SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Use of SPME with Ion Mobility Spectrometry Conditions stirring, KNO3 added Instrument 182 Anal. Lett. 30 (7): 20-22 (1997) Orzechowsa, G., Poziomek, E., Tersol, V. GC-MS 2610 VOCs Occurrence of volatile organic compounds (VOCs) in Liverpool Bay, Irish Sea headspace GC-MS in seawater Mar. Pollut. Bull. 54, #11, 1742-1753 Bravo-Linares, C.M.; Loyola-Sepulveda, R.H.; Mudge, S.M 228 VOCs SPME of Volatile Organic Compounds. Estimation of the Sorption Equilibrium from the Kovats Index Effect of Salinity 100µm PDMS GC-FID in seawater and Humic Acids and the Study of the Kinetics by the 45 min Development of an "Agitated/Static Layer" Model immersion J. Chromatogr. A 761: 205-217 (1997) stirring Dewulf, J., Everaert, M., Van-Langenhove, H. salt added 840 Squalene Determination of squalene in seawater by SPME-GC-MS and the concentration variation of squalene in redtide seawater. 100µm PDMS GC-MS in seawater Fenxi Huaxue (2000) 28(11) 1326-1330 45 min Zhao, M. Q.; Li, G. K.; Luan, T. G.; Zhang, Z. X. Development of a Prototype System for Quasi-Continuous immersion stirring 165 Triazines, organic Analysis of Organic Contaminants in Surface or Sewage 85µm polyacrylate GC-ECD, -FID pesticides Water Based on In-Line Coupling of SPME to GC 10 min in sewage water J. Chromatogr. A 737 (1): 59-65 (1996) Eisert, R., Levsen, K. 300mL/min flow 166 Pesticides Design of Automated SPME for Trace Analysis of Organic Compounds in Aqueous Samples 100µm PDMS GC-FID in water J. Chromatogr. A 776: 293-303 (1997) 30 min Eisert, R., Pawliszyn, J. stirring 184 BTEX, Sample Preparation for GC with SPE & SPME Chromatogr. 37: 205-236 (1997) 100µm PDMS GC-FID pesticides Penton, Z. 2-20 min in water Porous-Layer Solid-Phase Microextraction Using Silica immersion, stirring salt added 236 Aromatic Bonded Phase 30µm C8 silica bonded GC-FID hydrocarbons Anal. Chem. 69: 190-195 (1997) metal fiber in water Liu, Y., Shen, Y., Lee, M. High Temperature Water Extraction Combined with SPME 20 min stirring 189 PAHs in Anal. Commun. 33: 421-424 (1996) 30µm PDMS GC-FID water extract Daimon, H., Pawliszyn, J. Initial Bandwidth Resulting from Splitless and Solid-Phase 70 min stirring 220 C6-C11 hydrocarbons Microextraction Gas Chromatographic Injections 100µm PDMS GC-FID in water J. High Res. Chromatogr. 20 (2): 77-80 (1997) 10 min Snow, N., Okeyo, P. Optimizing Split/Splitless Injection Port Parameters for SPME immersion stirring 138 PAHs in J. Chromatogr. A 740 (1): 139-145 (1996) 7µm & 100µm PDMS GC-FID water Langenfeld, J., Hawthorne, S., Miller, D. Nitro Musks in Cosmetic Products: Determination by 5 hr immersion, stirring 211 Nitro musk compounds Headspace SPME and GC with Atomic Emission Detection: 100µm PDMS GC-AID in cosmetic products Dynamics of Organic Compound Extraction from Water, 1-60 min Using Liquid-Coated Fused Silica Fibers Chromatogrphia 45; 138-144 (1997) Struppe, C., Schaefer, B., Engewald, W. headspace Dynamics of Organic Compound Extraction from Water, Using Ambient temperature, unless otherwise indicated. 216
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 243 Liquid-Coated Fused Silica Fibers Anal. Chem. 66: 1186-1199 (1994) Arthur, C., Pawliszyn, J. 437 Review SPME and Its Utilization in Environmental Analysis Chem. Listy (1998), 92(8), 633-642 Sedlakova, J., Matisova, E., Slezackova, M. New materials in sorptive extraction techniques for polar compounds 2592 Review articles J. CHROMATOGR. A 1152, #1-2, 14-31 (08 JUN 2007) Fontanals, N.; Marce, R. M.; Borrull, F. 549 Review of 52 refs. Trends in SPME for determining organic pollutants in environmental samples Trends Anal. Chem. 1999, 18(8), 557-568 Penalver, A., Pocurull, E., Borrull, F., Marce, R. Varied Advances in Extraction Technology: A report from Extech '99 550 Proceeding of Extech LC-GC Current Trends and development in Sample Prep, Sept. 1999, Vol. 17., No. 90, S25-S30 Lord, H., Pawliszyn, J. Varied 551 Overview of SPME Sample Preparation for GC with SPE and SPME Advances in Chromatography, Vol. 37, 1966, 205-236 Book chapter by M. Dekker, New York, 1996 Penton, Z. Solid Phase Microextraction -- A Unique Tool for 244 Chemical Measurements Can. J. Chem. 74: 1297-1308 (1996) Gorecki, T., Boyd-Boland, A., Zhang, Z., Pawliszyn, J. Solvent Free Sample Preparation Techniques Based on Fiber 245 and Polymer Technologies Environ. Sci. Technol. 28: 569A-574A (1994) Boyd-Boland, A., Chai, M., Luo, Y., Zhang, Z., Yang, M., Gorecki, T., Pawliszyn, J. 246 BTEX, Solid Phase Microextraction Tech. Aquat. Toxicol. 459-477 (1996) 100µm PDMS GC-FID, -ECD pesticides Webster, G., Sarna, L., Graham, K. 10-30 min in water Solid Phase Microextraction Technique for Gas immersion stirring 247 Chromatography overview Huaxue 54 (3): 119 (1996) Huang, S. article 248 BTEX, Sample Preparation for Gas Chromatography with SPE and SPME 100µm PDMS GC-FID pesticides Adv. Chromatogr. (N.Y.) 37: 205-236 (1997) 2-20 min in water Penton, Z. Solid Phase Microextraction-SPME, State of the Art immersion, stirring salt added 249 BTEX, Chromatography Kaiser, O. (Ed.) Incom, Dusseldorf, 100µm PDMS GC-FID pesticides pp153-166 (1997) 2-20 min in water Kern, H., Penton, Z. immersion, stirring 2493 Contaminants Potential sources of background contaminants in solid phase extraction and microextraction 70µm CW/DVB in SPME process J Separation Sci. 30, #7, 1029-1036 (MAY 2007) Stiles, R.; Yang, Ill; Lippincott, R.; Murphy, E.; Buckley, B. 250 Reference book Solid Phase Microextraction: Theory and Practice VCH, New York, 275pp (1997) various fibers Ambient temperature, unless otherwise indicated. 217
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SPME Applications Guide - Overbrook Scientific

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