
in water/saliva Anal. Chem. 70 (9): 1788-1796 (1998) 10 min
Hall, B., Satterfield-Doeerr, M., Parikh, A., Brodbelt, J. immersion
665 Dibenzylamine
Direct comparison of SPE and SPME for the GC
determination of dibenzylamine in artificial saliva 85µm polyacrylate GC-MS
in saliva leachates from baby bottle teats
Anal Chim Acta 2000, 414(1-2), 133-140
Niessner, G., Klampfl, C.
pH 10
Extraction and analysis of different Cannabis samples by
2185 Cannabinoids headspace SPME combined with GC-MS headspace GC-MS
from Cannabis J SepSci. 28, #17, 2293-2300 (2005)
samples Ilias, Y.; Rudaz, S.; Mathieu, P.; Christen, P.; Veuthey, Jean
340 Cannabinoids
Solid-Phase Microextraction for Cannabinoids Analysis in Hair
and Its Possible Application to Other Drugs 30µm PDMS GC-MS
in hair J. Anal. Toxicology, Vol. 23, Jan./Feb. 1999 15 min, immersion
Strano-Rossi, S., Chiarotti, M.
Use of headspace SPME in hair analysis for
hair digested with
1N NaOH
666 Lipophilic drugs organic compounds
in hair Forensic Sci. Int. (2000), 107(1-3), 129-148 headspace
Sporkiert, F., Pragst, F. hair digested with
4% NaOH
941 Lipophilic drugs
Analysis of hair by headspace SPME and GC-MS.
Chromatogr Separation Tech (2001), 17(2), 4-8 headspace
in hair Pragst, F
SPME in Forensic Toxicology
hair digested with
4% NaOH
336 Review of use Jpn. J. Forensic Toxicol. 16 (1): 1-15 (1998) various fibers
Ambient temperature, unless otherwise indicated. 125