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TABLE OF CONTENTS - BGB Analytik AG

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LC and LC/MS<br />

ZORBAX Eclipse PAH<br />

High Resolution and Fast Analysis<br />

on RRHT Eclipse PAH Column<br />

Column: 959941-918<br />

4.6 x 50 mm, 1.8 µm<br />

Mobile Phase: A = Water;<br />

B = Acetonitrile<br />

Gradient: Time (Min) % B<br />

0.00 40<br />

3.5<br />

100<br />

5.2<br />

100<br />

5.5<br />

40<br />

6.5<br />

40<br />

Flow Rate: 2.0 mL/min<br />

Temperature: 25º C<br />

Detector:<br />

Stop Time = 7.0<br />

DAD 220,4 nm No Ref.<br />

DAD Stop Time = 6.0 min<br />

ZORBAX Eclipse PAH<br />

594 www.agilent.com/chem/supplies<br />

• High resolution separation of 16 PAHs in EPA 610.<br />

• Extensive range of particle sizes (1.8, 3.5 and 5 µm) and sizes for fast and high resolution<br />

separations.<br />

• Each batch of material is specifically tested with PAHs for maximum reproducibility under<br />

expected operating conditions.<br />

• Excellent performance using the high, quality, improved silica of the Eclipse Plus columns.<br />

• Good for applications requiring "shape selectivity" or the separation of geometric isomers.<br />

Agilent ZORBAX Eclipse PAH columns are recommended for the separation of polycyclic<br />

aromatic hydrocarbons. PAHs are considered priority pollutants and the analysis of these<br />

potentially carcinogenic compounds in water, soil and food is of major importance. The Eclipse<br />

PAH columns separate all of the 16 PAHS in EPA method 610 quickly with high resolution.<br />

Column Specifications<br />

Pore Surface Temp. pH<br />

Carbon<br />

Bonded Phase Size Area Limits Range Endcapped Load<br />

ZORBAX Eclipse PAH 95Å 160 m2/g 60°C 2.0-8.0 No 14%<br />

Specifications represent typical values only.<br />

mAU<br />

2000<br />

1750<br />

1500<br />

1250<br />

1000<br />

750<br />

500<br />

250<br />

0<br />

Rs = 2.2 vs. 2.0 for<br />

4.6 x 50 mm, 3.5 µm<br />

Rs = 2.2<br />

1 2 3<br />

Time (min)<br />

4 5<br />

LCEPlusPAH

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