TABLE OF CONTENTS - BGB Analytik AG

Sulfonamides - Fast Analysis with RRHT Columns
Column: SB-C18
824700-902
2.1 x 30 mm, 1.8 µm
824700-902
Mobile Phase: A: 90% 0.1% formic acid
B: 10% 0.1% formic acid in MeOH
Flow Rate: A: 0.2 mL/min
B: 0.8 mL/min
Temperature: 35°C
Detector: TIC, Single Quad
Sample: Sulfonamides
Fast Analysis of Pindolol
Column A: ZORBAX SB-CN
863953-905
4.6 x 150 mm, 3.5 µm
Column B: ZORBAX SB-CN
827975-905
4.6 x 50 mm, 1.8 µm
827975-905
Mobile Phase: A: 70% 50 mM NaAcetate
B: 30% ACN
Flow Rate: 1 mL/min
Temperature: Ambient
Detector: UV 219 nm
Sample: Pindolol, 2 µL
300000
250000
200000
150000
100000
50000
300000
250000
200000
150000
100000
50000
A
B
1
2
1 2
3
0.2 mL/min
3
4
1 2 3 4
Time (min)
5 6 7 8
4
5
0.8 mL/min
1 2 3 4
Time (min)
5 6 7 8
A
B
1 2
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Pharmaceutical Applications
1. Sulfanilamide
2. Sulfadiazine
3. Sulfathiazole
4. Sulfamerazine
5. Sulfamethazine
1 2
2 4 6
Time (min)
8 10
1. Indole
2. Pindolol
2 4 6
Time (min)
8 10
5
LCPC050
LCPC051
LC and LC/MS
791