SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 576 Chlorobenzenes compounds in water 100µm PDMS GC-ECD in water Lihua-Jianyan,-Huaxue-Fence. Mar 1999; 35(3): 103-105 5 min, agitated Yang,-HB Trace analysis of ten chlorinated benzenes in water 0.5gm NaOH immersed 697 Chlorinated by headspace SPME 100µm PDMS GC-MS benzenes in J. Chromatogr. A (2000) 874(1), 149-154 headspace water He, Y., Wang, Y., Lee, H. salt, agitated 698 Fungicides Determination of fungicides in natural waters using SPME and GC coupled with ECD and MS detection 100µm PDMS GC-MS in water J. Chromatorgr A., 893 (2000), 143-156 30 min, agitated Lambropoulou, D., Konstantinou, I., Albanis, T. New cloud vapor zone (CVZ) coupled headspace SPME technique 20% NaCl, pH 4 immersed 2527 Chlorothalonil Anal Bioanal Chem 388, #2, 377-83 (2007 May) 100µm PDMS in water Huang, Yi-Ching; Su, Yi-Song; Muniraj, Sarangapani; Zhang, W.; Jen, J. 5°C headspace 699 Chlorothalonil Determination of aqueous chlorothalonil with SPME-GC J. Chromatogr. A, 896 (2000) 105-110 100µm PDMS GC-ECD in water Chen, S., Su, Y., Jen, J. 40 min, 800 Alachlor Optimization of alachlor solid-phase micro-extraction from water samples using experimental design. 60µm PDMS/DVB HPLC in water J. Chromatogr. A (2000) 896(1-2), 373-379 120min @ 25°C Gonzalez-Barreiro, C.; Lores, M.; Casais, M. C.; Cela, R. stirred 2786 Pyrethroids in Simultaneous determination of traces of pyrethroids, organochlorines and other main plant protection agents in agricultural soils 85µm polyacrylate GC-µECD soil by headspace SPME-GC-MS headspace J. Chromatogr. A, 1188, #2, 154-163 (Apr 25 2008) 100 °C Cela, R.; Dagnac, Thierry; Fernandez-Alvarez, M.; Garcia-Jares, C.; Lamas, J.; Llompart, Maria; Lores, Marta Application of SPME for determination of pyrethroids in groundwater 2787 Pyrethroids in using LC with post-column photochemically induced 60µm PDMS/DVB LC fluorescencene groundwater fluorimetry derivatization and fluorescence detection fluorimetry J. Chromatogr. A, 1188, #2, 61-68 (Apr 25 2008) Galera, M. Martinez; Mughari, Ahmed R.; Vazquez, P. Parrilla derivatization 2403 Chloroacetanilide Analysis of chloroacetanilide herbicides in water samples by SPME-GC-MS Anal. Chim. Acta 591, #1, 87-96 (2007-05-15) GC-MS herbicides in water Xu, X. Q.; Yang, H. H.; Wang, L.; Han, B.; Wang, X. R.; Lee, F. S.-C Gas-Phase Post-Derivatization Following SPME for 293 Acidic herbicides Determining Acidic Herbicides in Water 85µm polyacrylate GC-MS in water Anal. Chem. 70 (9): 1963-1968 (1998) 50 min Lee, M., Lee, R., Lin, Y., Chen, C., Hwang, B. immersion, stirring pH 1, salt added diazomethane (deriv.) 905 Acidic herbicides Derivatisation/SPME followed by GC-MS for the analysis of phenoxy acid herbicieds in aqueous samples GC-MS in water J. Chromatogr. A (1998),826(2), 211-216 Nilsson, T., Baglio, D., Miguez, I., Madsen, J., Facchetti, S. 898 Acidic herbicides Automated on-line in-tube SPME followed by LC/electrospray ionization mass spectrometry for the determination of LC-MS in water chlorinated phenoxy acid herbicides in environmental waters Analyst (Cambridge, U. K.) 2001 , 126(5) 602-608 Takino, Masahiko; Daishima, Shigeki; Nakahara, Taketoshi Ambient temperature, unless otherwise indicated. 160
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 763 Profoxydim Application of on-site SPME in aquatic dissipation studies of profoxydim in rice 50µm Carbowax-TPR HPLC-UV in water J. Chromatogr A, 909 (2001) 29-36 30min. Eisert, R, Jackson, S., Krotzky, A. SPME of the antifouling Irgarol 1051 and fungicides salt added immersed 521 Fungicides dichlofluanid and 4-chloro-3-methylphenol in water samples 85µm polyacrylate GC-MS in water J. Chromatogr. A, (1999), 839(1+2), 253-260 1 hr. @ 60°C Penalver, A., Pocurull, E., Borrull, F., Marce, R. immersion, salt added 568 T2 mycotoxin Determination of trichothecene (T2 mycotoxin) in aqueous sample with solid-phase microextraction technique 85µm polyacrylate GC-FID in water followed by GC-FID 75 min, immersed J-High-Resolut-Chromatogr. Jul 1999; 22(7): 424-426 satr. salt Lee,-PK; Kee,-SYK; Ng,-W; Gopalakrishnakone,-P stirred 294 PAHs SPME of PAHs from Aqueous Samples, Using Fibers Coated with HPLC Chemically Bonded Silica Stationary Phases 100µm silica/epoxy GC-FID, -MS in water Anal. Chem. 69 (24): 5001-5005 (1997) 60°C, 30 min Liu, Y., Lee, M., Hageman, K., Yang, Y, Hawthorne, S. headspace 295 PAHs Separation and Determination of Polycyclic Aromatic Hydrocarbons by SPME/Cyclodextrin-Modified Capillary Electrophoresis Anal. Chem. 69 (9): 1726-1731 (1997) Nguye, A., Luong, J. 700 PAHs Monitoring of PAH in water using headspace SPME and capillary GC in water Microchem J. (1999), 63(2), 276-284 Djozan, D., Assadi, Y. 701 PAHs SPME for determining the distribution of sixteen USEPA polycyclic aromatic hydrocarbons in water samples in water J. Chromatogr. A. (2000) 879, 177 Doong, R., Chang, S., Sun, Y. Determination of Aromatic Compounds in Water by SPME 296 Aromatics and Ultraviolet Absorption Spectroscopy PDMS chip UV spectroscopy in water Anal. Chem. 69 (1): 1197-1203 (1997) 30-50 min 220-300nm Wittkamp, B., Hawthorne, S., Tilotta, D. immersion Trace Analysis of salt in Seawater Using SPME and 344 RDX, TNT metabolites GC-Ion Trap Mass Spectrometry Carbowax/DVB GC-MS in salt water Anal. Chem., Vol. 70, No. 14, July 15, 1998, pg. 3015-3020 10 min Barshick, S., Griest, W. immersion stirring Characterization of Water-Soluble Components of Slurries 297 Phthalates, surfactants Using SPME Coupled to LC-MS 65µm Carbowax/TPR LC-MS in water J. Microcolumn Sep. 10 (2): 225-234 (1998) 1-15 hr. Moder, M., Popp, P., Pawliszyn, J. pH 2, satr. salt 598 Organophosphorus Comparative studies of the leachate of an industrial landfill by GC-MS,LC-nuclear magnetic resonance and LC-MS GC-MS compounds J-Chromatogr,-A. 29 Jan 1999; 831(2): 243-256 in leachate Benfenati,-E; Pierucci,-P; Fanelli,-R; Preiss,-A Godejohann,-M; Astratov,-M; Levsen,-K; Barcelo,-D Development of a headspace SPME procedure for the 702 Fatty acids determination of free volatile fatty acids in waste wate 85µm Carboxen/PDMS GC-FID, MS in waste water J Chromatogr. A,(2000) 873(1), 107-115 headspace Abalos, M., Bayona, J., Pawliszyn, J. stirring 703 Fatty acids Application of GC coupled to chemical ionisation MS following headspace SPME for the determination of free volatile 85µm Carboxen/PDMS GC-CI-MS in water fatty acids in aqueous samples. 20 min headspace Ambient temperature, unless otherwise indicated. 161
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SPME Literature Literature No. Titl
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