TABLE OF CONTENTS - BGB Analytik AG
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TABLE OF CONTENTS - BGB Analytik AG

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Nitrogen/Phosphorus Containing Pesticides,<br />

EPA Method 507<br />

Column: HP-5ms<br />

19091S-433<br />

30 m x 0.25 mm, 0.25 µm<br />

Carrier: Helium, 30 cm/sec (13.6 psi) pressure<br />

program<br />

Oven: 80-178°C at 30°C/min<br />

178°C for 4 min<br />

178-205°C at 2°C/min<br />

205-310°C at 30°C/min<br />

310°C for 4 min<br />

Injection: Splitless, 260°C<br />

1 min purge delay<br />

Detector: NPD, 290°C<br />

Helium makeup gas at 30 mL/min<br />

Suggested Supplies<br />

Septum: 11 mm Advanced Green septa,<br />

5183-4759<br />

Liner: Direct connect, single taper,<br />

deactivated,<br />

4 mm ID, G1544-80730<br />

Syringe: 10 µl tapered, FN 23-26s/42/HP,<br />

5181-1267<br />

Organophosphorous Pesticides I,<br />

EPA Method 8141A<br />

Column: DB-5ms<br />

122-5532<br />

30 m x 0.25 mm, 0.25 µm<br />

Carrier: Helium at 35 cm/sec, measured at 50°C<br />

Oven: 50°C for 1 min<br />

50-100°C at 25°/min<br />

100-300°C at 5°/min<br />

300°C for 5 min<br />

Injection: Splitless, 250°C<br />

30 sec purge activation time<br />

Detector: MSD, 300°C transfer line<br />

Full scan m/z 50-500<br />

Sample: 1 µL of 40 µg/mL 8141A standards<br />

Accustandard Inc.<br />

Suggested Supplies<br />

Septum: 11 mm Advanced Green septa,<br />

5183-4759<br />

Liner: Splitless, single taper, deactivated,<br />

4 mm ID, 5181-3316<br />

Syringe: 10 µl tapered, FN 23-26s/42/HP,<br />

5181-1267<br />

Note: All standards used were supplied courtesy of<br />

Accustandard Inc., 25 Science Park, New Haven, CT<br />

06511, 800-442-5290.<br />

1<br />

Environmental Applications, Pesticides and Herbicides<br />

1<br />

0 5<br />

10 15 20 25<br />

Time (min) GCEP014<br />

2<br />

2 5 7<br />

3 6<br />

8<br />

3<br />

4<br />

9<br />

4<br />

10<br />

11<br />

13<br />

12<br />

14<br />

15<br />

16<br />

17<br />

20<br />

10 15 20 25 30<br />

35<br />

Time (min) GCEP015<br />

www.agilent.com/chem/supplies<br />

19<br />

5<br />

10<br />

18<br />

21<br />

1. 4-Chloro-3-nitrotrifluoride<br />

2. Dichlorovos<br />

3. Hexamethylphosphoramide<br />

4. Mevinphos<br />

5. TEPP<br />

6. Thionazin<br />

7. Demeton-O<br />

8. Ethoprop<br />

9. Naled<br />

10. Dicrotophos<br />

11. Sulfotepp<br />

12. Monocrotophos<br />

13. Phorate<br />

8<br />

14. Dimethoate<br />

15. Demeton-S<br />

7<br />

16. Simazine<br />

6<br />

22<br />

11<br />

12<br />

9<br />

1. Dichlorvos<br />

2. EPTC<br />

3. Butylate<br />

4. Mevinphos<br />

5. Vernolate<br />

6. Pebulate<br />

7. Tebuthiuron<br />

8. Molinate<br />

9. Ethoprop<br />

10. Cycloate<br />

11. Chlorpropham<br />

12. Atraton<br />

23<br />

24<br />

13<br />

25, 26<br />

14, 15<br />

17<br />

16<br />

18<br />

20<br />

27<br />

28<br />

19<br />

30<br />

29 31<br />

21<br />

22<br />

27<br />

30<br />

24<br />

23<br />

32<br />

17. Atrazine<br />

18. Dioxathion<br />

19. Terbufos<br />

20. Fonofos<br />

21. Diazinon<br />

22. Disulfoton<br />

23. Phosphamidon<br />

24. Dichlofenthion<br />

25. Chlorpyrifos-methyl<br />

26. Methyl parathion<br />

29<br />

25 26<br />

28<br />

31<br />

32<br />

35<br />

34<br />

33<br />

36<br />

37<br />

34<br />

13. Simazine<br />

14. Prometon<br />

15. Atrazine<br />

16. Propazine<br />

17. Terbufos<br />

18. Pronamide<br />

19. Diazinon<br />

20. Disulfoton<br />

21. Terbacil<br />

22. Metribuzin<br />

23. Simetryn<br />

24. Alachlor<br />

33<br />

35<br />

38<br />

39<br />

36<br />

37<br />

38<br />

39<br />

40<br />

40<br />

41<br />

27. Ronnel<br />

28. Fenitrothion<br />

29. Malathion<br />

30. Aspon<br />

31. Chlorpyrifos<br />

32. Fenthion<br />

33. Ethyl parathion<br />

34. Trichloronate<br />

35. Chlorfenvinphos<br />

36. Crotoxyphos<br />

37. Stirophos<br />

41 42<br />

44<br />

43<br />

42<br />

25. Ametryn<br />

26. Prometryn<br />

27. Terbutryn<br />

28. Bromacil<br />

29. Metolachlor<br />

30. Triademefon<br />

31. MGK-264<br />

32. Diphenamid<br />

33. Stirofos<br />

34. Butachlor<br />

35. Fenamiphos<br />

36. Napropamide<br />

37. Tricyclazole<br />

38. Merphos<br />

39. Carboxin<br />

40. Norflurazon<br />

41. Hexazinone<br />

42. Fenarimol<br />

43. Fluridone<br />

45<br />

43<br />

38. Tokuthion<br />

39. Merphos<br />

40. Fensulfothion<br />

41. Ethion<br />

42. Bolstar<br />

43. Famphur<br />

44. Carbophenothion<br />

45. Phosmet<br />

46. EPN<br />

47. Leptophos<br />

48. Azinphos methyl<br />

49. Tri-o-cresyl phosphate<br />

50. Azinphos ethyl<br />

51. Coumaphos<br />

* Breakdown products<br />

47<br />

48<br />

46<br />

49<br />

50<br />

51<br />

GC and GC/MS<br />

369

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