TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Industrial Chemical Applications
Phenols III
Column: DB-WAX
122-7032
30 m x 0.25 mm, 0.25 µm
Carrier: Hydrogen at 43 cm/sec
Oven: 165°C isothermal
Injection: Split, 250°C
Split ratio 1:50
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Split, single taper, low pressure drop, glass wool, 5183-4647
Seal: Gold plated seal, 18740-20885
Syringe: 5 µl tapered, FN 23-26s/42/HP, 5181-1273
Halocarbons
Column: GS-GasPro
113-4332
30 m x 0.32 mm
Carrier: Helium at 30 cm/sec
Oven: 130°C for 4 min
130-225°C at 10°/min
225°C Hold
Injection: Split, 250°C
Split ratio 1:67
Detector: FID, 250°C
Sample: 1 µL
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Direct, 1.5 mm ID, 18740-80200
Seal: Gold plated seal, 18740-20885
Time (min)
444 www.agilent.com/chem/supplies
0
1
2
3
1
4
2
3
11.5 min
5
6 7
6, 7
4 5
8
9
8
9
10
10
11, 12
1. CH4
2. CHCIF2 (Freon 22)
3. CCI2F2 (Freon 12)
4. CICF2 CF2 Cl (Freon 114)
5. CHCI2 F (Freon 21)
6. CCI3F (Freon 11)
7. CF2Br2 (Freon 12B2)
8. CH3I
9. CH2CI2
10. trans-CICH=CHCI
11. CF3CCl3 (Freon 113)
12
13
17
18
19
15
11
20
14 16
13 14
GCIC054
21 22
1. 2,6-Xylenol
2. 2-Cresol
3. Phenol
4. 2-Ethylphenol
5. 2,5-Xylenol
6. 4-Cresol
7. 2,4-Xylenol
8. 3-Cresol
9. 2-Isopropylphenol
10. 2,3-Xylenol
11. 3,5-Xylenol
12. 4-Ethylphenol
13. 3,4-Xylenol
14. 2,3,5-Trimethylphenol
16 18
GCIC055
12. cis-CICH=CHCI
13. CHCI3
14. ? from CCI4
15. CCI4
16. ? from CCI4
17. CH3CH2I
18. CH2Br2
19. CHCI2Br
20. C4F9I
21. CHCIBr2
22. CH3CH2CH2I