TABLE OF CONTENTS - BGB Analytik AG

PFBHA Derivative
Column: DB-1
123-1012
15 m x 0.32 mm, 0.25 µm
Carrier: Helium at 40 cm/sec,
measured at 60°C
Oven: 60-100°C at 10°C/min
Injection: Split, 250°C
Split ratio 1:100
Detector: FID, 375°C
Nitrogen makeup gas at 35 mL/min
Aromatics I
Column: DB-1
125-1034
30 m x 0.53 mm, 3.00 µm
Carrier: Helium at 30 cm/sec,
measured at 40°C
Oven: 40°C for 5 min
40-260°C at 10°C/min
Injection: Split, 250°C
Split ratio 1:10
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: General Purpose Split/Splitless Liner, taper, glass wool, 5183-4711
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
CS2
1
2
3
1. Formaldehyde-PFBHA
www.agilent.com/chem/supplies
Industrial Chemical Applications
0 1 2
Time (min)
3 4
0 5
10 15 20 25
Time (min)
4 5
12, 13, 14, 15
6, 7
1. Benzene
2. Fluorobenzene
3. Toluene
4. Chlorobenzene
5. Ethylbenzene
6. m-Xylene
7. p-Xylene
8. Styrene
9. o-Xylene
10. Isopropylbenzene (cumene)
11. Bromobenzene
12. Propylbenzene
13. 2-Chlorotoluene
14. 3-Chlorotoluene
15. 4-Chlorotoluene
16. 1,3,5-Trimethylbenzene (mesitylene)
17.
18. tert-Butylbenzene
19. 1,2,4-Trimethylbenzene (pseudocumene)
20. 4-Methylstyrene
21. 1,3-Dichlorobenzene
8
9
1011 18, 19, 20
21
17
16
22, 23
30, 31
24 28, 29
25
26
36
27
35
32 37
34 38
33
39
41 40
42 43
1
GCIC018
GCIC017
22. 1,4-Dichlorobenzene
23. Isobutylbenzene
24. sec-Butylbenzene
25. 1,2,3-Trimethylbenzene (hemimellitene)
26. 1,2-Dichlorobenzene
27. Iodobenzene
28. Styrene oxide
29. Butylbenzene
30. 4-Chlorostyrene
31. Nitrobenzene
32. 4-tert-Butyltoluene
33. 1,3,5-Trichlorobenzene
34. 2-Nitrotoluene
35. 1,3-Diisopropylbenzene
36. 1,4-Diisopropylbenzene
37. 1,2,4-Trichlorobenzene
38. 3-Nitrotoluene
39. 4-Nitrotoluene
40. 1,2,3-Trichlorobenzene
41. 1-Chloro-4-nitrobenzene
42. 1,2,4,5-Tetrachlorobenzene
43. Pentachlorobenzene
GC and GC/MS
425