TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Environmental Applications, Pesticides and Herbicides
CLP Pesticides
Column: DB-35ms
123-3832
30 m x 0.32 mm, 0.25 µm
Column: DB-XLB
123-1236
30 m x 0.32 mm, 0.50 µm
Carrier: Helium at 45 cm/sec (EPC in constant flow mode)
Oven: 110°C for 0.5 min
110-320°C at 15°C/min
320°C for 2 min
Injection: Splitless, 250°C
30 sec purge activation time
Detector: µECD, 350°C
Nitrogen makeup gas
(column + makeup flow = 30 mL/min constant flow)
Sample: 50 pg per component
DB-35ms
1
2
3
4
5 6
Time (min)
Complete resolution and confirmation of 22 CLP Pesticides in under 16 minutes!
362 www.agilent.com/chem/supplies
7
8 9 10
12
13
11
14
15 16
18
17
19
6 8 10 12 14 16
DB-XLB
1
2
3
4
6
5
7
9 10 11
8
20
21
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Splitless, single taper, deactivated, 4 mm ID, 5181-3316
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
22
GCEP001
6 8 10 12 14 16
Time (min)
GCEP002
12
13
14
16
15
18 19
17
20
21
22
1. Tetrachloro m-xylene (SS)
2. α-BHC
3. γ-BHC
4. b-BHC
5. Heptachlor
6. δ-BHC
7. Aldrin
8. Heptachlor epoxide
9. γ-Chlordane
10. α-Chlordane
11. Endosulfan I
12. 4,4'-DDE
13. Dieldrin
14. Endrin
15. 4,4'-DDD
16. Endosulfan II
17. 4,4'-DDT
18. Endrin aldehyde
19. Endosulfan sulfate
20. Methoxychlor
21. Endrin ketone
22. Decachlorobiphenyl (SS)
SS - Surrogate Standard